Microgel suspensions: fundamentals and applications
Gespeichert in:
| Weitere Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH
2011
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| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | XXI, 461 S. Ill., graph. Darst. |
| ISBN: | 9783527321582 |
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Datensatz im Suchindex
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IMAGE 1
CONTENTS
PREFACE XIII LIST OF CONTRIBUTORS XVII
PART ONE SYNTHESIS 1
1 MICROGELS AND THEIR SYNTHESIS: AN INTRODUCTION 3 ROBERT PELTON AND
LOAD HOARE 1.1 INTRODUCTION 3
1.1.1 DEFINING MICROGELS 3 1.1.1.1 THE GENERIC MICROGEL: STRUCTURE AND
CHARACTERIZATION 4 1.1.2 MICROGELS ARE SPECIAL 6 1.1.3 THE MICROGEL
LANDSCAPE 7 1.2 MICROGEL SYNTHESIS 8
1.2.1 INTRODUCTION 8
1.2.2 APPROACH 1: MICROGELS FORMED BY HOMOGENEOUS NUCLEATION 10 1.2.2.1
EMULSION POLYMERIZATION AND SURFACTANT-FREE EMULSION POLYMERIZATION 11
1.2.2.2 HOMOGENEOUS NUCLEATION OF MICROGELS FROM LINEAR POLYMERS 14
1.2.2.3 CORE-SHELL MICROGELS 14 1.2.3 APPROACH 2: MICROGELS FROM
EMULSIFICATION 15 1.2.4 APPROACH 3: MICROGELS BY POLYMER COMPLEXATION 16
1.2.5 EXOTIC MICROGELS 18 1.2.6 SUMMARY 19
1.3 PARTICLE DERIVATIZATION 19
1.3.1 CHEMICAL COUPLING TO MICROGELS 19 1.3.2 MICROGEL DECROSS-IINKING
19 1.3.3 CHARGED MICROGELS FROM NONIONIC PRECURSORS 20 1.3.4
NANOPARTIDE-FILLED GELS 21 1.4 MICROGEL PURIFICATION AND STORAGE 22
1.4.1 MICROGEL CHARACTERIZATION 22 1.5 CONCLUSIONS 25
REFERENCES 25
BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/1005391319
DIGITALISIERT DURCH
IMAGE 2
VI CONTENTS
2 POLYMERIZATION KINETICS OF MICROGEL PARTICLES 33
ABDELHAMID ELAISSARI AND ALI REZA MAHAAVIAN 2.1 INTRODUCTION 33
1.1 POLYMERIZATION PROCESSES 36 2.3 KINETICS OF POLYMERIZATION REACTION
37 2.3.1 THE INFLUENCE OF INITIATORS 39
13.1 THE EFFECT OF THE CROSS-LINKING AGENT 41 2.3.3 THE EFFECT OF
FUNCTIONAL MONOMERS 42 2.3.4 KINETIC ASPECTS OF MICROGEL FORMATION 45
2.4 CONCLUSIONS 49
REFERENCES 49
3 NEW FUNCTIONAL MICROGELS FROM MICROFLUIDICS 53 J'M-WOONG KIM AND
LIANG-YIN CHU 3.1 INTRODUCTION 53
3.2 MONODISPERSE THERMOSENSITIVE MICROGELS FABRICATED IN A PDMS
MICROFLUIDIC CHIP 54 3.3 MONODISPERSE THERMOSENSITIVE MICROGELS
FABRICATED IN A CAPILLARY MICROFLUIDIC DEVICE 57
3.4 MONODISPERSE THERMOSENSITIVE MICROGELS WITH TUNABLE VOLUME-PHASE
TRANSITION KINETICS 62 3.5 MONODISPERSE THERMOSENSITIVE MICROGELS WITH
CORE-SHELL STRUCTURES CONTAINING FUNCTIONAL MATERIALS 63 3.6
MONODISPERSE THERMOSENSITIVE MICROGELS WITH MULTIPHASE
COMPLEX STRUCTURES 65 3.7 CONCLUSIONS 68
REFERENCES 68
PART TWO PHYSICAL PROPERTIES OF MICROGEL PARTICLES 71
4 SWELLING THERMODYNAMICS OF MICROGEL PARTICLES 73 BENJAMIN
SIERRA-MARTIN,JUANJOSE LIETOR-SANTOS, ANTONIO FERNANDEZ-BARBERO, TOAN T.
