Hierarchically structured porous materials: from nanoscience to catalysis, separation, optics, energy, and life science
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| Beschreibung: | XXV, 651 S. Ill., graph. Darst. |
| ISBN: | 9783527327881 3527327886 |
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IMAGE 1
CONTENTS
PREFACE XVII LIST OF CONTRIBUTORS XXI
PART I INTRODUCTION 1
1 INSIGHTS INTO HIERARCHICALLY STRUCTURED POROUS MATERIALS: FROM
NANOSCIENCE TO CATALYSIS, SEPARATION, OPTICS, ENERGY, AND LIFE SCIENCE 3
BAO-LIAN SU, CLEMENT SANCHEZ, AND XIAO-YU YANG 1.1 INTRODUCTION 3
1.2 SYNTHESIS STRATEGIES TO HIERARCHICALLY STRUCTURED POROUS MATERIALS 8
1.3 EMERGING APPLICATIONS OF HIERARCHICALLY STRUCTURAL POROUS MATERIALS
16 1.4 CONCLUSIONS 20
ACKNOWLEDGMENTS 20 REFERENCES 21
2 HIERARCHY IN NATURAL MATERIALS 29 PETER FRATZL AND MARIE MADELEINE
GIRAUD GUILLE 2.1 NATURAL MATERIALS AS A SOURCE OF INSPIRATION IN
MATERIALS SCIENCE 29 2.2 HIERARCHIES BASED ON FIBER ARCHITECTURES 31 2.3
LIQUID CRYSTALLINE ASSEMBLIES, CLUES TO MIMIC HIERARCHICAL
STRUCTURES 33
2.4 MINERALIZED BIOLOGICAL TISSUES, MODELS FOR HYBRID MATERIALS 34 2.5
CONCLUDING REMARKS 37
REFERENCES 37
BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/1011200376
DIGITALISIERT DURCH
IMAGE 2
VI CONTENTS
PART II SYNTHESIS STRATEGIES TO HIERARCHICALLY STRUCTURED POROUS
MATERIALS 41
3 HIERARCHICALLY STRUCTURED POROUS MATERIALS BY DUALLY MICELLAR
TEMPLATING APPROACH 43 OEZLEM SEL AND BERND M. SMARSLY
3.1 INTRODUCTION 43
3.2 NANOCASTING - TRUE LIQUID CRYSTALLINE TEMPLATING 43 3.2.1
SURFACTANTS AND BLOCK COPOLYMER MESOPHASES AS TEMPLATES 45 3.2.2 IONIC
LIQUIDS AS TEMPLATES 45 3.3 BASICS OF MICELLIZATION 46 3.3.1 THE DRIVING
FORCE FOR MICELLIZATION - HYDROPHOBIE EFFECT 47 3.3.2 THERMODYNAMICS OF
MICELLE FORMATION 48 3.4 MIXED SURFACTANT SOLUTIONS 49 3.4.1 MIXED
SURFACTANT SYSTEMS AT HIGHER CONCENTRATIONS 49 3.5 HIERARCHICAL
SELF-ASSEMBLY OF CONCENTRATED AQUEOUS SURFACTANT
MIXTURES - HIERARCHICAL MESOPOROUS STRUCTURES 50 3.6 CONCLUSIONS 52
REFERENCES 52
4 COLLOIDAL CRYSTAL TEMPLATING APPROACHES TO MATERIALS WITH HIERARCHICAL
POROSITY 55
NICHOLAS D. PETKOVICH AND ANDREAS STEIN
4.1 INTRODUCTION AND HISTORICAL OVERVIEW 55 4.1.1 OPALS AND COLLOIDAL
CRYSTALS 56 4.1.2 INVERSE OPALS AND THREE-DIMENSIONALLY ORDERED
MACROPOROUS MATERIALS 58
4.2 THE PREPARATION OF 3D0M MATERIALS 61 4.2.1 MONODISPERSE COLLOIDAL
SPHERES 61 4.2.2 METHODS TO ASSEMBLE COLLOIDAL CRYSTALS 63 4.2.3
INFILTRATION AND PROCESSING ROUTES 66 4.3 3DOM MATERIALS WITH INTRINSIC
SECONDARY POROSITY 69 4.3.1 POROSITY PRODUCED IN SOL-GEL SYNTHESES 69
4.3.2 TEXTURAL MESOPORES IN NANOCRYSTALLINE WALLS 72 4.3.3 POROSITY IN
CARBON MATERIALS 75 4.3.4 USING NANOCOMPOSITES TO GENERATE POROSITY 76
4.3.5 POROSITY IN 3D0M CLAY MINERALS 76 4.4 HIERARCHICAL MATERIALS FROM
MULTIMODAL COLLOIDAL CRYSTAL
TEMPLATES 77
4.4.1 TEMPLATES FROM COMBINATIONS OF POLYMER SPHERES WITH SIMILAR SIZES
