Verfügbarkeit: Solid state chemistry

Solid state chemistry: an introduction

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Bibliographische Detailangaben
Hauptverfasser:	Smart, Lesley (VerfasserIn), Moore, Elaine (VerfasserIn)
Format:	Buch
Sprache:	English
Veröffentlicht:	Boca Raton [u.a.] CRC Press 2012
Ausgabe:	4. ed.
Schlagworte:	Ferromagnetismus Festkörperchemie Gitterbaufehler Supraleiter Lehrbuch
Online-Zugang:	Inhaltsverzeichnis Klappentext
Beschreibung:	XXVII, 465 S. Ill., graph. Darst.
ISBN:	9781439847909 1439847908

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Datensatz im Suchindex

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adam_text	Contents Preface to the Fourth Edition ...................................................................................xv Preface to the Third Edition ..................................................................................xvii Preface to the Second Edition .................................................................................xix Preface to the First Edition .....................................................................................xxi Authors .................................................................................................................xxiii List of Units, Prefixes, and Constants ....................................................................xxv Chapter 1 An Introduction to Crystal Structures ..................................................1 1.1 1.2 1.3 1.4 1.5 Introduction ...............................................................................1 Close Packing ............................................................................2 Body-Centred and Primitive Structures ....................................6 Symmetry ..................................................................................8 Symmetry Notation ......................................................9 Axes of Symmetry .......................................................9 Planes of Symmetry ...................................................10 Inversion .....................................................................11 Inversion Axes and Improper Symmetry Axes and the Identity Element ............................................11 Operations ..................................................................13 Symmetry in Crystals .................................................13 .4.1 .4.2 .4.3 .4.4 .4.5 .4.6 .4.7 Lattices and Unit Cells ............................................................14 .5.1 Lattices .......................................................................14 .5.2 One- and Two-Dimensional Unit Cells ......................15 .5.3 Translational Symmetry Elements .............................16 .5.4 Three-Dimensional Lattices and Their Unit Cells .....18 1.5.5 Miller Indices .............................................................23 1.5.6 Interplanar Spacings ...................................................25 1.5.7 Packing Diagrams ......................................................25 1.6 Crystalline Solids ....................................................................27 1.6.1 Ionic Solids with Formula MX ...................................28 1.6.2 Solids with General Formula MX2 .............................33 1.6.3 Other Important Crystal Structures ...........................37 1.6.4 Ionic Radii ..................................................................40 1.6.5 Extended Covalent Arrays ..........................................47 1.6.6 Bonding in Crystals ....................................................49 1.6.7 Atomic Radii ..............................................................51 1.6.8 Molecular Structures ..................................................51 1.6.9 Silicates ......................................................................54 1.6.10 Quasicrystals ..............................................................57 VII viii Contents 1.7 Lattice Energy .........................................................................59 1.7.1 Born-Haber Cycle...................................................... 59 1.7.2 Calculating Lattice Energies ......................................61 1.7.3 Calculations Using Thermochemical Cycles and Lattice Energies ...................................................67 1.8 Conclusion ...............................................................................69 Questions ............................................................................................70 Chapter 2 Physical Methods for Characterising Solids ......................................75 2.1 Introduction .............................................................................75 2.2 Х -Ray Diffraction ....................................................................75 2.2.1 Generation of Х -Rays................................................. 75 2.2.2 Diffraction of Х -Rays................................................. 77 2.3 Powder Diffraction ..................................................................79 2.3.1 Powder Diffraction Patterns .......................................79 2.3.2 Absences Due to Lattice Centring .............................80 2.3.3 Systematic Absences Due to Screw Axes and Glide Planes .........................................................84 2.3.4 Uses of Powder X Ray Diffraction .............................86 2.4 Single Crystal Х -Ray Diffraction ............................................90 2.4.1 Importance of Intensities ............................................90 2.4.2 Solving Single Crystal Structures ..............................93 2.4.3 High-Energy Х -Ray Diffraction .................................95 2.5 Neutron Diffraction .................................................................96 2.5.1 Uses of Neutron Diffraction .....................................100 2.6 Electron Microscopy ............................................................. 