Regioselektive Synthese von Pyranocarbazolalkaloiden:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | German |
| Veröffentlicht: |
2010
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | 181 S. graph. Darst. 21 cm |
Internformat
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| 100 | 1 | |a Gruner, Konstanze K. |d 1984- |e Verfasser |0 (DE-588)143643347 |4 aut | |
| 245 | 1 | 0 | |a Regioselektive Synthese von Pyranocarbazolalkaloiden |c von Konstanze Katharina Gruner |
| 264 | 1 | |c 2010 | |
| 300 | |a 181 S. |b graph. Darst. |c 21 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |a Dresden, Techn. Univ., Diss., 2010 | ||
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
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Datensatz im Suchindex
| _version_ | 1804145602237300736 |
|---|---|
| adam_text | INHALTSVERZEICHNIS
THEORETISCHER
TEIL..
1
EINLEITUNG
.............................................................................................................................
1
1.1
WAS
SIND
CARBAZOLE?
......................................................................................................
1
1.2
SYNTHESEMOEGLICHKEITEN
FUER
CARBAZOLE
.............................................................................
2
1.2.1
KLASSISCHE
METHODEN
................................................................................................
2
1.2.2
EISENVERMITTELTE
CARBAZOLSYNTHESE
..........................................................................
4
1.2.3
PALLADIUMKATALYSIERTE
CARBAZOLSYNTHESE
.................................................................
6
1.3
PYRANOCARBAZOLALKALOIDE
................................................................................................
11
1.4
METHODEN
ZUR
PYRANRINGANELLIERUNG
..............................................................................
13
2
SYNTHESEN
............................................................................................................................
18
2.1
GIRINIMBIN
(36)
UND
DIHYDROXYGIRINIMBIN
(44)
...............................................................
18
2.1.1
AKTUELLER
STAND
DER
GIRINIMBINFORSCHUNG
...............................................................
18
2.1.2
NEUE
GIRINIMBINSYNTHESEN
......................................................................................
21
2.1.3
ALLGEMEINES
ZU
DIHYDROXYGIRINIMBIN
(44)
...............................................................
27
2.1.4
ENANTIOSELEKTIVE
SYNTHESE
VON
DIHYDROXYGIRINIMBIN
(44)
NACH
KATSUKI
................
28
2.1.5
ENANTIOSELEKTIVE
SYNTHESE
VON
DIHYDROXYGIRINIMBIN
NACH
SHI
.............................
36
2.1.6
AUFKLAERUNG
DER
ABSOLUTEN
KONFIGURATION
.................................................................40
2.2
2,7-DIOXYGENIERTE
PYRANO[3,2-A]CARBAZOLE
...................................................................
46
2.2.1
ALLGEMEINES
............................................................................................................
46
2.2.2
ERSTE
TOTALSYNTHESE
VON
7-HYDROXYGIRINIMBIN
(39)
UND
7-HYDROXYMURRAYACIN
(116)
47
2.3
2,8-DIOXYGENIERTE
PYRANOCARBAZOLE
.............................................................................
51
2.3.1
TOTALSYNTHESE
VON
CARBALEXIN
B
(3B),
MUPAMIN
(123),
CLAUSIN
A
(134)
UND
CLAUSZOLIN-M
(137)
.................................................................................................
51
2.3.2
TOTALSYNTHESEN
DER
CLAUSZOLINE-B
(126),
-H
(127),
-G
(124)
UND
VON
HEPTAZOLICIN
(125)
.......................................................................................................................
62
2.4
2,6,8-TRIOXYGENIERTES
PYRANO[3,2-A]CARBAZOL:
MUKONICIN
(159)
..................................
76
2.5 CYCLISCHE
MONOTERPENOIDE
CARBAZOLE
.........................................................................
79
2.5.1
MAHANIMBIN
(40),
CYCLOMAHANIMBIN
(41)
UND
CURRYANGIN
(165)
.........................
82
2.5.2
MAHANIN
(166)
UND
MURRAYAMIN
D
(167)
...............................................................
89
2.5.3
MURRAYAMIN
B
(169)
UND
MURRAYAMIN
H
(170)
.......................................................
95
3
ZUSAMMENFASSUNG
UND
AUSBLICK
.......................................................................................
99
EXPERIMENTELLER
TEIL
..................................................................................................................