NGUYEN, AND ALBERTO FERNANDEZ-NIEVES 4.1 INTRODUCTION 73
4.2 SWELLING THERMODYNAMICS 76 4.2.1 POLYMER/SOLVENT MIXING 76 4.1.1
RUBBER ELASTICITY 79 4.2.3 IONIC EFFECTS 81
4.2.3.1 IDEAL GAS CONTRIBUTION 81 4.2.3.2 ELECTROSTATIC ENERGY OF A
HOMOGENEOUSLY CHARGED MICROGEL 83 4.2.3.3 CONTRIBUTION FROM COUNTERION
CORRELATIONS 84 4.2.3.4 EFFECT OF A SLIGHTLY INHOMOGENEOUS FIXED-CHARGE
DISTRIBUTION 86 4.2.4 EQUILIBRIUM: EQUATION OF STATE 88 4.3 THEORY
VERSUS EXPERIMENT 94
4.3.1 ROLE OF FLORY SOLUBILITY PARAMETER 94
IMAGE 3
CONTENTS VII
4.3.2 INFLUENCE OF CROSS-LINKING DENSITY 97
4.3.3 EFFECT OF CHARGE DENSITY 98 4.3.4 SALT EFFECTS 100
4.3.5 EFFECT OF ADDED POLYMER 102 4.3.6 CONONSOLVENCY: SWELLING IN
SOLVENT MIXTURES 104 4.3.7 SURFACTANT EFFECTS 106 4.4 ADDITIONAL ASPECTS
108
4.4.1 ELASTIC MODULI 108
4A.I BRIEF REMARKS ON SWELLING KINETICS 108 4.5 SUMMARY 110
REFERENCES 113
5 DETERMINATION OF MICROGEL STRUCTURE BY SMALL-ANGLE NEUTRON SCATTERING
117 WALTER RICHTERING, INGO BERNDT, AND JAN SKOV PEDERSEN 5.1
INTRODUCTION 117
5.2 FORM FACTOR OF MICROGELS 118
5.3 CORE-SHELL PARTICLES 129
5.2 SUMMARY 131
REFERENCES 131
6 INTERACTIONS AND COLLOID STABILITY OF MICROGEL PARTICLES 133 BRIAN
VINCENT AND BRIAN SOUNDERS 6.1 THEORETICAL BACKGROUND 133 6.1.1
INTRODUCTION 133
6.1.2 VAN DER WAALS INTERACTIONS 136 6.1.3 ELECTROSTATIC INTERACTIONS
137 6.1.4 DEPLETION INTERACTIONS 139 6.1.5 CRITERIA FOR DISPERSION
STABILITY 140 6.2 EXPERIMENTAL STUDIES 141
6.2.1 TEMPERATURE- AND ELECTROLYTE-INDUCED AGGREGATION 141 6.2.2
DEPLETION-INDUCED AGGREGATION 151 6.2.3 HETEROAGGREGATION 153 6.2.4
PROBING INTERACTIONS BETWEEN MICROGEL PARTICLES 154
REFERENCES 160
PART THREE PHASE BEHAVIOR AND DYNAMICS OF MICROGEL SUSPENSIONS 163
7 STRUCTURE AND THERMODYNAMICS OF IONIC MICROGELS 165 CHRISTOS N. LIKOS
7.1 INTRODUCTION 165
7.2 EFFECTIVE INTERPARTICLE POTENTIALS 167 7.3 THE FLUID PHASE OF IONIC
MICROGELS 174 7.4 GENETIC ALGORITHMS FOR THE CRYSTAL STRUCTURES 178 7.5
PHASE BEHAVIOR 182
IMAGE 4
VIII CONTENTS
7.6 SUMMARY AND CONCLUDING REMARKS 189
REFERENCES 191
8 ELASTICITY OF SOFT PARTICLES AND COLLOIDS NEAR THE JAMMING THRESHOLD
195
MATTHIEU WYART
8.1 INTRODUCTION 195
8.2 STRUCTURE AND MECHANICAL STABILITY 196 8.3 ELASTIC MODULI 199
8.3.1 FORCE BALANCE AND CONTACT DEFORMATION OPERATORS 199 8.3.2 ENERGY
EXPANSION AND VIRTUAL FORCE FIELD 200 8.3.3 ELASTIC MODULI 202
8.4 SUMMARY AND CONCLUSION 204
REFERENCES 205
9 CRYSTALLIZATION OF MICROGEL SPHERES 207 ZHIBING HU 207 9.1
INTRODUCTION 207
9.2 SYNTHESIS AND CHARACTERIZATION OF PNIPAM MICROGELS 208 9.3 PHASE
BEHAVIOR OF DISPERSIONS OF PNIPAM MICROGELS AT ROOM TEMPERATURE 210
9.3.1 CHARACTERIZATION OF DIFFERENT PHASES USING UV-VISIBLE
SPECTROSCOPY 212
9.4 TEMPERATURE- AND POLYMER CONCENTRATION-DEPENDENT PHASES OF THE
PNIPAM MICROGEL DISPERSIONS 213 9.5 THEORETICAL INVESTIGATION OF PHASE