78 4.4.2 TEMPLATES FROM COMBINATIONS OF POLYMER SPHERES AND SMALL SILICA
COLLOIDS 81 4.4.3 HETEROSTRUCTURED COLLOIDAL CRYSTAL TEMPLATES 83
IMAGE 3
CONTENTS VII
4.5 HIERARCHICAL MATERIALS FROM COMBINATIONS OF SOFT AND COLLOIDAL
CRYSTAL TEMPLATING 84 4.5.1 COLLOIDAL CRYSTAL TEMPLATED ZEOLITES 86
4.5.2 INTRODUCTION TO SOFT TEMPLATING OF MESOPORES 86 4.5.3 HIERARCHICAL
SILICA STRUCTURES 88 4.5.3.1 CATIONIC SURFACTANT TEMPLATES 88 4.5.3.2
NONIONIC SURFACTANT TEMPLATES 89 4.5.3.3 IONIC-LIQUID SURFACTANT
TEMPLATES 92 4.5.4 HIERARCHICAL CARBON-CONTAINING STRUCTURES 92 4.5.4.1
PURE CARBON STRUCTURES 92 4.5.4.2 CARBON-SILICA COMPOSITES AND DERIVED
STRUCTURES 93
4.5.5 HIERARCHICAL ALUMINA STRUCTURES 96 4.5.6 HIERARCHICAL STRUCTURES
CONTAINING OTHER COMPOUNDS 97 4.5.7 STRUCTURES SYNTHESIZED VIA MULTIPLE
HARD AND SOFT TEMPLATES 98 4.5.8 FORMATION AND STRUCTURE OF MESOPORES
CONFINED IN COLLOIDAL
CRYSTALS 100
4.5.9 DISASSEMBLY AND REASSEMBLY OF 3DOM/M MATERIALS 301 4.6
HIERARCHICAL OPALS AND RELATED STRUCTURES 103 4.6.1 MONODISPERSE
MESOPOROUS SILICA SPHERES 103
4.6.2 SELF-ASSEMBLED HIERARCHICAL SILICA, CARBON, AND TIN OXIDE OPALS
104 4.6.3 3DOM ZEOLITES FROM HIERARCHICAL SILICA OPALS 307 4.6.4
ENCAPSULATED NON-CLOSE-PACKED HIERARCHICAL OPAL 108
4.6.5 INVERSE OPALS AS TEMPLATES FOR HIERARCHICAL OPALS 309 4.7
CONCLUSIONS AND OUTLOOK 332
ACKNOWLEDGMENTS 113 REFERENCES 334
5 TEMPLATING OF MACROPOROUS OR SWOLLEN MACROSTRUCTURED POLYMERS 131
MARYLINE CHEE KIMLING AND RACHEL A. CARUSO 5.1 INTRODUCTION 333
5.2 MACROPOROUS POLYMER GELS FORMED IN AMPHIPHILE SOLUTIONS 133 5.3
MACROPOROUS STARCH OR AGAROSE GELS 136 5.4 POLYMER FOAMS 140
5.5 POLYMERIC FILMS AND FIBROUS MATS 153 5.6 POLYMER SPHERES 359
5.7 CLOSING REMARKS 366
REFERENCES 368
6 BIOINSPIRED APPROACH TO SYNTHESIZING HIERARCHICAL POROUS MATERIALS 373
TIAN-YI MA AND ZHONG-YONG YUAN 6.1 INTRODUCTION 373
6.2 HIERARCHICAL POROUS MATERIALS FROM BIOTEMPLATES 3 76
IMAGE 4
VIM I CONTENTS
6.2.1 PLANT PARTS AS TEMPLATES 376
6.2.2 CELL AND BACTERIA AS TEMPLATES 381 6.2.3 SACCHARIDE AS TEMPLATES
185 6.2.4 DIATOMACEOUS EARTH AS TEMPLATES 188
6.2.5 EGGSHELL AS TEMPLATES 193 6.3 HIERARCHICAL POROUS MATERIALS FROM
THE BIOMIMETIC PROCESS 194 6.4 CONCLUSIONS AND PERSPECTIVES 203
REFERENCES 202
7 POROUS MATERIALS BY TEMPLATING OF SMALL LIQUID DROPS 209 HAIFEI ZHANG
7.1 INTRODUCTION 209
7.2 EMULSION TEMPLATING 210 7.2.1 HIPE TEMPLATING FOR HYDROPHILIC
POLYMERS AND RELATED MATERIALS 212
7.2.1.1 O/W HIPES 212 7.2.1.2 C/W HIPES 214 7.2.1.3 RELATED MATERIALS
216 7.2.2 MICROEMULSION TEMPLATING 218 7.2.3 FREEZE-DRYING OF EMULSIONS
221 7.3 BREATH FIGURES TEMPLATING 223 7.3.1 BREATH FIGURES 224 7.3.2
POLYMER 226
7.3.2.1 GENERAL POLYMERS 226 7.3.2.2 PROTEINS RELATED 228 7.3.2.3
MODIFICATION OF FILM CASTING AND EVAPORATION PROCESS 230 7.3.3 PARTICLES
231
7.3.3.1 POLYMER + NANOPARTIDES 231 7.3.3.2 NANOPARTIDES ONLY 231 7.3.4
POSTTREATMENT OF BF-TEMPLATED FILMS 234 7.3.4.1 CROSS-LINKING 234
