Single-Sided NMR:
Gespeichert in:
| Weitere Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Heidelberg [u.a.]
Springer
2011
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| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | XII, 244 S. graph. Darst. |
| ISBN: | 9783642163067 |
Internformat
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Datensatz im Suchindex
| _version_ | 1805095468561072128 |
|---|---|
| adam_text |
IMAGE 1
CONTENTS
1 SINGLE-SIDED NMR 1
FEDERICO CASANOVA, JUAN PERLO, AND BERNHARD BLUEMICH 1.1 DEVELOPMENT OF
OPEN NMR SENSORS 2
1.1.1 WELL-LOGGING TOOLS 2
1.1.2 MOBILE SINGLE-SIDED SENSORS 3
1.1.3 THE NMR-MOUSE 4
1.2 METHODS FOR MOBILE NMR 6
REFERENCES 7
2 NMR IN INHOMOGENEOUS FIELDS 11
FEDERICO CASANOVA AND JUAN PERLO 2. 1 INTRODUCTION 11
2.1.1 EVOLUTION OF THE MAGNETIZATION DURING A PULSE SEQUENCE . 12 2.1.2
SEPARATION OF THE MAGNETIZATION INTO COHERENCE PATHWAYS 14 2.1.3
NUMERICAL CALCULATION OF THE NMR SIGNAL 20
2.2 PULSE SEQUENCE ANALYSIS 21
2.2.1 SINGLE RF PULSE 21
2.2.2 THE GENERATION OF HAHN ECHOES 23
2.2.3 THE CPMG SEQUENCE 28
2.2.4 INVERSION AND SATURATION RECOVERY 35
2.2.5 DIFFUSION MEASUREMENTS 42
2.3 THE SNR IN INHOMOGENEOUS FIELDS 47
2.3.1 THE RECIPROCITY PRINCIPLE 48
2.3.2 NUMERICAL CALCULATIONS OF THE SNR 49
2.3.3 AN ANALYTICAL SOLUTION FOR THE SNR 55
REFERENCES 55
3 EX SITU MEASUREMENT OF ONE- AND TWO-DIMENSIONAL DISTRIBUTION FUNCTIONS
57
MARTIN D. HIIRLIMANN 3.1 INTRODUCTION 57
3.1.1 RELAXATION 57
BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/1006507558
DIGITALISIERT DURCH
IMAGE 2
X CONTENTS
3.1.2 DIFFUSION 58
3.1.3 DIFFUSION-RELAXATION DISTRIBUTION FUNCTIONS 58 3.2 PULSE SEQUENCES
AND SPIN DYNAMICS IN INHOMOGENEOUS FIELDS 59 3.2.1 RELAXATION
MEASUREMENT: CARR-PURCELL-MEIBOOM-GILL SEQUENCE 59
3.2.2 DIFFUSION MEASUREMENTS WITH STATIC GRADIENTS 62 3.2.3 T\
MEASUREMENTS IN INHOMOGENEOUS FIELDS 64
3.3 ONE-DIMENSIONAL DISTRIBUTION FUNCTIONS 64
3.3.1 DATA INVERSION 65
3.3.2 REGULARIZATION 67
3.3.3 SYSTEMATIC ERRORS 68
3.3.4 UNCERTAINTIES 68
3.4 TWO-DIMENSIONAL DIFFUSION-RELAXATION DISTRIBUTION FUNCTIONS . . 69
3.4.1 TWO-DIMENSIONAL DIFFUSION-RELAXATION MEASUREMENTS . 69 3.4.2 DATA
ANALYSIS 71
3.4.3 INTERPRETATION OF DISTRIBUTION FUNCTIONS 73
3.5 APPLICATIONS OF TWO-DIMENSIONAL DISTRIBUTION FUNCTIONS 74 3.5.1
TWO-COMPONENT SYSTEMS 75
3.5.2 WETTABILITY 76
3.5.3 COMPLEX MISCIBLE FLUID 77
3.5.4 STRUCTURED FLUID 78
3.5.5 PORE GEOMETRY OF POROUS MEDIA 79
3.6 CONCLUSION 81
REFERENCES 82
4 MAGNETS AND COILS FOR SINGLE-SIDED NMR 87
