Industrial scale natural products extraction:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH
2011
|
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | XVII, 296 S. Ill., graph. Darst. |
| ISBN: | 9783527325047 |
Internformat
MARC
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IMAGE 1
CONTENTS
PREFACE XIII LIST OF CONTRIBUTORS XV
1 EXTRACTION OF NATURAL PRODUCTS FROM PLANTS-AN INTRODUCTION 1 HANS-JOERG
BART 1.1 INTRODUCTION 1
1.2 CULTIVATION 6
1.3 EXTRACTION 8
1.3.1 SOLVENTS 8 1.4 EXTRACTION TECHNIQUES 15 1.5 PURIFICATION 37
1.5.1 CHROMATOGRAPHY 17 1.5.1.1 ADSORPTION CHROMATOGRAPHY 17 1.5.1.2
PARTITION CHROMATOGRAPHY 18 1.5.1.3 ION EXCHANGE CHROMATOGRAPHY 18
1.5.1.4 GEL CHROMATOGRAPHY 19 1.5.1.5 (BIO-) AFFINITY CHROMATOGRAPHY 19
1.5.2 CONTINUOUS TECHNIQUES 19 1.5.2.1 TRUE MOVING BED (TMB)
CHROMATOGRAPHY 20 1.5.2.2 SIMULATED MOVING BED (SMB) CHROMATOGRAPHY 20
1.5.2.3 ANNULAR CHROMATOGRAPHY 22 1.5.2.4 CARROUSEL ADSORBERS 22
REFERENCES 24
2 SOLUBILITY OF COMPLEX NATURAL AND PHARMACEUTICAL SUBSTANCES 27 FEELLY
RUETHER AND GABRIELE SADOWSKI 2.1 INTRODUCTION 27
2.2 SOLUBILITY CALCULATIONS 27 2.2.1 SOLUBILITY OF A PURE SOLUTE IN
SOLVENTS AND SOLVENT MIXTURES 27 2.2.2 PH-DEPENDENCE OF SOLUBILITY 29
2.2.3 SOLUBILITY OF RACEMIC COMPOUNDS 29 2.3 THERMODYNAMIC MODELING 30
BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/1008658766
DIGITALISIERT DURCH
IMAGE 2
VI CONTENTS
2.3.1 PC-SAFT EQUATION OF STATE 30
2.3.1.1 HARD-CHAIN CONTRIBUTION A HC 30 2.3.1.2 DISPERSION CONTRIBUTION
A^ 31 2.3.1.3 ASSOCIATION CONTRIBUTION A ASSOC 31 2.3.2 ESTIMATION OF
PC-SAFT PARAMETERS 33
2.4 EXAMPLES 35
2.4.1 SOLUBILITY OF ESTRIOL, ESTRONE, AND SITOSTEROL IN DIFFERENT
SOLVENTS 35 2.4.2 SOLUBILITY OF BETA-CAROTENE IN SUPERCRITICAL CARBON
DIOXIDE 37 2.4.3 SOLUBILITY OF PARACETAMOL IN PURE SOLVENTS AND SOLVENT
MIXTURES 40 2.4.4 SOLUBILITY OF DL-METHIONINE AS FUNCTION OF PH 44 2.4.5
SOLUBILITY OF MANDELIC ACID ENANTIOMERS AND RACEMIC
MANDELIC ACID IN WATER 45 2.5 SUMMARY 49
SYMBOLS 49 LATIN SYMBOLS 49 GREEK SYMBOLS AND SPECIAL CHARACTERS 50
SUPERSCRIPTS 50
SUBSCRIPTS 50 APPENDIX 51 HARD-CHAIN REFERENCE CONTRIBUTION 51
DISPERSION CONTRIBUTION 52
ASSOCIATION CONTRIBUTION 53 REFERENCES 53
3 ALTERNATIVE SOLVENTS IN PLANT EXTRACTION 55 VOLKMAR JORDAN AND ULRICH
MUELLER 3.1 INTRODUCTION 55
3.2 IONIC LIQUIDS IN THE EXTRACTION OF NATURAL COMPOUNDS FROM PLANT AND
FUNGI 56 3.2.1 CHARACTERISTICS OF IONIC LIQUIDS 57 3.2.1.1
PHYSICOCHEMICAL PROPERTIES 57 3.2.1.2 ENVIRONMENTAL AND SAFETY ASPECTS
60 3.2.2 APPLICATION OF IONIC LIQUIDS IN PLANT EXTRACTION 61 3.2.2.1
APPLICATION OF ILS IN EXTRACTION 61 3.2.2.2 REMOVAL OF TARGET SUBSTANCE
FROM EXTRACT AND SEPARATION OF SOLVENT