7.3.4.2 CARBONIZATION 235 7.3.4.3 CALCINATION 235 7.4 CONCLUSIONS 236
ACKNOWLEDGMENT 237 REFERENCES 237 FURTHER READING 239
8 HIERARCHICALLY POROUS MATERIALS BY PHASE SEPARATION: MONOLITHS 241
KAZUKI NAKANISHI 8.1 INTRODUCTION 241
8.2 BACKGROUND AND CONCEPTS 242 8.2.1 POLYMERIZATION-INDUCED PHASE
SEPARATION IN OXIDE SOL GELS 242 8.2.2 STRUCTURE FORMATION PARALLELED
WITH SOL-GEL TRANSITION 246
8.2.3 MACROPORE CONTROL 247
IMAGE 5
CONTENTS IX
8.2.4 MESOPORE CONTROL 247
8.3 EXAMPLES OF MATERIALS WITH CONTROLLED MACRO/MESOPORES 248 8.3.1 PURE
SILICA 248
8.3.1.1 TYPICAL SYNTHESIS CONDITIONS 248 8.3.1.2 ADDITIONAL MESOPORE
FORMATION BY AGING 249 8.3.1.3 HIERARCHICALLY POROUS MONOLITHS 250
8.3.1.4 SUPRAMOLECULAR TEMPLATING OF MESOPORES 251 8.3.1.5 APPLICATIONS
252 8.3.2 SILOXANE-BASED ORGANIC-INORGANIC HYBRIDS 253 8.3.2.1 NETWORK
FROM PRECURSORS CONTAINING THE TRIALKOXYSILYL GROUP 253 8.3.2.2
HIERARCHICAL PORES IN AN MTMS-DERIVED NETWORK 253 8.3.2.3 NETWORK FROM
BRIDGED ALKOXYSILANES 254 8.3.2.4 CONVERSION INTO POROUS SIC CERAMICS
AND CARBON MONOLITHS 254 8.3.3 TITANIA AND ZIRCONIA 255
8.3.3.1 CHOICE OF STARTING COMPOUNDS 255 8.3.3.2 CONTROLS OVER
REACTIVITY 256 8.3.3.3 APPLICATIONS 257 8.3.4 ALUMINA AND ALUMINATES
FROM AN IONIC SOURCE 258 8.3.4.1 EPOXIDE-MEDIATED GEL FORMATION INTO
MACROPOROUS MONOLITHS 258
8.3.4.2 EXTENSION TO COMPLEX OXIDES 259 8.3.4.3 EXTENSION TO PHOSPHATES
259 8.3.5 HIGHLY CROSS-LINKED ORGANIC-POLYMER SYSTEM 260 8.3.5.1
DIVINYLBENZENE MONOLITHS 260 8.3.5.2 ACRYLATES AND OTHER NETWORKS 261
8.3.5.3 CONVERSION INTO CARBON MONOLITHS 261 8.4 SUMMARY 262
ACKNOWLEDGMENTS 263 REFERENCES 263
9 FEATURE SYNTHESIS OF HIERARCHICALLY POROUS MATERIALS BASED ON GREEN
EASY-LEACHING CONCEPT 269 GE TIAN, LI-HUA CHEN, XIAO-YU YANG, AND
BAO-LIAN SU
9.1 INTRODUCTION 269
9.2 HIERARCHICALLY STRUCTURED POROUS MATERIALS SYNTHESIZED BY
EASY-LEACHING AIR TEMPLATES 270 9.3 HIERARCHICALLY STRUCTURED POROUS
MATERIALS SYNTHESIZED BY EASY-LEACHING ICE TEMPLATE 272
9.3.1 CERAMICS 273
9.3.2 POLYMER 274
9.3.3 HYDROGELS (SILICA) 274 9.3.4 COMPOSITES 275
9.3.5 DEVELOPMENT OF METHODOLOGY 277 9.4 HIERARCHICALLY STRUCTURED
POROUS MATERIALS SYNTHESIZED BY EASY SELECTIVE-LEACHING METHOD 283
IMAGE 6
X| CONTENTS
9.5 OTHER EASY-LEACHING CONCEPTS IN THE SYNTHESIS OF HIERARCHICALLY
STRUCTURED POROUS MATERIALS 290 9.5.1 THREE-DIMENSIONAL
MESO-MACROSTRUCTURED SPONGELIKE SILICA MEMBRANES BY INORGANIC SALTS 290
9.5.2 BIOMODAL MESOPOROUS SILICAS BY DILUTE ELECTROLYTES 290 9.5.3
HIERARCHICAL BIOACTIVE POROUS SILICA GELS BY GAS TEMPLATING 293 9.5.4
HIERARCHICALLY POROUS MATERIALS BY CHEMICAL ETCHING 294
9.5.5 HIERARCHICALLY POROUS MATERIALS BY SUBLIMATION 294 9.6 SUMMARY 296
ACKNOWLEDGMENTS 296 REFERENCES 296
10 INTEGRATIVE CHEMISTRY ROUTES TOWARD ADVANCED FUNCTIONAL HIERARCHICAL
FOAMS 301 HERVE DELEUZE AND RENAL BACKOV 10.1 INTRODUCTION 301
10.2 ORGANIC-INORGANIC POLYHIPES PREPARED FROM WATER-IN-OIL EMULSIONS
304 10.2.1 NON-CHEMICALLY BONDED (CLASS I) HYBRID POLYHIPES 304 10.2.1.1