101 2.6.1 Scanning Electron Microscopy ................................102 2.6.2 Transmission Electron Microscopy ..........................104 2.6.3 Energy Dispersive Х -Ray Analysis ..........................107 2.6.4 Scanning Transmission Electron Microscopy ..........108 2.6.5 Electron Energy Loss Spectroscopy ........................108 2.6.6 superSTEM ............................................................... Ill 2.7 Scanning Probe Microscopy ................................................. 111 2.7.1 Scanning Tunnelling Microscopy ............................ 112 2.8 Atomic Force Microscopy ..................................................... 114 2.9 Х -Ray Absorption Spectroscopy ........................................... 116 2.9.1 Extended Х -Ray Absorption Fine Structure ............ 116 2.9.2 Х -Ray Absorption Near-Edge Structure and Near-Edge Х -Ray Absorption Fine Structure ..........122 2.10 Solid-State Nuclear Magnetic Resonance Spectroscopy ......... 124 2.11 Thermal Analysis ..................................................................128 2.11.1 Differential Thermal Analysis .................................128 2.11.2 Thermogravimetric Analysis ....................................129 2.11.3 Differential Scanning Calorimetry ..........................130 Contents IX 2.12 Temperature-Programmed Reduction ...................................131 2.13 Other Techniques ...................................................................131 Questions ..........................................................................................132 Chapter 3 Synthesis of Solids ...........................................................................137 3.1 Introduction ...........................................................................137 3.2 H ig h-Te m perature Ceramic Methods ....................................138 3.2.1 Direct Heating of Solids ...........................................138 3.2.2 Reducing the Particle Size and Lowering the Temperature ........................................................ 141 3.3 Microwave Synthesis ............................................................. 145 3.3.1 High-Temperature Superconductor YBa2Cu,O7_v ....... 146 3.3.2 Batteries and Fuel Cells ............................................ 147 3.3.3 Graphene .................................................................. 147 3.4 Combustion Synthesis ........................................................... 147 3.5 High-Pressure Methods ......................................................... 149 3.5.1 Hydrothermal Methods ............................................ 149 3.5.2 High-Pressure Gases ................................................ 153 3.5.3 Hydrostatic Pressures ............................................... 153 3.5.4 Using Ultrasound ...................................................... 155 3.5.5 Detonation ................................................................ 155 3.6 Chemical Vapour Deposition ................................................ 155 3.6.1 Preparation of Semiconductors ................................156 3.6.2 Diamond Films .........................................................157 3.6.3 Optical Fibres ...........................................................157 3.6.4 Lithium Niobáte .......................................................158 3.7 Preparing Single Crystals ......................................................159 3.7.1 Epitaxy Methods ......................................................159 3.7.2 Chemical Vapour Transport .....................................160 3.7.3 Melt Methods ........................................................... 161 3.7.4 Solution Methods ......................................................163 3.8 Intercalation ...........................................................................164 3.8.1 Graphite Intercalation Compounds ..........................164 3.9 Synthesis of Nanomaterials ...................................................166 3.9.1 Top-Down Methods ..................................................166 3.9.2 Bottom-Up Methods: Manipulating Atoms and Molecules ........................................................... 170 3.9.3 Synthesis Using Templates ....................................... 173 3.10 Choosing a Method ................................................................ 177 Questions .......................................................................................... 177 Chapter 4 Solids: Their Bonding and Electronic Properties ............................ 179 4.1 Introduction ........................................................................... 179 4.2 Bonding in Solids: Free-Electron Theory ............................. 179 4.2.1 Electronic Conductivity ............................................184 к Contents 4.3 Bonding in Solids: Molecular Orbital Theory ......................185 4.3.1 Simple Metals ...........................................................188 4.4 Semiconductors: Si and Ge .................................................... 