Synthesis of inorganic materials:
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH
2012
|
| Ausgabe: | 3., compl. rev. and enl. ed. |
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | XXII, 370 S. Ill., graph. Darst. |
| ISBN: | 9783527327140 3527327142 |
Internformat
MARC
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| 100 | 1 | |a Schubert, Ulrich |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Synthesis of inorganic materials |c Ulrich Schubert and Nicola Hüsing |
| 250 | |a 3., compl. rev. and enl. ed. | ||
| 264 | 1 | |a Weinheim |b Wiley-VCH |c 2012 | |
| 300 | |a XXII, 370 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
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Datensatz im Suchindex
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IMAGE 1
CONTENTS
PREFACE X I
ACKNOWLEDGEMENT X V LIST O F ABBREVIATIONS X I X
1 INTRODUCTION 1
2 SOLID-STATE REACTIONS 5
2.1 REACTIONS BETWEEN SOLID COMPOUNDS 5
2.1.1 CERAMIC METHOD 5
2.1.1.1 A N EXAMPLE 6
2.1.1.2 GENERAL ASPECTS O F SOLID-STATE REACTIONS 8 2.1.2
MECHANOCHEMICAL SYNTHESIS 16 2.1.3 CARBOTHERMAL REDUCTION 17
2.1.4 COMBUSTION SYNTHESIS 22
2.1.4.1 CLASSIFICATION O F COMBUSTION SYNTHESIS REACTIONS 26 2.1.5
SINTERING 28
2.1.5.1 STAGES'OF SINTERING 30
2.1.5.2 FACTORS AFFECTING SINTERING 31 2.1.5.3 CERAMICS PROCESSING 31
2.2 SOLID-GAS REACTIONS 36
2.3 INTERCALATION REACTIONS 39
2.3.1 , GENERAL ASPECTS 39
2.3.1.1 MECHANISTIC ASPECTS O F INTERCALATION REACTIONS 43 2.3.2
PREPARATIVE METHODS 44
2.3.2.1 TYPES O F INTERCALATION REACTIONS 44 2.3.2.2 INTERCALATION O F
POLYMERS IN LAYERED SYSTEMS 48 2.3.3 * PILLARING O F LAYERED COMPOUNDS
50
"U-
3 FORMATION O F SOLIDS FROM T H E G A S P H A S E 5 5
3.1 CHEMICAL VAPOR TRANSPORT 55
3.1.1 HALOGEN LAMPS 56
SYNTHESIS O F INORGANIC MATERIALS, T H I R D E D I T I O N . U L R I C H
S C H U B E R T A N D N I C O L A H L I S I N G . 2 0 1 2 W I L E Y -
V C H V E R L A G G M B H & C O . K G A A , W E I N H E I M .
P U B L I S H E D 2 0 1 2 B Y W I L E Y - V C H V E R L A G G M B H & C
O . K G A A
HTTP://D-NB.INFO/1011200317
IMAGE 2
C O N T E N T S
3.1.2 TRANSPORT REACTIONS 59
3.2 CHEMICAL VAPOR DEPOSITION 62
3.2.1 GENERAL ASPECTS 63
3.2.1.1 EQUIPMENT 67
3.2.1.2 GROWTH RATES 69
3.2.1.3 SELECTIVE DEPOSITION 71 3.2.1.4 CVD AND CVD-RELATED TECHNIQUES
72 3.2.1.5 NON-CVD PROCESSES FOR THE GAS-PHASE DEPOSITION O F THIN FILMS
74 3.2.2 METAL CVD 77
3.2.2.1 A L U M I N U M 78
3.2.2.2 TUNGSTEN 81
3.2.2.3 COPPER 82
3.2.3 DIAMOND CVD 84
3.2.4 CVD O F METAL OXIDES 87
3.2.4.1 S I 0 2 A N D SILICATE GLASSES 87
3.2.4.2 YTTRIUM BARIUM COPPER OXIDE (YBCO) 89 3.2.5 CVD O F METAL
NITRIDES 90
3.2.6 CVD O F COMPOUND SEMICONDUCTORS 92
3.2.7 CHEMICAL VAPOR INFILTRATION 96
3.3 AEROSOL PROCESSES 97
3.3.1 AEROSOL PROCESS ROUTES 100
3.3.2 REACTORS 103
3.3.3 PRODUCTS 105
3.3.4 FILM GENERATION 107
4 FORMATION O F SOLIDS FROM SOLUTIONS A N D MELTS 111
4.1 GLASS 111
4.1.1 THE STRUCTURAL THEORY O F GLASS FORMATION 113
4.1.2 CRYSTALLIZATION VERSUS GLASS FORMATION 117 4.1.3 GLASS MELTING 122
