Laser-induced breakdown spectroscopy: fundamentals and applications
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin [u.a.]
Springer
2012
|
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | Literaturangaben |
| Beschreibung: | XII, 543 S. Ill., graph. Darst. 25 cm |
| ISBN: | 9783642206672 3642206670 9783642443732 |
Internformat
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| 100 | 1 | |a Noll, Reinhard |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Laser-induced breakdown spectroscopy |b fundamentals and applications |c Reinhard Noll |
| 264 | 1 | |a Berlin [u.a.] |b Springer |c 2012 | |
| 300 | |a XII, 543 S. |b Ill., graph. Darst. |c 25 cm | ||
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Datensatz im Suchindex
| _version_ | 1805146042983776256 |
|---|---|
| adam_text |
IMAGE 1
CONTENTS
1 INTRODUCTION 1
REFERENCES 5
2 LASER-INDUCED BREAKDOWN SPECTROSCOPY 7
2.1 PRINCIPLE AND MEASURING PARAMETERS 7
2.2 SETUP FOR LASER-INDUCED BREAKDOWN SPECTROSCOPY 12
2.3 MEASURING PROCEDURE 14
2.4 APPLICATIONS AND METHODICAL EXTENSIONS 14
REFERENCES 15
3 PROCESS PARAMETERS 17
3.1 LASER PULSE ENERGY AND REPETITION RATE 17
3.2 TEMPORAL CHARACTERISTICS OF THE LASER PULSE 22
3.3 LASER WAVELENGTH 25
3.4 BEAM QUALITY AND FOCUSING 27
3.5 AMBIENT GAS ATMOSPHERE 29
3.6 SPATIAL RESOLUTION AND SPATIAL AVERAGING 33
3.7 DIRECTION OF INCIDENCE OF THE LASER BEAM AND DIRECTION OF
OBSERVATION OF THE PLASMA EMISSION 38
3.8 WARMING-UP PULSES, PREPULSES, AND MEASURING PULSES 39 3.9 STATE OF
THE MEASURING OBJECT 41
REFERENCES 43
4 INSTRUMENTAL COMPONENTS 47
4. 1 LASER 47
4.2 SPECTROMETER 51
4.3 BEAM GUIDING OPTICS 56
4.4 DETECTORS 61
4.5 SIGNAL ELECTRONICS 65
4.6 SAMPLE STAND AND MEASURING CHAMBER 66
REFERENCES 70
BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/1010702815
DIGITALISIERT DURCH
IMAGE 2
X CONTENTS
5 EVAPORATION AND PLASMA GENERATION 75
5. 1 EVAPORATION 75
5.2 PLASMA GENERATION 78
5.3 ABSORPTION OF LASER RADIATION IN THE PLASMA 79
REFERENCES 81
6 MULTIPLE PULSES FOR LIBS 83
6.1 DOUBLE PULSES 84
6.2 TRIPLE AND MULTIPLE PULSES 92
6.3 TAILORED PULSE TRAINS 93
REFERENCES 94
7 MATERIAL ABLATION 97
7.1 CRATER FORMATION 97
7.2 ABLATED MASS 99
7.3 MATERIAL ABLATION IN DIFFERENT AMBIENT GASES BY COLLINEAR MULTIPLE
LASER PULSES 102
7.4 MATERIAL ABLATION BY COLLINEAR DOUBLE LASER PULSES AT REDUCED
AMBIENT GAS PRESSURES 110
REFERENCES 117
8 PLASMA DYNAMICS AND PLASMA PARAMETERS 119
8.1 EXPANSION AND DECAY OF THE PLASMA 119
8.2 SPATIALLY INTEGRATED ELECTRON DENSITY AND TEMPERATURE 132 8.3
SPATIALLY RESOLVED ELECTRON DENSITY 152
8.4 CHARACTERISTIC TIME SCALES AND LOCAL TEMPERATURE EQUILIBRIUM
CONDITIONS OF THE LASER-INDUCED PLASMA 160 REFERENCES 166
9 PLASMA EMISSION 1 67
9.1 BREMSSTRAHLUNG AND RECOMBINATION RADIATION 167
9.2 LINE EMISSION 169
9.3 ABSORPTION AND OPTICAL THICKNESS 171
9.4 LINE BROADENING 173
REFERENCES 182
10 MODELING OF PLASMA EMISSION 185
10.1 HEURISTIC MODEL 189
10.2 CALCULATION OF EMISSION SPECTRA 193
10.3 SIMULATION OF SPECTRA 198
10.3.1 FE SPECTRUM 198
10.3.2 AL RESONANCE LINE WITH SELF-REVERSAL 201
10.4 ENTHALPY OF PLASMA 203
REFERENCES 204
11 QUANTITATIVE ANALYSIS 207
11.1 MEASURING METHOD 207
11.2 CALIBRATION 212
IMAGE 3
CONTENTS XI
11.3 MEASUREMENT AND DETERMINATION OF ANALYTES 216
11.4 RECALIBRATION 216
11.5 INTERELEMENT CORRECTION 218
REFERENCES 220
12 COMBINATION OF LIBS AND LIF 221
REFERENCES 228
13 BULK ANALYSIS OF METALLIC ALLOYS 229
13.1 STEEL 229
13.1.1 SOLID STEEL SAMPLES 229
13.1.2 SOLID STEEL SAMPLES WITH SCALE LAYER 235
13.1.3 LIQUID STEEL 245
13.2 HIGH-ALLOY STEEL 252
13.3 ALUMINUM 264
REFERENCES 271
14 BULK ANALYSIS OF NONCONDUCTING MATERIALS 275
14.1 POLYMERS 275
14.1.1 IDENTIFICATION OF PLASTIC MATERIALS 275
14.1.2 DETECTION OF HEAVY METALS AND FLAME RETARDANTS IN TECHNICAL
POLYMERS 285
14.2 SLAG 303
14.2.1 CONVERTER SLAGS 304
14.2.2 VACUUM SLAG 314
14.3 SOIL 318
14.4 CEMENT 326