INORGANIC PRECURSOR IN THE HIPE AQUEOUS PHASE 304 10.2.1.2 METAL
PARTICLE GENERATION ONTO POLYHIPE SURFACE 305 10.2.1.3 NANOCOMPOSITES
308
10.2.1.4 ORGANIC-INORGANIC INTERPENETRATING NETWORKS 313 10.2.1.5 HARD
TEMPLATE REPLICA 313 10.2.2 CHEMICALLY BONDED (CLASS II) HYBRID
POLYHIPES 313 10.2.2.1 INORGANIC-ORGANIC PRECURSOR'S COPOLYMERIZATION
313
10.2.2.2 ORGANIC-ORGANOMETALLIC PRECURSORS COPOLYMERIZATION 314 10.2.2.3
ORGANOMETALLIC POLYHIPE FUNCTIONALIZARION 316 10.3 ORGANIC-INORGANIC
POLYHIPES PREPARED FROM DIRECT EMULSIONS 316 10.3.1 FUNCTIONAL
ORGANIC-INORGANIC POLYHIPES 316 10.3.1.1 SILICA FOAMS (SI-HIPE) 316
10.3.1.2 EU 3+ @ORGANO-SI(HIPE) MACRO-MESOCELLULAR HYBRID FOAMS
GENERATION AND PHOTONIC PROPERTIES 317 10.3.1.3 PD@ORGANO-SI(HIPE)
HYBRID MONOLITHS: GENERATION OFFERING CYCLING HECK CATALYSIS REACTIONS
318 10.3.1.4 ENZYME@ORGANO-SI(HIPE) HYBRID MONOLITHS: HIGHLY EFFICIENT
BIOCATALYSTS 321
10.3.2 SI(HIPE) AS HARD TEMPLATE TO CARBONACEOUS FOAMS AND APPLICATIONS
324 10.3.2.1 FROM SI(HIPE) TO CARBON(HIPE) AND THEIR USE AS LI-ION
NEGATIVE ELECTRODES 325 10.3.2.2 FROM CARBON(HIPE) TO LIBH 4
@CARBON(HIPE) FOR HYDROGEN STORAGE
AND RELEASE PROPERTIES 326 10.4 PARTICLES-STABILIZED POLYHIPE 328 10.4.1
WATER-IN-OIL PICKERING EMULSIONS 329
IMAGE 7
CONTENTS XI
10.4.2 OIL-IN-WATER PICKERING EMULSION 329
10.5 CONCLUSION AND PERSPECTIVES 330 REFERENCES 331
11 HIERARCHICALLY STRUCTURED POROUS COATINGS AND MEMBRANES 335 CEDRIC
BOISSIERE, ERIC PROUZET, DAVID GROSSO, AND CLEMENT SANCHEZ 11.1
INTRODUCTION 335
11.2 THE MULTIPLE TEMPLATING STRATEGY 336 11.2.1 HIERARCHICAL INORGANIC
NANOPATTERNING 337 11.2.2 IONIC LIQUID (IL)/BLOCK COPOLYMER SOFT-SOFT
TEMPLATING 338 11.2.3 POLYMER/BLOCK COPOLYMER SOFT-SOFT TEMPLATING 338
11.2.4 BLOCK COPOLYMER/LATEX BEADS SOFT-HARD TEMPLATING FOR HIERARCHICAL
METALLIC THIN FILMS 339 11.3 DYNAMIC TEMPLATING 340
11.3.1 CONTROLLED PHASE SEPARATION 340 11.3.2 BREATH FIGURES AS SMART
TEMPLATES 341 11.4 BUILDING BLOCK ASSEMBLIES FOR PHOTONIC BAND GAP
MATERIALS 343 11.4.1 THE LATEX GAMES 343
11.4.2 MULTILAYER DEPOSITION OF POMTF 344 11.5 INK-JET PRINTING AND
COOPERATIVE SELF-ASSEMBLY 345 11.6 FOAMING PROCESSES 345
11.6.1 2D MESOMACROCELLULAR 345 11.7 FILTRATION MEMBRANES 347
11.7.1 MICROPOROUS HIERARCHICAL MEMBRANES 348 11.7.1.1 MESOSTRUCTURED
HIERARCHICAL MEMBRANES GENERATED INTO THE POROUS SUBSTRATE 353 11.7.2
MESOSTRUCTURED HIERARCHICAL MEMBRANES GENERATED BY EISA 353 11.8
CONCLUSION 357
REFERENCES 358
12 SELF-FORMATION PHENOMENON TO HIERARCHICALLY STRUCTURED POROUS
MATERIALS 363 XIAO-YU YANG, GE TIAN, LI-HUA CHEN, AND BAO-LIAN SU 12.1
INTRODUCTION 363
12.2 HISTORY OF SELF-FORMATION PHENOMENON 364 12.3 FEATURES OF
SELF-FORMATION PHENOMENON 367 12 A STRUCTURAL FEATURES OF HIERARCHICAL
POROUS MATERIALS BASED ON THE SELF-FORMATION PHENOMENON 368 12.5 THE
MECHANISM OF SELF-FORMATION PROCEDURE 373 12.5.1 SURFACTANT-TEMPLATING
MECHANISM 373
12.5.2 AGGREGATION MECHANISM FOR THE FORMATION OF MESOPOROUS STRUCTURES