4.1.3.1 RAW MATERIALS O F GLASS PRODUCTION 123 4.1.3.2 BATCH MELTING 123
4.1.3.3 FINING O F MELTS 125
4.1.3.4 HOMOGENIZATION O F MELT 126 4.1.4 METALLIC GLASSES 126
4.1.4.1 BULK METALLIC GLASSES 129 4.2 PRECIPITATION 130
4.2.1 MONODISPERSE CRYSTALS 132
4.2.2 SHAPE CONTROL O F CRYSTALS 134
4.3 BIOMATERIALS 135
4.3.1 BIOGENIC MATERIALS A N D BIOMINERALIZATION 136 4.3.1.1 AMORPHOUS:
DIATOMS 138 4.3.1.2 ORDERED MESOSCOPIC CRYSTALLINE AGGREGATES: BONE 140
4.3.1.3 CRYSTALLINE MATERIALS 141 4.3.1.4 MINERALIZATION PROCESSES 142
IMAGE 3
C O N T E N T S V I I
4.3.2 SYNTHETIC BIOMATERIALS 146
4.3.2.1 BIOACTIVE CERAMICS AND GLASSES 148 4.3.2.2 BONE SUBSTITUTES 149
4.3.3 BIOMIMETIC MATERIALS CHEMISTRY 149 4.4 SOLVOTHERMAL PROCESSES 155
4.4.1 HYDROTHERMAL SYNTHESIS O F SINGLE CRYSTALS 155 4.4.1.1 GENERAL
ASPECTS O F SOLVOTHERMAL PROCESSES 156 4.4.1.2 NON-AQUEOUS SOLVENTS 162
4.4.2 HYDROTHERMAL SYNTHESIS 163
4.4.2.1 SYNTHESIS O F ZEOLITES 164
4.4.3 HYDROTHERMAL LEACHING 165
4.5 SOL-GEL PROCESSES 165
4.5.1 THE PHYSICS O F SOLS 170
4.5.2 SOL-GEL PROCESSING O F SILICATE MATERIALS 173 4.5.2.1 HYDROLYSIS A
N D CONDENSATION REACTIONS 173 4.5.2.2 THE SOL-GEL TRANSITION (GELATION)
179 4.5.2.3 AGING 183
4.5.2.4 DRYING 184
4.5.3 SOL-GEL CHEMISTRY O F METAL OXIDES 185
4.5.3.1 INORGANIC PRECURSORS (METAL SALTS) 185 4.5.3.2 ALKOXIDE
PRECURSORS 188 4.5.4 INORGANIC-ORGANIC HYBRID MATERIALS 191 4.5.4.1
EMBEDDING O F ORGANIC MOLECULES 192 4.5.4.2 INORGANIC-ORGANIC HYBRID
POLYMERS 195 4.5.5 NON-HYDROLYTIC SOL-GEL PROCESSES 202
4.5.6 AEROGELS 203
4.5.6.1 DRYING METHODS 204
4.5.6.2 PROPERTIES A N D APPLICATIONS 207
5 PREPARATION A N D MODIFICATION O F INORGANIC POLYMERS 211
5.1 GENERAL ASPECTS 211
5.1.1 POLYMERIC MATERIALS 213
5.1.2 CROSSLINKING 214
5.1.3 PRECERAMIC POLYMERS 216
5.2 POLYSILOXANES (SILICONES) 219
5.2.1 PROPERTIES AND APPLICATIONS O F SILICONES 219 5.2.1.1 SILICONE
OILS 219
5.2.1.2 SILICONE ELASTOMERS 220 5.2.1.3 SILICONE RESINS 222
5.2.2 STRUCTURE O F SILICONES 223
5.2.3 PREPARATION O F SILICONES 224
5.2.3.1 PRECURSOR SYNTHESES 224
5.2.3.2 HYDROLYSIS, METHANOLYSIS, AND POLYCONDENSATION REACTIONS 226
5.2.3.3 EQUILIBRATION A N D RING-OPENING POLYMERIZATION OF
CYCLOSILOXANES 228
IMAGE 4
V I I I C O N T E N T S
5.2.3.4 CURING ("VULCANIZING") 230
5.2.3.5 POLYSILOXANE COPOLYMERS 232 5.3 POLYPHOSPHAZENES 233
5.3.1 PROPERTIES AND APPLICATIONS O F POLYPHOSPHAZENES 233 5.3.2
PREPARATION A N D MODIFICATION 236
5.4 POLYSILANES 239
5.4.1 PROPERTIES AND APPLICATIONS O F POLYSILANES 239 5.4.1.1 EFFECTS
ORIGINATING FROM THE SUBSTITUENTS 239 5.4.1.2 EFFECTS ORIGINATING FROM
THE BACKBONE 239 5.4.2 PREPARATION AND MODIFICATION O F POLYSILANES 242
5.5 POLYCARBOSILANES 247
5.5.1 SIC FIBERS FROM POLYCARBOSILANES (YAJIMA PROCESS) 247 5.5.1.1
PREPARATION O F SIC FIBERS 248
5.5.2 CHEMICAL ISSUES O F POLYMER PREPARATION, CURING, A N D PYROLYSIS
249 5.5.2.1 POLYMER PREPARATION 249
5.5.2.2 CROSSLINKING 252
5.5.2.3 PYROLYSIS 253
5.6 POLYSILAZANES AND POLYBOROSILAZANES 254
5.6.1 PREPARATION O F POLYSILAZANES A N D POLYBOROSILAZANES 255 5.6.2
CURING A N D PYROLYSIS REACTIONS 258