14.5 DROPLETS 337
14.6 GASES 349
14.7 PARTICULATES 355
14.8 AEROSOLES 361
14.8.1 AEROSOLES SAMPLED ON SUBSTRATES 361
14.8.2 AEROSOLES IN AN AIR STREAM 372
REFERENCES 380
15 SPATIALLY RESOLVED ANALYSIS 387
15. 1 HIGH-SPEED LIBS FOR MICROANALYSIS 387
15.2 ELEMENT MAPPINGS 396
REFERENCES 398
16 DEPTH PROFILING 401
16.1 MEASUREMENT OF THE THICKNESS OF COATINGS 401
16.2 CHARACTERIZATION OF DEPTH PROFILES 416
REFERENCES 426
17 LIBS INSTRUMENTS 429
17.1 LABORATORY SYSTEMS 429
17.2 INSPECTION SYSTEMS FOR INLINE PROCESS CONTROL 437
IMAGE 4
XII CONTENTS
17.3 MOBILE SYSTEMS 447
17.4 REMOTE SYSTEMS 454
REFERENCES 463
18 INDUSTRIAL APPLICATIONS 467
18.1 IDENTIFICATION TESTING OF HIGH-ALLOY PIPE FITTINGS 467 18.2
ANALYSIS OF SLAGS 469
18.3 CHARACTERIZATION OF INCLUSIONS AND SEGREGATIONS 472
18.4. RECYCLING OF ALUMINUM SCRAP 484
REFERENCES 488
A ANNEX 491
A. 1 DISPLACEMENT OF AMBIENT ATMOSPHERE 491
A.2 ABBREVIATIONS 494
A.3 LIST OF SYMBOLS 498
A.4 STARK DATA 511
A.5 WAVELENGTHS AND ELEMENTS 511
A.6 SPECTRAL LINE SELECTION FOR BOLTZMANN PLOTS 511
REFERENCES 533
INDEX 535 |
| any_adam_object | 1 |
| author | Noll, Reinhard |
| author_facet | Noll, Reinhard |
| author_role | aut |
| author_sort | Noll, Reinhard |
| author_variant | r n rn |
| building | Verbundindex |
| bvnumber | BV039868733 |
| classification_rvk | UH 5710 |
| ctrlnum | (OCoLC)725042526 (DE-599)DNB1010702815 |
| dewey-full | 530.44 543.5 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 530 - Physics 543 - Analytical chemistry |
| dewey-raw | 530.44 543.5 |
| dewey-search | 530.44 543.5 |
| dewey-sort | 3530.44 |
| dewey-tens | 530 - Physics 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik |
| format | Book |
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| institution | BVB |
| isbn | 9783642206672 3642206670 9783642443732 |
| language | English |
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| physical | XII, 543 S. Ill., graph. Darst. 25 cm |
| publishDate | 2012 |
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| publishDateSort | 2012 |
| publisher | Springer |
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| spelling | Noll, Reinhard Verfasser aut Laser-induced breakdown spectroscopy fundamentals and applications Reinhard Noll Berlin [u.a.] Springer 2012 XII, 543 S. Ill., graph. Darst. 25 cm txt rdacontent n rdamedia nc rdacarrier Literaturangaben Laserinduzierte Breakdown-Spektroskopie (DE-588)4745837-9 gnd rswk-swf Laserinduzierte Breakdown-Spektroskopie (DE-588)4745837-9 s DE-604 Erscheint auch als Online-Ausgabe Laser-Induced Breakdown Spectroscopy X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=3705628&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024728109&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Noll, Reinhard Laser-induced breakdown spectroscopy fundamentals and applications Laserinduzierte Breakdown-Spektroskopie (DE-588)4745837-9 gnd |
| subject_GND | (DE-588)4745837-9 |
| title | Laser-induced breakdown spectroscopy fundamentals and applications |
| title_auth | Laser-induced breakdown spectroscopy fundamentals and applications |
| title_exact_search | Laser-induced breakdown spectroscopy fundamentals and applications |
| title_full | Laser-induced breakdown spectroscopy fundamentals and applications Reinhard Noll |
| title_fullStr | Laser-induced breakdown spectroscopy fundamentals and applications Reinhard Noll |
| title_full_unstemmed | Laser-induced breakdown spectroscopy fundamentals and applications Reinhard Noll |
| title_short | Laser-induced breakdown spectroscopy |
| title_sort | laser induced breakdown spectroscopy fundamentals and applications |
| title_sub | fundamentals and applications |
| topic | Laserinduzierte Breakdown-Spektroskopie (DE-588)4745837-9 gnd |
| topic_facet | Laserinduzierte Breakdown-Spektroskopie |
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