375 12.5.3 MICROPHASE-SEPARATED MECHANISM FOR THE FORMATION OF
MACROPOROUS STRUCTURES 376 12.5.4 POROGEN MECHANISM 376
IMAGE 8
XII I CONTENTS
12.6 CONTROLLED SYNTHESIS BASED ON THE SELF-FORMATION PHENOMENA 384
12.6.1 THE EFFECT OF METAL ALKOXIDE 384 12.6.2 THE EFFECT OF SURFACTANT
388 12.6.3 THE EFFECT OF PH VALUES 390 12.6.4 THE EFFECT OF SOLVENT 392
12.6.5 THE EFFECT OF HYDROTHERMAL SYNTHESIS 394 12.7 DEVELOPMENT OF
SYNTHESIS METHODOLOGY 396 12.7.1 COMBINATION OF S ELF- FORMATION AND
TEMPLATING STRATEGY 396 12.7.2 COMBINATION OF SELF-FORMATION AND
TEMPLATE REPLICATE 396 12.7.3 COMBINATION OF SELF-FORMATION AND ZEOLITIC
CRYSTALLIZATION
PROCEDURES: PERSPECTIVES 399 12.8 APPLICATIONS AND HIERARCHICAL
CATALYSIS 399 12.9 SUMMARY 402
ACKNOWLEDGMENTS 403 REFERENCES 403
13 AUTO-GENERATED HIERARCHICAL MESO-MACROPOROUS ALUMINOSILICATE
MATERIALS WITH HIGH TETRAHEDRAL AI CONTENT FROM THE SINGLE-MOLECULAR
ALKOXY-PRECURSOR (SMAP) STRATEGY 407 ARNAUD LEMAIRE AND BAO-LIAN SU 13.1
INTRODUCTION 407
13.2 HIERARCHICALLY STRUCTURED MESO-MACROPOROUS ALUMINOSILICATES 409
13.2.1 SINGLE-MOLECULAR ALKOXY PRECURSOR (SMAP): EFFECT OF PH 409 13.2.2
SINGLE-MOLECULAR ALKOXY PRECURSOR: EFFECT OF CHELATING AGENTS 413 13.2.3
SINGLE-MOLECULAR ALKOXY PRECURSOR: EFFECT OF TMOS 436 13.2.3.1 GENERAL
FEATURES OF MATERIALS OBTAINED 416 13.2.3.2 DIRECT OBSERVATION OF
MACROPORE FORMATION BY AN OPTICAL
MICROSCOPE 418
13.2.3.3 CONCLUSIONS 423 13.2.4 SINGLE-MOLECULAR ALKOXY PRECURSOR:
EFFECT OF TAOS 423 13.2.4.1 GENERAL FEATURES OF MATERIALS OBTAINED 423
13.2.4.2 MECHANISTIC CONSIDERATIONS 425 13.2.4.3 CONCLUSIONS 425 13.3
CONCLUSION 426
ACKNOWLEDGMENT 426 REFERENCES 427 FURTHER READING 433
14 ZEOLITES WITH HIERARCHICALLY POROUS STRUCTURE: MESOPOROUS ZEOLITES
435 FENG-SHOU XIAO AND XIANGJU MENG
14.1 INTRODUCTION 435
14.2 MESOPOROUS ZEOLITES FORMED BY POSTTREATMENTS 437 14.3 MESOPOROUS
ZEOLITES CREATED BY SOLID TEMPLATES 438 14.4 MESOPOROUS ZEOLITES CREATED
BY SOFT TEMPLATES 442
IMAGE 9
CONTENTS XIII
14.5 FUNCTIONALIZATION OF MESOPOROUS ZEOLITES 449
14.6 PERSPECTIVES IN THE SYNTHESIS OF ORDERED MESOPOROUS ZEOLITES 452
REFERENCES 453
15 MICRO-MACROPOROUS STRUCTURED ZEOLITE 457 YA-HONG ZHANG, LI-HUA CHEN,
YI TANG, XIAO-YU YANG, AND BAO-LIAN SU 15.1 INTRODUCTION 457
15.2 HOLLOW MICRO-MACROPOROUS STRUCTURE 457 15.3 MICRO-MACROPOROUS
MONOLITHS 465 15.4 CONCLUSION AND REMARKS 471 REFERENCES 475
PART III EMERGING APPLICATIONS OF HIERARCHICALLY STRUCTURED POROUS
MATERIALS 481
16 HIERARCHICALLY POROUS MATERIALS IN CATALYSIS 483 TOSHIYUKI YOKOI AND
TAKASHI TATSUMI 16.1 INTRODUCTION 483
16.2 ACID CATALYST 484
16.2.1 ALKALI POSTTREATMENT OF ZEOLITE 484 16.2.2 SYNTHESIS OF MICRO-AND
MESOPOROUS COMPOSITES 486 16.2.3 CREATION OF INTRACRYSTALLINE
MESOPOROSITY BY USING HARD TEMPLATE 486
16.2.3.1 USE OF SILANE-FUNCTIONALIZED POLYMER 487 16.2.3.2
AL-SBA-15/CARBON COMPOSITE 488 16.2.3.3 USE OF CATIONIC POLYMER 490