BEHAVIOR 215 9.6 PHASE DIAGRAM IN TERMS OF VOLUME FRACTION 217
9.7 THE INTERPARTIDE POTENTIAL 219
9.8 ANNEALING AND AGING EFFECTS 220 9.9 KINETICS OF CRYSTALLIZATION 222
9.10 CRYSTALLIZATION ALONG A SINGLE DIRECTION 224 9.11 SUMMARY AND
OUTLOOK 225
REFERENCES 226
10 MELTING AND GEOMETRIC FRUSTRATION IN TEMPERATURE-SENSITIVE COLLOIDS
229 AHMED M. ALSAYED, YILONG HAN, AND ARJUN C. YODH 10.1 INTRODUCTION
229
10.2 THE EXPERIMENTAL SYSTEM 232 10.2.1 SYNTHESIS OF NIPA MICROGEL
PARTICLES 232 10.2.2 MICROSCOPY AND TEMPERATURE CONTROL 235 10.2.3
CHARACTERIZATION: DYNAMIC LIGHT SCATTERING 238 10.2.4 CHARACTERIZATION:
VIDEO MICROSCOPY MEASUREMENT OF INTERPARTIDE
POTENTIALS 240
10.3 "FIRST" MELTING IN BULK (3D) COLLOIDAL CRYSTALS 242
IMAGE 5
CONTENTS IX
10.3.1 BACKGROUND 242
10.3.2 SAMPLE PREPARATION AND IMAGING 244 10.3.3 POSITIONAL FLUCTUATIONS
AND THE LINDEMANN PARAMETER 246 10.3.4 BULK MELTING 247 10.3.5 "FIRST"
MELTING NEAR GRAIN BOUNDARIES 248 10.3.6 "FIRST" MELTING NEAR
DISLOCATIONS 250 10.3.7 POSITIONAL AND ANGULAR FLUCTUATIONS NEAR DEFECTS
251 10.3.8 SUMMARY 253 10.4 MELTING IN TWO DIMENSIONS: THE HEXATIC PHASE
254 10.4.1 THEORETICAL BACKGROUND 254 10.4.2 EXPERIMENTAL BACKGROUND 257
10.4.3 2D SAMPLES 258 10.4.4 DATA ANALYSIS 259 10.4.5 THE HEXATIC PHASE
AND OTHER FEATURES OF THE PHASE DIAGRAM 264 10.4.6 THE ORDER OF THE
PHASE TRANSITIONS 265 10.4.7 SUMMARY 265
10.5 GEOMETRIC FRUSTRATION IN COLLOIDAL "ANTIFERROMAGNETS" 266 10.5.1
BACKGROUND 266 10.5.2 THE EXPERIMENTAL SYSTEM 269 10.5.3
ANTIFERROMAGNETIC ORDER 270 10.5.4 STRIPES AND THE ZIGZAGGING GROUND
STATE 270 10.5.5 DYNAMICS 271 10.5.6 SUMMARY 273 10.6 FUTURE 273
REFERENCES 274
PART FOUR MECHANICAL PROPERTIES 283
11 YIELDING, FLOW, AND SLIP IN MICROGEL SUSPENSIONS:
FROM MICROSTRUCTURE TO MACROSCOPIC RHEOLOGY 285 MICHEL CLOITRE 11.1
INTRODUCTION 285
11.2 ADVANCED TECHNIQUES FOR MICROGEL RHEOLOGY 286 11.2.1 MACROSCOPIC
SHEAR RHEOLOGY 286 11.2.2 DWS-BASED MICRORHEOLOGY 288 11.2.3 REAL SPACE
PARTICLE-TRACKING TECHNIQUES 290 11.3 NEAR-EQUILIBRIUM PROPERTIES AND
LINEAR RHEOLOGY OF MICROGEL
SUSPENSIONS 291
11.3.1 DILUTE REGIME AND PASTE FORMATION 291 11.3.2 LINEAR
VISCOELASTIDTY OF MICROGEL PASTES 293 11.3.3 ELASTIC PROPERTIES OF
CONCENTRATED MICROGEL PASTES 294 11.4 YIELDING, FLOW, AND AGING 297
11.4.1 YIELDING 297 11.4.2 FLOW OF MICROGEL PASTES 299 11.4.3 SLOW
DYNAMICS AND AGING OF MICROGEL PASTES 301
IMAGE 6
CONTENTS
11.5 SLIP AND FLOW OF MICROGEL SUSPENSIONS NEAR CONFINING SURFACES 303
11.5.1 WALL SLIP 303
11.5.2 DIRECT MEASUREMENTS OF SLIP VELOCITY 304 11.5.3
ELASTOHYDRODYNAMIC LUBRICATION AS THE ORIGIN OF WALL SLIP 306 11.6
OUTLOOK 307
REFERENCES 307
12 MECHANICS OF SINGLE MICROGEL PARTICLES 311 HANS M. WYSS, JOHAN
MATTSSON, THOMAS FRANKE, ALBERTO FERNANDEZ-NIEVES, AND DAVID A. WEITZ