189 4.4.1 Photoconductivity .....................................................191 4.4.2 Doped Semiconductors ............................................192 4.4.3 p -п Junction and Field Effect Transistors ................193 4.5 Bands in Compounds: Gallium Arsenide ..............................195 4.6 Bands in d-Block Compounds: Transition Metal Monoxides ............................................................................196 4.7 Classical Modelling ...............................................................197 4.7.1 Intrinsic Defects in Alkali Halide Crystals ..............197 4.7.2 Zeolites .....................................................................198 4.7.3 Ionic Conductors for Fuel Cells ................................199 Questions ..........................................................................................199 Chapter 5 Defects and Nonstoichiometry .........................................................201 5.1 Point Defects: An Introduction ..............................................201 5.2 Defects and Their Concentration ...........................................201 5.2.1 Intrinsic Defects .......................................................201 5.2.2 Concentration of Defects ..........................................204 5.2.3 Extrinsic Defects ......................................................208 5.3 Ionic Conductivity in Solids ..................................................208 5.4 Solid Electrolytes ...................................................................214 5.4.1 Fast-Ion Conductors: Silver Ion Conductors .............214 5.4.2 Fast-Ion Conductors: Oxygen Ion Conductors .........218 5.4.3 Fast-Ion Conductors: Sodium Ion Conductors .........220 5.5 Applications of Solid Electrolytes .........................................223 5.5.1 Batteries ....................................................................224 5.5.2 Fuel Cells ..................................................................229 5.5.3 Oxygen Sensor ..........................................................234 5.5.4 Oxygen Separation Membranes ...............................236 5.5.5 Electrochromic Devices ...........................................237 5.6 Colour Centres .......................................................................239 5.7 Nonstoichiometric Compounds .............................................240 5.7.1 Introduction ..............................................................240 5.7.2 Nonstoichiometry in Wustite (FeO) and МО -Type Oxides ......................................................242 5.7.3 Uranium Dioxide ......................................................246 5.7.4 Titanium Monoxide Structure ..................................248 5.8 Extended Defects ...................................................................250 5.8.1 Crystallographic Shear Planes .................................252 5.8.2 Planar Intergrowths ..................................................256 5.9 Three-Dimensional Defects ..................................................257 5.9.1 Block Structures .......................................................257 Contents Xl 5.9.2 Pentagonal Columns .................................................259 5.9.3 Infinitely Adaptive Structures ..................................260 5.10 Electronic Properties of Nonstoichiometric Oxides ..............260 5.11 Conclusions ............................................................................266 Questions ..........................................................................................266 Chapter 6 Microporous and Mesoporous Solids ...............................................271 6.1 Zeolites ..................................................................................271 6.1.1 Composition and Structure of Zeolites ....................271 6.1.2 Frameworks ..............................................................272 6.1.3 Synthesis of Zeolites ................................................275 6.1.4 Zeolite Nomenclature ...............................................277 6.1.5 Si/Al Ratios in Zeolites ............................................277 6.1.6 Exchangeable Cations ..............................................277 6.1.7 Channels and Cavities ..............................................278 6.1.8 Structure Determination ...........................................285 6.1.9 Zeolites as Dehydrating Agents ...............................286 6.1.1 0 Zeolites as Ion Exchangers .......................................286 6.1.1 1 Zeolites as Adsorbents .............................................287 6.1.12 Zeolites as Catalysts .................................................289 6.2 Other Microporous Framework Structures ...........................296 6.3 Mesoporous Structures ..........................................................297 6.3.1 Mesoporous Aluminosilicate Structures ..................297 6.3.2 Modified Mesoporous Aluminosilicates ..................299 6.3.3 Periodic Mesoporous Organosilicas .........................300 6.3.4 Metal Organic Frameworks ......................................301 6.3.5 Metal Oxide Frameworks .........................................310 6.4 New Materials .......................................................................310 6.5 Clay Minerals ........................................................................ ЗІ І 6.6 Summary ...............................................................................313 6.7 Postscript ...............................................................................313 Questions ..........................................................................................314 Chapter 7 Optical Properties of Solids .............................................................315 7.1 Introduction ...........................................................................315 7.2 Interaction of Light with Atoms ............................................316 7.2.1 Ruby Laser ...............................................................318 7.2.2 Phosphors in Fluorescent Lights ..............................320 7.3 Absorption and Emission of Radiation in Continuous Solids ..........................................................322 7.3.1 Light-Emitting Diodes ..............................................325 7.3.2 Gallium Arsenide Laser ...........................................326 7.3.3 Quantum Wells: Blue Lasers ....................................327 xii Contents 7.4 Refraction ..............................................................................328 7.4.1 Calcite .......................................................................330 7.4.2 Optical Fibres ...........................................................331 7.5 Photonic Crystals ...................................................................333 7.6 Metamaterials: Cloaks of Invisibility ....................................335 Questions ..........................................................................................338 Chapter 8 Magnetic and Electrical Properties ..................................................341 8.1 Introduction ...........................................................................341 8.2 Magnetic Susceptibility .........................................................341 8.3 Paramagnetism in Metal Complexes .....................................344 8.4 Ferromagnetic Metals ............................................................346 8.4 Л Ferromagnetic Domains ...........................................348 8.4.2 Permanent Magnets ..................................................351 8.5 Ferromagnetic Compounds: Chromium Dioxide ..................351 8.6 Antiferromagnetism: Transition Metal Monoxides ...............352 8.7 Ferrimagnetismi Ferrites....................................................... 353 8.7.1 Magnetic Strips on Swipe Cards ..............................355 8.8 Spiral Magnetism ..................................................................355 8.9 Giant, Tunnelling and Colossal Magnetoresistance..............356 8.9.1 Giant Magnetoresistance..........................................356 8.9.2 Tunnelling Magnetoresistance.................................358 8.9.3 Hard-Disk Read Heads .............................................359 8.9.4 Colossal Magnetoresistance: Manganites................360 8.10 Electrical Polarisation ...........................................................361 8.11 Piezoelectric Crystals: α -Quartz........................................... 362 8.12 Ferroelectric Effect ................................................................363 8.12.1 Multilayer Ceramic Capacitors ................................366 8.13 Multiferroics ..........................................................................367 8.13.1 Type I Multiferroics: Bismuth Ferrite ......................368 8.13.2 Type II Multiferroics: Terbium Manganite ..............368 Questions ..........................................................................................370 Chapter 9 Superconductivity .............................................................................373 9.1 Introduction ...........................................................................373 9.2 Conventional Superconductors ..............................................373 9.2.1 Discovery of Superconductors .................................373 9.2.2 Magnetic Properties of Superconductors .................374 9.2.3 BCS Theory of Superconductivity ...........................377 9.3 High-Temperature Superconductors ......................................378 9.3.1 Cuprate Superconductors .........................................379 9.3.2 Iron Superconductors ...............................................384 9.3.3 Theory of High Tc Superconductors ........................385 Contents xiii 9.4 Uses of High-Temperature Superconductors .........................386 Questions ..........................................................................................387 Chapter 10 Nanostructures and Solids with Low-Dimensional Properties ........389 10.1 Nanoscience ...........................................................................389 10.2 Consequences of the Nanoscale ............................................390 10.2.1 Nanoparticle Morphology ........................................390 10.2.2 Electronic Structure .................................................390 10.2.3 Optical Properties .....................................................394 10.2.4 Magnetic Properties .................................................396 10.2.5 Mechanical Properties ..............................................398 10.2.6 Melting .....................................................................398 10.3 Low-Dimensional and Nanostructural Carbon .....................399 10.3.1 Carbon Black ............................................................399 10.3.2 Graphite ....................................................................399 10.3.3 Intercalation Compounds of Graphite ......................400 10.3.4 Graphene ..................................................................402 10.3.5 Buckminster Fullerene .............................................403 10.3.6 Carbon Nanotubes ....................................................404 10.4 Carbon-Based Conducting Polymers ....................................405 10.4.1 Discovery of Polyacetylene ......................................405 10.4.2 Bonding in Polyacetylene and Related Polymers ......407 10.4.3 Organic LEDs and Photovoltaic Cells .....................408 10.4.4 Polymers and