16.2.4 USE OF AMPHIPHILIC SURFACTANT 493 16.2.5 ZEOLITE NANOSHEETS 493
16.2.6 PILLARING AND DELAMINATION 498 16.2.6.1 DELAMINATION OF THE
ZEOLITIC-LAYERED PRECURSOR 498 16.2.6.2 INTERLAYER-EXPANDED ZEOLITE 499
16.3 TITANOSILICATES 500
16.3.1 TS-1-BASED MATERIAL 500 16.3.2 MWW-BASED MATERIAL 502 16.3.3
HIERARCHICAL MESOPOROUS TITANOSILICATE 506 16.4 CONCLUSIONS AND OUTLOOK
511
REFERENCES 531
17 HIERARCHICALLY STRUCTURED POROUS MATERIALS: APPLICATION TO SEPARATION
SCIENCES 537 KAZUKI NAKANISHI 17.1 INTRODUCTION 537
17.2 SEPARATION MEDIUM FOR HPLC 517 17.2.1 PARTIDE-PACKED COLUMNS AS
SEPARATION MEDIA FOR HPLC 537 17.2.2 MONOLITHIC SILICA FOR HPLC COLUMNS
538
IMAGE 10
XIV CONTENTS
17.2.3 COMPARISON BETWEEN MONOLITHIC AND PARTICLE-PACKED
COLUMNS 520
17.2.3.1 BACKPRESSURE 520 17.2.3.2 EFFICIENCY 521 17.2.3.3 ROBUSTNESS
522 17.2.3.4 CLADDING AND PORE HOMOGENEITY 522 17.3 VARIATIONS IN COLUMN
FORMAT AND PORE STRUCTURES 523 17.3.1 LONG CAPILLARY COLUMNS WITH HIGH
PERMEABILITY 523 17.3.2 COLUMNS WITH FINER DOMAINS 525 17.3.3 MONOLITHS
WITH FULLY TEMPLATED MESOPORES 526 17.4 PRODUCTS 526
17.4.1 PRECONCENTRATION DEVICES 526 17.4.2 BIOREACTORS AND DNA PURIFIERS
527 17.4.3 THERAPEUTIC APHERESIS DEVICE 527 17.5 SUMMARY 527
ACKNOWLEDGMENTS 528 REFERENCES 528
18 COLLOIDAL PHOTONIC CRYSTALS: FABRICATION AND APPLICATIONS 531
QJNGFENG YAN, JIE YU, ZHONGYU CAI, AND X. S. ZHAO 18.1 PHOTONIC CRYSTALS
531 18.2 COLLOIDAL SELF-ASSEMBLY APPROACH TO PHOTONIC CRYSTALS 532
18.2.1 SEDIMENTATION 533 18.2.2 SPIN COATING 535
18.2.3 PHYSICAL CONFINEMENT 536 18.2.4 VERTICAL DEPOSITION 537 18.2.5
HORIZONTAL DEPOSITION 539 18.2.6 SPRAY COATING AND PRINTING 540
18.2.7 LAYER-BY-LAYER METHOD 540 18.2.8 OTHER METHODS 541 18.3 OPTICAL
DOPING IN COLLOIDAL PHOTONIC CRYSTALS 542
18.3.1 LINE DEFECT ENGINEERING 544 18.3.2 PLANAR DEFECT ENGINEERING 549
18.3.3 POINT DEFECT ENGINEERING 553 18.4 BAND-GAP ENGINEERING IN
COLLOIDAL PHOTONIC CRYSTALS 557
18.4.1 HETEROSTRUCTURES 558 18.4.2 SUPERLATTICES 560 18.4.3 OTHER
HIERARCHICAL COLLOIDAL PHOTONIC CRYSTAL STRUCTURES 560 18.5 PHOTONIC
DEVICES BASED ON COLLOIDAL PHOTONIC CRYSTALS 562
18.5.1 LASING IN 3D COLLOIDAL PHOTONIC CRYSTALS 562 18.5.2 SENSORS BASED
ON 3D COLLOIDAL PHOTONIC CRYSTALS 564 18.5.3 WAVEGUIDE IN 3D COLLOIDAL
PHOTONIC CRYSTALS 564 18.5.4 STRUCTURAL COLOR AND DISPLAY DEVICES 566
IMAGE 11
CONTENTS XV
18.6 OUTLOOK 569
ACKNOWLEDGMENTS 573 REFERENCES 571
19 HIERARCHICALLY STRUCTURED POROUS MATERIALS FOR ENERGY CONVERSION AND
STORAGE 577 BAO-LIAN SU
19.1 INTRODUCTION 577
19.2 HIERARCHICALLY STRUCTURED POROUS MATERIALS FOR ENERGY CONVERSION
579 19.2.1 SUNLIGHT CONVERSION TO CHEMICALS AND ELECTRICITY 579 19.2.1.1
HIERARCHICALLY STRUCTURED POROUS MATERIALS FOR LIGHT HARVESTING,
PHOTOCHEMICAL H2 PRODUCTION, AND PHOTOCATALYSIS 579 19.2.1.2
HIERARCHICALLY STRUCTURED POROUS MATERIALS FOR DYE-SENSITIZED SOLAR
CELLS (DSSCS) 583 19.2.1.3 HIERARCHICALLY STRUCTURED POROUS MATERIALS
FOR IMMOBILIZATION OF