5.7 OTHER INORGANIC POLYMERS 258
5.7.1 PRECERAMIC POLYMERS FOR BN 259
5.7.2 OTHER PHOSPHORUS-CONTAINING POLYMERS 260 5.7.3 POLYMERS WITH S-N
BACKBONES 262
5.8 METAL-CONTAINING POLYMERS 262
5.8.1 ONE-DIMENSIONAL COORDINATION POLYMERS 263 5.8.2 METAL-ORGANIC
FRAMEWORKS 265
6 T E M P L A T E D MATERIALS 2 7 5
6.1 INTRODUCTION TO POROSITY AND HIGH SURFACE AREA MATERIALS 276
6.2 METALLIC FOAMS AND POROUS METALS 280
6.2.1 CASTING TECHNIQUES 281
6.2.1.1 FOAMING 281
6.2.1.2 LOST-FOAM CASTING 282
6.2.1.3 INFILTRATION 282
6.2.2 GAS-EUTECTIC TRANSFORMATION 283
6.2.3 POWDER METALLURGY 284
6.2.3.1 POWDER SINTERING 284
6.2.3.2 COMPACTING WITH FOAMING AGENTS 285 6.2.4 METAL DEPOSITION 286
6.3 SOFT TEMPLATES/ENDOTEMPLATING 286
6.3.1 TEMPLATING WITH MOLECULES 287
6.3.2 TEMPLATING WITH SUPRAMOLECULAR ARRANGEMENTS O F MOLECULES 294 6.4
H A R D TEMPLATES/EXOTEMPLATING 300
6.4.1 NANOCASTING 301
IMAGE 5
C O N T E N T S I X
6.4.1.1 ORDERED SILICA AS TEMPLATE/MOLD 301
6.4.1.2 COLLOIDAL CRYSTALS AS TEMPLATES/MOLDS 302 6.5 TEMPLATING TOWARDS
MULTISCALE POROSITY 304
6.5.1 DUAL OR MULTIPLE TEMPLATING 305
6.5.2 PHASE-SEPARATION STRATEGIES 306 6.6 INCORPORATION O F FUNCTIONAL
GROUPS INTO POROUS MATERIALS 308
7 N A N O S T R U C T U R E D MATERIALS 313
7.1 THE ORIGIN O F NANOEFFECTS 314
7.2 PROPERTIES O F NANOMATERIALS 316
7.2.1 PROPERTIES ORIGINATING FROM SURFACE EFFECTS 316 7.2.1.1 CHEMICAL
PROPERTIES 316 7.2.1.2 PHOTOCATALYSIS 317
7.2.1.3 MELTING POINTS 318
7.2.1.4 PHASE TRANSITIONS 318
7.2.1.5 DIFFUSION A N D SINTERABILITY 319 7.2.2 PROPERTIES ORIGINATING
FROM Q U A N T U M CONFINEMENT 319 7.2.2.1 OPTICAL PROPERTIES 319
7.2.2.2 ELECTRICAL PROPERTIES 322 7.2.2.3 MAGNETIC PROPERTIES 322 7.3
SYNTHESES O F NANOPARTICLES 324
7.3.1 MECHANICAL ATTRITION 326
7.3.2 FORMATION O F NANOPARTICLES FROM VAPORS 326 7.3.2.1 GAS
CONDENSATION METHOD 327 7.3.2.2 SOLVATED METAL ATOM DISPERSION METHOD
328 7.3.3 FORMATION O F NANOPARTICLES FROM SOLUTION 329
7.3.3.1 TWO-PHASE METHOD 330 7.3.3.2 HOT-INJECTION METHOD 332 7.3.3.3
SYNTHESES IN CONFINED SPACES 333
7.3.4 SURFACE MODIFICATION O F NANOPARTICLES 335 7.3.5 NANOCOMPOSITES
337
7.4 ONE-DIMENSIONAL NANOSTRUCTURES 340
7.4.1 NANOWIRES AND NANORODS 340
7.4.2 NANOTUBES 342
7.4.2.1 . CHEMICAL FUNCTIONALIZATION O F CARBON NANOTUBES 345 7.5
NANOMETER-SCALE LAYERS 347
7.5.1 GRAPHENE 348
7.5.2 SELF-ASSEMBLED MONOLAYERS 349
GLOSSARY 353
INDEX 361 |
| any_adam_object | 1 |
| author | Schubert, Ulrich Hüsing, Nicola 1969- |
| author_GND | (DE-588)115836349 |
| author_facet | Schubert, Ulrich Hüsing, Nicola 1969- |
| author_role | aut aut |
| author_sort | Schubert, Ulrich |
| author_variant | u s us n h nh |
| building | Verbundindex |
| bvnumber | BV039853201 |
| classification_rvk | VE 9301 VH 5500 VN 6020 ZM 6000 |
| ctrlnum | (OCoLC)758984615 (DE-599)DNB1011200317 |
| dewey-full | 541.39 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 541 - Physical chemistry |
| dewey-raw | 541.39 |
| dewey-search | 541.39 |
| dewey-sort | 3541.39 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Werkstoffwissenschaften / Fertigungstechnik |