12.1 COMPRESSIVE MEASUREMENTS BY VARIATION OF THE OSMOTIC PRESSURE 312
12.2 CAPILLARY MICROMECHANICS: FULL MECHANICAL BEHAVIOR OF A SINGLE
MICROGEL PARTICLE 315 12.3 DISCUSSION: EFFECTS OF PARTICLE SOFTNESS ON
SUSPENSION RHEOLOGY 322 12.4 MICROGELS AS MODEL GLASSES: SOFT PARTICLES
MAKE STRONG GLASSES 323
12.5 ANALOGY TO EMULSIONS AND FOAMS 324 REFERENCES 324
13 RHEOLOGY OF INDUSTRIALLY RELEVANT MICROGELS 327 JASON R. STOKES 13.1
INTRODUCTION 327
13.2 FLOW BEHAVIOR 328
13.2.1 INFLUENCE OF PHASE VOLUME AND CONCENTRATION 329 13.2.2 SHEAR
RHEOLOGY OF CONCENTRATED MICROGEL SUSPENSIONS 332 13.2.3 LINEAR
VISCOELASTICITY OF CONCENTRATED MICROGEL SUSPENSIONS 335 13.3 MICROGEL
SUSPENSION RHEOLOGY IN APPLICATIONS 338
13.3.1 COATING FORMULATIONS 339 13.3.2 BIOMEDICAL, PHARMACEUTICAL,
PERSONAL CARE, AND COSMETIC PRODUCTS 342 13.3.3 BIOPOLYMER MICROGELS FOR
FOOD AND OTHER APPLICATIONS 345 13.3.3.1 STARCH MICROGELS 345
13.3.3.2 BIOPOLYMER MICROGELS AND PARTICLE ANISOTROPY 347 13.4 OUTLOOK
350
REFERENCES 351
PART FIVE APPLICATIONS 355
14 EXPLOITING THE OPTICAL PROPERTIES OF MICROGELS AND HYDROGELS AS
MICROLENSES AND PHOTONIC CRYSTALS IN SENSING APPLICATIONS 357 L ANDREW
LYON, GRANT R. HENDRICKSON, ZHIYONG MENG, AND ASHLEE N. ST. JOHN IYER
14.1 INTRODUCTION 357
14.2 RESPONSIVE MICROGEL AND HYDROGEL-BASED LENSES 358 14.3 PHOTONIC
CRYSTALS 362
14.4 OTHER RESPONSIVE SYSTEMS 368
IMAGE 7
CONTENTS XI
14.5 SUMMARY 372
REFERENCES 372
15 MICROGELS IN DRUG DELIVERY 375 MARTIN MALMSTEN 15.1 INTRODUCTION 375
15.2 POLYMER GELS 376
15.3 POLYMER MICROGELS 378 15.3.1 TEMPERATURE TRIGGERING OF MICROGELS
380 15.3.2 ELECTROSTATIC TRIGGERING OF MICROGELS 382 15.3.3 TRIGGERING
OF MICROGELS BY SPECIFIC METABOLITES 385
15.3.4 MICROGEL TRIGGERING BY EXTERNAL FIELDS 385 15.3.5 MICROGEL
TRIGGERING BY DEGRADATION 389 15.4 POLYMER MICROCAPSULES 393 15.4.1
MICROCAPSULE TRIGGERING 395
15.5 SWELLING, LOADING, AND RELEASE KINETICS 399 15.6 OUTLOOK 402
REFERENCES 403
16 MICROGELS FOR OIL RECOVERY 407 YUXING BEN, IAN ROBB, PENG
TONMUKAYAKUL, AND QIANG WANG 16.1 INTRODUCTION 407
16.2 MICROGELS USED IN OIL RECOVERY 410 16.2.1 GUAR 410
16.2.1.1 GEL FORMATION 411 16.2.2 RHEOLOGY OF GUAR GELS AND ITS RELATION
TO PROPPANT TRANSPORT 415 16.2.2.1 PROPPANT TRANSPORT 416 16.2.3 XANTHAN
416
16.2.4 GELS FOR GRAVEL PACKING 418 16.2.5 GELS FOR FLUID LOSS CONTROL
419 16.2.6 GELS FOR PILLS 420
16.3 CONCLUDING REMARKS 421 REFERENCES 421
17 APPLICATIONS OF BIOPOLYMER MICROGELS 423 EUGENE PASHKOVSKI 17.1
INTRODUCTION 423
17.2 ORIGIN, PRODUCTION, AND MOLECULAR PROPERTIES OF XANTHAN GUM 425
17.3 CHARACTERIZATION OF XANTHAN AND CMC MICROGELS 429 17.4 RHEOLOGY OF
SILICA SUSPENSIONS IN XANTHAN MICROGEL PASTES 436 17.5 AGING OF
CONCENTRATED XANTHAN SUSPENSIONS 442 17.6 CONCLUSIONS 446
REFERENCES 447
INDEX 451 |
| any_adam_object | 1 |
| author2 | Fernandez-Nieves, Alberto |
| author2_role | edt |