102
4
ALLGEMEINE
ANGABEN
........................................................................................................
103
4.1
CHEMIKALIEN
.................................................................................................................
103
4.2
ANALYTIK
..........................................................................................................................
104
5
SYNTHESEN
..........................................................................................................................
106
5.1
SYNTHESE
DER
PRECURSOR
...............................................................................................
106
5.2
SHI-KATALYSATOREN
.........................................................................................................
110
5.3
EUCHRESTIFOLIN
(65)
UND
GIRINIMBIN
(36)
........................................................................
116
5.4
SYNTHESE
VON
GIRINIMBIN
(36)
UEBER
DIE
EISENVERMITTELTE
VARIANTE
..............................
119
5.5
SYNTHESE
VON
GIRINIMBIN
(36)
UEBER
DIE
PALLADIUMKATALYSIERTE
VARIANTE
.....................
120
5.6
DIHYDROXYGIRINIMBIN
(44)
..............................................................................................
124
5.7
SYNTHESEN
VON
2,7-DIOXYGENIERTEN
PYRANOCARBAZOLEN
..............................................
133
5.8
SYNTHESEN
VON
2,8-DIOXYGENIERTEN
PYRANOCARBAZOLEN
..............................................
136
5.9
2,6,8-TRIOXYGENIERTES
PYRANO[3,2-A]CARBAZOL:
MUKONICIN
(159)
..................................
158
5.10
CYCLISCHE
MONOTERPENOIDE
PYRANOCARBAZOLE
.........................................................
161
LITERATURVERZEICHNIS
..................................................................................................................
173
ABKUERZUNGSVERZEICHNIS
.............................................................................................................
177
DANKSAGUNG
..............................................................................................................................
179
|
| any_adam_object | 1 |
| author | Gruner, Konstanze K. 1984- |
| author_GND | (DE-588)143643347 |
| author_facet | Gruner, Konstanze K. 1984- |
| author_role | aut |
| author_sort | Gruner, Konstanze K. 1984- |
| author_variant | k k g kk kkg |
| building | Verbundindex |
| bvnumber | BV037322512 |
| ctrlnum | (OCoLC)724706402 (DE-599)DNB1010320688 |
| dewey-full | 547.27 547.596 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 547 - Organic chemistry |
| dewey-raw | 547.27 547.596 |
| dewey-search | 547.27 547.596 |
| dewey-sort | 3547.27 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Thesis Book |
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| genre_facet | Hochschulschrift |
| id | DE-604.BV037322512 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T23:22:03Z |
| institution | BVB |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-022476675 |
| oclc_num | 724706402 |
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| physical | 181 S. graph. Darst. 21 cm |
| publishDate | 2010 |
| publishDateSearch | 2010 |
| publishDateSort | 2010 |
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| spelling | Gruner, Konstanze K. 1984- Verfasser (DE-588)143643347 aut Regioselektive Synthese von Pyranocarbazolalkaloiden von Konstanze Katharina Gruner 2010 181 S. graph. Darst. 21 cm txt rdacontent n rdamedia nc rdacarrier Dresden, Techn. Univ., Diss., 2010 (DE-588)4113937-9 Hochschulschrift gnd-content DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022476675&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Gruner, Konstanze K. 1984- Regioselektive Synthese von Pyranocarbazolalkaloiden |
| subject_GND | (DE-588)4113937-9 |
| title | Regioselektive Synthese von Pyranocarbazolalkaloiden |
| title_auth | Regioselektive Synthese von Pyranocarbazolalkaloiden |
| title_exact_search | Regioselektive Synthese von Pyranocarbazolalkaloiden |
| title_full | Regioselektive Synthese von Pyranocarbazolalkaloiden von Konstanze Katharina Gruner |
| title_fullStr | Regioselektive Synthese von Pyranocarbazolalkaloiden von Konstanze Katharina Gruner |
| title_full_unstemmed | Regioselektive Synthese von Pyranocarbazolalkaloiden von Konstanze Katharina Gruner |
| title_short | Regioselektive Synthese von Pyranocarbazolalkaloiden |
| title_sort | regioselektive synthese von pyranocarbazolalkaloiden |
| topic_facet | Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022476675&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT grunerkonstanzek regioselektivesynthesevonpyranocarbazolalkaloiden |