| edition | 3., compl. rev. and enl. ed. |
| format | Book |
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| id | DE-604.BV039853201 |
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| indexdate | 2024-07-21T00:22:40Z |
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| isbn | 9783527327140 3527327142 |
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| owner | DE-91G DE-BY-TUM DE-20 DE-11 DE-703 DE-92 DE-19 DE-BY-UBM DE-355 DE-BY-UBR DE-83 DE-384 DE-188 |
| owner_facet | DE-91G DE-BY-TUM DE-20 DE-11 DE-703 DE-92 DE-19 DE-BY-UBM DE-355 DE-BY-UBR DE-83 DE-384 DE-188 |
| physical | XXII, 370 S. Ill., graph. Darst. |
| publishDate | 2012 |
| publishDateSearch | 2012 |
| publishDateSort | 2012 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Schubert, Ulrich Verfasser aut Synthesis of inorganic materials Ulrich Schubert and Nicola Hüsing 3., compl. rev. and enl. ed. Weinheim Wiley-VCH 2012 XXII, 370 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Ausgangsmaterial (DE-588)4143518-7 gnd rswk-swf Anorganischer Werkstoff (DE-588)4142570-4 gnd rswk-swf Anorganische Synthese (DE-588)4068736-3 gnd rswk-swf Verfahrenstechnik (DE-588)4062781-0 gnd rswk-swf Anorganischer Werkstoff (DE-588)4142570-4 s Ausgangsmaterial (DE-588)4143518-7 s Anorganische Synthese (DE-588)4068736-3 s Verfahrenstechnik (DE-588)4062781-0 s DE-604 Hüsing, Nicola 1969- Verfasser (DE-588)115836349 aut X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=3718069&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024712898&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Schubert, Ulrich Hüsing, Nicola 1969- Synthesis of inorganic materials Ausgangsmaterial (DE-588)4143518-7 gnd Anorganischer Werkstoff (DE-588)4142570-4 gnd Anorganische Synthese (DE-588)4068736-3 gnd Verfahrenstechnik (DE-588)4062781-0 gnd |
| subject_GND | (DE-588)4143518-7 (DE-588)4142570-4 (DE-588)4068736-3 (DE-588)4062781-0 |
| title | Synthesis of inorganic materials |
| title_auth | Synthesis of inorganic materials |
| title_exact_search | Synthesis of inorganic materials |
| title_full | Synthesis of inorganic materials Ulrich Schubert and Nicola Hüsing |
| title_fullStr | Synthesis of inorganic materials Ulrich Schubert and Nicola Hüsing |
| title_full_unstemmed | Synthesis of inorganic materials Ulrich Schubert and Nicola Hüsing |
| title_short | Synthesis of inorganic materials |
| title_sort | synthesis of inorganic materials |
| topic | Ausgangsmaterial (DE-588)4143518-7 gnd Anorganischer Werkstoff (DE-588)4142570-4 gnd Anorganische Synthese (DE-588)4068736-3 gnd Verfahrenstechnik (DE-588)4062781-0 gnd |
| topic_facet | Ausgangsmaterial Anorganischer Werkstoff Anorganische Synthese Verfahrenstechnik |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=3718069&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024712898&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT schubertulrich synthesisofinorganicmaterials AT husingnicola synthesisofinorganicmaterials |