JUAN PERLO 4.1 MAGNETS 88
4.1.1 BO PERPENDICULAR TO THE SENSOR SURFACE, THE BAR MAGNET GEOMETRY 89
4.1.2 BO PARALLEL TO THE SENSOR SURFACE, THE U-SHAPED GEOMETRY 93 4.1.3
MAGNETS FOR DEPTH PROFILING 95
4.1.4 SWEET-SPOT MAGNETS 99
4.2 RF COILS 102
4.2.1 COILS FOR DEPTH PROFILING 103
4.2.2 COILS FOR SWEET-SPOT MAGNETS 105
4.3 GRADIENT COILS 107
REFERENCES 108
5 SINGLE-SIDED TOMOGRAPHY I LL
FEDERICO CASANOVA 5.1 DEPTH RESOLUTION USING THE STATIC FIELD GRADIENT I
LL
5.2 SPATIAL ENCODING BY FOURIER IMAGING 113
5.3 MULTI-ECHO ACQUISITION SCHEMES 117
IMAGE 3
CONTENTS XI
5.3.1 RARE-LIKE IMAGING SEQUENCE 117
5.3.2 CPMG-CP FOR QUADRATURE DETECTION 121
5.4 PERFORMANCE OF THE MULTI-ECHO DETECTION SCHEME 125 5.4.1 SENSITIVITY
IMPROVEMENT 125
5.4.2 RELAXATION AND DIFFUSION CONTRAST 126
5.4.3 3D IMAGING 128
5.5 DISPLACEMENT ENCODING 129
5.5.1 PFG METHODS IN INHOMOGENEOUS FIELDS 130
5.5.2 MEASUREMENT OF VELOCITY DISTRIBUTIONS 135
5.6 SPATIALLY RESOLVED VELOCITY DISTRIBUTIONS 137
5.6.1 2D VELOCITY MAPS 137
REFERENCES 140
6 HIGH-RESOLUTION NMR IN INHOMOGENEOUS FIELDS 143
VASILIKI DEMAS, JOHN M. FRANCK, JEFFREY A. REIMER, AND ALEXANDER PINES
6.1 INTRODUCTION 143
6.2 APPROACHES BASED ON SPIN INTERACTIONS 144
6.3 EX SITU NMR: SPATIALLY DEPENDENT "Z-ROTATIONS" 145 6.3.1 EX SITU
MATCHING: COMPENSATING STATIC FIELD INHOMOGENEITIES VIA SPATIALLY
MATCHED IF 147 6.3.2 SHIM PULSES: CORRECTIONS BASED ON GRADIENT
MODULATIONS DURING AN ADIABATIC DOUBLE PASSAGE 157 6.3.3 ADJUSTED CHIRP
SHIM PULSES 160
6.4 SUMMARY 162
REFERENCES 162
7 HIGH-RESOLUTION SPECTROSCOPY IN HIGHLY HOMOGENEOUS STRAY FIELDS . 165
ERNESTO P. DANIELI 7.1 SENSOR DESIGN 166
7.1.1 MAIN UNIT 166
7.1.2 SHIM UNIT 167
7.2 SHIMMING MAGNETIC FIELDS WITH MOVABLE PERMANENT MAGNETS 170 7.2.1
GENERATION OF LINEAR TERMS ALONG Y 171
7.2.2 GENERATION OF LINEAR TERMS ALONG X AND Z 172
7.2.3 GENERATION OF QUADRATIC TERMS X 2 AND Z 2 172
7.3 EXPERIMENTAL RESULTS 175
7.4 SHIMMING THE MAGNET TO HIGHER ORDER 177
7.4.1 IMPROVING RESOLUTION AND WORKING VOLUME SIZE 178 7.5 TEMPERATURE
COMPENSATION 181
7.6 CONCLUSIONS 185
REFERENCES 185
8 APPLICATIONS IN BIOLOGY AND MEDICINE 1 87
BERNHARD BLUEMICH 8.1 SKIN 188
8.2 TENDON 192
IMAGE 4
XII CONTENTS
8.3 MUMMIES AND BONES 194
8.4 UNILATERAL IMAGING OF BIOLOGICAL MATTER 196
8.5 CONCLUSIONS 198
REFERENCES 199
9 APPLICATIONS IN MATERIAL SCIENCE AND CULTURAL HERITAGE 203 JUERGEN KOLZ
9.1 ELASTOMERS 204
9.1.1 CROSSLINK DENSITY 204
9.1.2 AGING 206
9.1.3 IMAGING 209
9.2 HARD POLYMERS 212