| author2_variant | a f n afn |
| author_GND | (DE-588)143415298 |
| author_facet | Fernandez-Nieves, Alberto |
| building | Verbundindex |
| bvnumber | BV037239537 |
| classification_rvk | VE 8000 |
| ctrlnum | (OCoLC)707081284 (DE-599)DNB1005391319 |
| dewey-full | 541.34513 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 541 - Physical chemistry |
| dewey-raw | 541.34513 |
| dewey-search | 541.34513 |
| dewey-sort | 3541.34513 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
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| id | DE-604.BV037239537 |
| illustrated | Illustrated |
| indexdate | 2024-07-20T10:59:25Z |
| institution | BVB |
| isbn | 9783527321582 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-021153049 |
| oclc_num | 707081284 |
| open_access_boolean | |
| owner | DE-29T DE-11 DE-703 |
| owner_facet | DE-29T DE-11 DE-703 |
| physical | XXI, 461 S. Ill., graph. Darst. |
| publishDate | 2011 |
| publishDateSearch | 2011 |
| publishDateSort | 2011 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Microgel suspensions fundamentals and applications Ed. by Alberto Fernandez-Nieves ... Weinheim Wiley-VCH 2011 XXI, 461 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Suspension (DE-588)4058671-6 gnd rswk-swf Kolloidchemie (DE-588)4134420-0 gnd rswk-swf Mikrogel (DE-588)4169820-4 gnd rswk-swf Mikrogel (DE-588)4169820-4 s Suspension (DE-588)4058671-6 s DE-604 Kolloidchemie (DE-588)4134420-0 s 1\p DE-604 Fernandez-Nieves, Alberto (DE-588)143415298 edt X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=3520440&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=021153049&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Microgel suspensions fundamentals and applications Suspension (DE-588)4058671-6 gnd Kolloidchemie (DE-588)4134420-0 gnd Mikrogel (DE-588)4169820-4 gnd |
| subject_GND | (DE-588)4058671-6 (DE-588)4134420-0 (DE-588)4169820-4 |
| title | Microgel suspensions fundamentals and applications |
| title_auth | Microgel suspensions fundamentals and applications |
| title_exact_search | Microgel suspensions fundamentals and applications |
| title_full | Microgel suspensions fundamentals and applications Ed. by Alberto Fernandez-Nieves ... |
| title_fullStr | Microgel suspensions fundamentals and applications Ed. by Alberto Fernandez-Nieves ... |
| title_full_unstemmed | Microgel suspensions fundamentals and applications Ed. by Alberto Fernandez-Nieves ... |
| title_short | Microgel suspensions |
| title_sort | microgel suspensions fundamentals and applications |
| title_sub | fundamentals and applications |
| topic | Suspension (DE-588)4058671-6 gnd Kolloidchemie (DE-588)4134420-0 gnd Mikrogel (DE-588)4169820-4 gnd |
| topic_facet | Suspension Kolloidchemie Mikrogel |
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