Ionic Conduction: Rechargeable Lithium Batteries ......................................................409 10.5 Noncarbon Nanoparticles ......................................................412 10.5.1 Fumed Silica .............................................................412 10.5.2 Quantum Dots ..........................................................413 10.5.3 Explosives .................................................................414 10.5.4 Magnetic Nanoparticles ...........................................415 10.5.5 Medical and Cosmetic Use .......................................415 10.6 Noncarbon Nanofilms and NanoJayers ..................................416 10.7 Noncarbon Nanotubes, Nanorods and Nanowires ................417 Questions ..........................................................................................418 Further Reading ...................................................................................................421 Answers to Questions ...........................................................................................425 Index ......................................................................................................................453 FOURTH EDITION SOLID STATE CHEMISTRY AN INTRODUCTION Building a foundation with a thorough description of crystalline structures, Solid State Chemistry: An Introduction, Fourth Edition presents a wide range of the synthetic and physical techniques used to prepare and character¬ ize solids. Going beyond basic science, the book explains and analyzes modern techniques and areas of research. The book covers • A range of synthetic and physical techniques used to prepare and characterize solids • Bonding, superconductivity, and electrochemical, magnetic, optical, and conductive properties • STEM, ionic conductivity, nanotubes and related structures such as graphene, metal organic frameworks, and FeAs superconductors • Biological systems in synthesis, solid state modeling, and metamaterials This largely nonmathematical introduction to solid state chemistry includes basic crystallography and structure determination, as well as practical examples of applications and modern developments to offer students the opportunity to apply their knowledge in real-life situations and serve them well throughout their degree course. New in the Fourth Edition • Coverage of multiferroics, graphene, and iron-based high temperature superconductors, the techniques available with synchrotron radiation, and metal organic frameworks (MOFs) • More space devoted to electron microscopy and preparative methods • New discussion of conducting polymers in the expanded section on carbon nanoscience
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genre_facet	Lehrbuch
id	DE-604.BV040026887
illustrated	Illustrated
indexdate	2024-07-10T00:16:25Z
institution	BVB
isbn	9781439847909 1439847908
language	English
oai_aleph_id	oai:aleph.bib-bvb.de:BVB01-024883864
oclc_num	796191945
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physical	XXVII, 465 S. Ill., graph. Darst.
publishDate	2012
publishDateSearch	2012
publishDateSort	2012
publisher	CRC Press
record_format	marc
spelling	Smart, Lesley Verfasser aut Solid state chemistry an introduction Lesley E. Smart ; Elaine A. Moore 4. ed. Boca Raton [u.a.] CRC Press 2012 XXVII, 465 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Ferromagnetismus (DE-588)4154131-5 gnd rswk-swf Festkörperchemie (DE-588)4129288-1 gnd rswk-swf Gitterbaufehler (DE-588)4125030-8 gnd rswk-swf Supraleiter (DE-588)4184140-2 gnd rswk-swf (DE-588)4123623-3 Lehrbuch gnd-content Festkörperchemie (DE-588)4129288-1 s Gitterbaufehler (DE-588)4125030-8 s Supraleiter (DE-588)4184140-2 s Ferromagnetismus (DE-588)4154131-5 s 1\p DE-604 Moore, Elaine Verfasser (DE-588)1024503143 aut Digitalisierung UB Regensburg - ADAM Catalogue Enrichment application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024883864&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis Digitalisierung UB Regensburg - ADAM Catalogue Enrichment application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024883864&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA Klappentext 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk
spellingShingle	Smart, Lesley Moore, Elaine Solid state chemistry an introduction Ferromagnetismus (DE-588)4154131-5 gnd Festkörperchemie (DE-588)4129288-1 gnd Gitterbaufehler (DE-588)4125030-8 gnd Supraleiter (DE-588)4184140-2 gnd
subject_GND	(DE-588)4154131-5 (DE-588)4129288-1 (DE-588)4125030-8 (DE-588)4184140-2 (DE-588)4123623-3
title	Solid state chemistry an introduction
title_auth	Solid state chemistry an introduction
title_exact_search	Solid state chemistry an introduction
title_full	Solid state chemistry an introduction Lesley E. Smart ; Elaine A. Moore
title_fullStr	Solid state chemistry an introduction Lesley E. Smart ; Elaine A. Moore
title_full_unstemmed	Solid state chemistry an introduction Lesley E. Smart ; Elaine A. Moore
title_short	Solid state chemistry
title_sort	solid state chemistry an introduction
title_sub	an introduction
topic	Ferromagnetismus (DE-588)4154131-5 gnd Festkörperchemie (DE-588)4129288-1 gnd Gitterbaufehler (DE-588)4125030-8 gnd Supraleiter (DE-588)4184140-2 gnd
topic_facet	Ferromagnetismus Festkörperchemie Gitterbaufehler Supraleiter Lehrbuch
url	http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024883864&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024883864&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA
work_keys_str_mv	AT smartlesley solidstatechemistryanintroduction AT mooreelaine solidstatechemistryanintroduction

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