9.2.1 INGRESS OF SOLVENTS 215
9.3 CULTURAL HERITAGE 217
REFERENCES 219
10 SPECTROMETER HARDWARE 221
JOERG FELDER 10.1 SINGLE-SIDED VS. CONVENTIONAL: SYSTEMATIC DIFFERENCES
222 10.2 FRONTEND DESIGN 223
10.2.1 MATCHING AND BALANCING 223
10.2.2 TRANSMIT-RECEIVE SWITCHING 226
10.3 TRANSMITTER DESIGN 228
10.3.1 CONVENTIONAL POWER AMPLIFIERS 229
10.3.2 ALTERNATIVE AMPLIFIER DESIGNS 230
10.4 RECEIVER DESIGN 233
10.4.1 LOW-NOISE AMPLIFIER 234
10.4.2 FREQUENCY GENERATION AND MIXING 235
10.5 DIGITAL HARDWARE 237
10.5.1 FRONTEND SIGNAL PROCESSOR SELECTION 237
10.5.2 DIGITAL PHASE SENSITIVE DETECTOR 239
REFERENCES 239
INDEX 241 |
| any_adam_object | 1 |
| author2 | Casanova, Federico |
| author2_role | edt |
| author2_variant | f c fc |
| author_facet | Casanova, Federico |
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| dewey-full | 538.362 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 538 - Magnetism |
| dewey-raw | 538.362 |
| dewey-search | 538.362 |
| dewey-sort | 3538.362 |
| dewey-tens | 530 - Physics |
| discipline | Chemie / Pharmazie Maschinenbau / Maschinenwesen Physik |
| format | Book |
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| indexdate | 2024-07-20T10:59:46Z |
| institution | BVB |
| isbn | 9783642163067 |
| language | English |
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| physical | XII, 244 S. graph. Darst. |
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| spelling | Single-Sided NMR Federico Casanova ... (eds.) Heidelberg [u.a.] Springer 2011 XII, 244 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier NMR-Spektroskopie (DE-588)4075421-2 gnd rswk-swf NMR-Spektroskopie (DE-588)4075421-2 s DE-604 Casanova, Federico edt X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=3531997&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=021158301&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Single-Sided NMR NMR-Spektroskopie (DE-588)4075421-2 gnd |
| subject_GND | (DE-588)4075421-2 |
| title | Single-Sided NMR |
| title_auth | Single-Sided NMR |
| title_exact_search | Single-Sided NMR |
| title_full | Single-Sided NMR Federico Casanova ... (eds.) |
| title_fullStr | Single-Sided NMR Federico Casanova ... (eds.) |
| title_full_unstemmed | Single-Sided NMR Federico Casanova ... (eds.) |
| title_short | Single-Sided NMR |
| title_sort | single sided nmr |
| topic | NMR-Spektroskopie (DE-588)4075421-2 gnd |
| topic_facet | NMR-Spektroskopie |
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