PHOTOSYNTHETIC SPECIES 585 19.2.2 HIERARCHICALLY STRUCTURED POROUS
MATERIALS FOR FUEL CELLS (FCS) 588 19.3 HIERARCHICALLY STRUCTURED POROUS
MATERIALS FOR ENERGY
STORAGE 593
19.3.1 HIERARCHICALLY STRUCTURED POROUS MATERIALS FOR LI BATTERIES 593
19.3.2 HIERARCHICALLY STRUCTURED POROUS MATERIALS FOR SUPERCAPACITORS
594 19.4 CONCLUSION AND OUTLOOK 597
REFERENCES 597
20 HIERARCHICALLY STRUCTURED POROUS MATERIALS-APPLICATIONS IN
BIOCHEMISTRY: BIOCERAMICS, LIFE SCIENCE, AND DRUG DELIVERY 603 MARIA
VALLET-REGI AND MIGUEL MANZANO
20.1 INTRODUCTION 601
20.2 BIOCERAMICS 601
20.2.1 FIRST GENERATION: BIO-INERTS 603 20.2.2 SECOND GENERATION:
BIOACTIVES AND RESORBABLES 603 20.2.3 THIRD GENERATION: DRIVING LIVING
TISSUE REGENERATION 603
20.3 LIFE SCIENCE 603
20.3.1 BONE TISSUE ENGINEERING 603 20.3.2 POROUS CALCIUM PHOSPHATES 606
20.3.3 POROUS BIOGLASSES 606 20.3.4 SILICA MESOPOROUS MATERIALS 608 20.4
DRUG DELIVERY 610
20.4.1 SILICA MESOPOROUS MATERIALS 633 20.4.2 TEMPLATED GLASSES 633
20.4.3 STIMULI-RESPONSIVE DRUG DELIVERY SYSTEMS 614 20.5
THREE-DIMENSIONAL SCAFFOLDS 616
REFERENCES 616
IMAGE 12
XVI CONTENTS
21 ON THE OPTIMAL MECHANICAL PROPERTIES OF HIERARCHICAL
BIOMATERIALS 621 H. X. ZHU, T. X. FAN, AND D. ZHANG 21.1 INTRODUCTION
621
21.2 MECHANICS OF MATERIALS OF FIRST-LEVEL HIERARCHY 622 21.2.1 YOUNG'S
MODULUS E X 623 21.2.2 TENSILE STRENGTH SI 625 21.2.3 FLAW TOLERANCE 627
21.2.4 TOUGHNESS 627 21.3 MECHANICS OF MATERIALS OF THE HIGHER LEVEL
HIERARCHY 628
21A RESULTS AND DISCUSSION 629 REFERENCES 630
PART IV CONCLUSION 633
22 CONCLUDING REMARKS 635 BAO-LIAN SU, CLEMENT SANCHEZ, AND XIAO-YU YANG
22.1 LOOKING BACK 635 22.2 LOOKING FORWARD 636
INDEX 639 |
| any_adam_object | 1 |
| author2 | Su, Bao-Lian |
| author2_role | edt |
| author2_variant | b l s bls |
| author_GND | (DE-588)1017521905 |
| author_facet | Su, Bao-Lian |
| building | Verbundindex |
| bvnumber | BV039811432 |
| classification_rvk | VE 9300 VE 9850 |
| ctrlnum | (OCoLC)766264623 (DE-599)DNB1011200376 |
| dewey-full | 620.116 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 620 - Engineering and allied operations |
| dewey-raw | 620.116 |
| dewey-search | 620.116 |
| dewey-sort | 3620.116 |
| dewey-tens | 620 - Engineering and allied operations |
| discipline | Chemie / Pharmazie Maschinenbau / Maschinenwesen |
| format | Book |
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| id | DE-604.BV039811432 |
| illustrated | Illustrated |
| indexdate | 2024-07-21T00:20:59Z |
| institution | BVB |
| isbn | 9783527327881 3527327886 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-024671731 |
| oclc_num | 766264623 |
| open_access_boolean | |
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| owner_facet | DE-29T DE-92 DE-19 DE-BY-UBM |
| physical | XXV, 651 S. Ill., graph. Darst. |
| publishDate | 2012 |
| publishDateSearch | 2012 |
| publishDateSort | 2012 |
| publisher | Wiley-VCH-Verl. |
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| spelling | Hierarchically structured porous materials from nanoscience to catalysis, separation, optics, energy, and life science ed. by Bao-Lian Su ... Weinheim Wiley-VCH-Verl. 2012 XXV, 651 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Literaturangaben Poröser Stoff (DE-588)4046811-2 gnd rswk-swf Bionik (DE-588)4006888-2 gnd rswk-swf Nanoporöser Stoff (DE-588)4800345-1 gnd rswk-swf Mikroporosität (DE-588)4604721-9 gnd rswk-swf Size-Effekt (DE-588)4181611-0 gnd rswk-swf Makroporosität (DE-588)4831894-2 gnd rswk-swf Poröser Stoff (DE-588)4046811-2 s Makroporosität (DE-588)4831894-2 s Mikroporosität (DE-588)4604721-9 s Nanoporöser Stoff (DE-588)4800345-1 s Size-Effekt (DE-588)4181611-0 s Bionik (DE-588)4006888-2 s DE-604 Su, Bao-Lian (DE-588)1017521905 edt X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=3718075&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024671731&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Hierarchically structured porous materials from nanoscience to catalysis, separation, optics, energy, and life science Poröser Stoff (DE-588)4046811-2 gnd Bionik (DE-588)4006888-2 gnd Nanoporöser Stoff (DE-588)4800345-1 gnd Mikroporosität (DE-588)4604721-9 gnd Size-Effekt (DE-588)4181611-0 gnd Makroporosität (DE-588)4831894-2 gnd |
| subject_GND | (DE-588)4046811-2 (DE-588)4006888-2 (DE-588)4800345-1 (DE-588)4604721-9 (DE-588)4181611-0 (DE-588)4831894-2 |
| title | Hierarchically structured porous materials from nanoscience to catalysis, separation, optics, energy, and life science |
| title_auth | Hierarchically structured porous materials from nanoscience to catalysis, separation, optics, energy, and life science |
| title_exact_search | Hierarchically structured porous materials from nanoscience to catalysis, separation, optics, energy, and life science |
| title_full | Hierarchically structured porous materials from nanoscience to catalysis, separation, optics, energy, and life science ed. by Bao-Lian Su ... |
| title_fullStr | Hierarchically structured porous materials from nanoscience to catalysis, separation, optics, energy, and life science ed. by Bao-Lian Su ... |
| title_full_unstemmed | Hierarchically structured porous materials from nanoscience to catalysis, separation, optics, energy, and life science ed. by Bao-Lian Su ... |
| title_short | Hierarchically structured porous materials |
| title_sort | hierarchically structured porous materials from nanoscience to catalysis separation optics energy and life science |
| title_sub | from nanoscience to catalysis, separation, optics, energy, and life science |
| topic | Poröser Stoff (DE-588)4046811-2 gnd Bionik (DE-588)4006888-2 gnd Nanoporöser Stoff (DE-588)4800345-1 gnd Mikroporosität (DE-588)4604721-9 gnd Size-Effekt (DE-588)4181611-0 gnd Makroporosität (DE-588)4831894-2 gnd |
| topic_facet | Poröser Stoff Bionik Nanoporöser Stoff Mikroporosität Size-Effekt Makroporosität |
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