FROM SPENT BIOMASS 61 3.2.2.3 EXAMPLE 1: EXTRACTION OF ARTEMISININ 62
3.2.2.4 EXAMPLE 2: EXTRACTION OF LIGNIN 64 3.3 SURFACTANTS AND AQUEOUS
TWO-PHASE SYSTEMS IN PLANT EXTRACTION 65 3.3.1 CHARACTERISTICS OF
SURFACTANT-WATER MIXTURES 67 3.3.2 BEHAVIOR OF NONIONIC SURFACTANTS IN
AQUEOUS SOLUTION 71 3.3.3 MICELLAR EXTRACTION AND CLOUD POINT EXTRACTION
73 3.3.4 REVERSED MICELLAR EXTRACTION 74 3.3.5 EQUILIBRIUM PARTITION OF
TARGET SUBSTANCES IN AQUEOUS SURFACTANT
SOLUTIONS 75
IMAGE 3
CONTENTS VII
3.3.6 EXAMPLES FOR THE USE OF SURFACTANTS IN PLANT EXTRACTION 77
3.3.6.1 PLANT EXTRACTION USING MICELLAR AND CLOUD POINT EXTRACTION 77
3.3.6.2 PLANT EXTRACTION USING REVERSE MICELLES 80 3.4 SUMMARY 83
REFERENCES 84
4 HIGH PRESSURE PROCESSING 87 RUDOLF EGGERS AND STEPHAN PILZ 4.1
INTRODUCTION 87
4.2 SUPERCRITICAL FLUIDS 90 4.2.1 GENERAL 91 4.2.2 PHYSICAL PROPERTIES
93 4.2.3 SOLVENT POWER AND SOLUBILITY 94 4.3 PHYSICAL PROPERTIES-MASS
TRANSFER CHARACTERISTICS 95 4.4 PROCESS UNITS 99
4.4.1 PRE-TREATMENT 99 4.4.1.1 MECHANICAL PRE-TREATMENT 100 4.4.1.2
THERMAL AND HYDROTHERMAL TREATMENT 103 4.4.1.3 INNOVATIVE METHODS 104
4.4.2 EXTRACTION 104 4.4.3 SEPARATION 106 4.4.4 POST-TREATMENT 107
4.4.4.1 DEGASSING 107 4.4.4.2 FURTHER SEPARATION 107 4.4.4.3
STABILIZATION 107 4.4.4.4 FORMULATION 108 4.5 PROCESS DESIGN AND
OPERATION 108 4.5.1 PROCESS CONCEPT 108 4.5.2 PRESSURIZATION AND
DEPRESSURIZATION 109 4.5.3 CO 2 RECYCLE LOOP 110 4.5 A SCALE-UP 111
4.5.5 COSTS 113 4.6 APPLICATIONS 113
ACKNOWLEDGMENTS 120 REFERENCES 120
5 PROCESS ENGINEERING AND MINI-PLANT TECHNOLOGY 123 JOCHEN STRUBE,
WERNER BAECKER AND MICHAEL SCHULTE 5.1 INTRODUCTION 123
5.2 CHROMATOGRAPHIE SCREENING 132 5.3 PREPARATIVE TASK 134 5.3.1 CRUDE
MIXTURE PRE-TREATMENT 137 5.3.2 FINAL PURIFICATION OF THE END PRODUCT
139 5.3.2.1 BATCH CHROMATOGRAPHY 140 5.3.2.2 ANNULAR CHROMATOGRAPHY 140
IMAGE 4
VIII CONTENTS
5.3.2.3 STEADY-STATE RECYCLING CHROMATOGRAPHY 141
5.3.2.4 SIMULATED MOVING BED (SMB) CHROMATOGRAPHY 142 5.4 LIQUID-LIQUID
EXTRACTION 143 5.4.1 INTRODUCTION 143 5.4.2 CHOICE OF EXTRACTING AGENT
144
5.4.2.1 SELECTION CRITERIA 145 5.4.3 DATA OF CHEMICAL AND PHYSICAL
PROPERTIES 146 5.4.4 SPECIFICATION OF SEPARATION SEQUENCE 147 5.4.5
OPERATION CONCEPTS IN EXTRACTION 148
5.4.6 DETERMINATION OF EQUIPMENT EFFORTS 151 5.5 MINI-PLANT TECHNOLOGY
FOR EXTRACTION PROCESS DEVELOPMENT 155 5.6 COST ESTIMATION 159 5.7 TOTAL
PROCESS DEVELOPMENT 160 5.7.1 MINI-PLANT TECHNOLOGY 360
5.7.2 EXAMPLES OF TYPICAL PROCESSES 164 5.7.2.1 QUASSIA EXTRACTS 164
5.7.2.2 SPRUCE BARK EXTRACTS 165 5.7.2.3 PEPPER EXTRACTS 167 5.7.2.4
VANILLA EXTRACTS 167
5.7.2.5 TAXOL EXTRACTS 168 5.7.3 PROCESS MODELING AND SCALE-UP 171 5.8
FUTURE DEVELOPMENTS 175 ACKNOWLEDGMENTS 175
REFERENCES 176
6 EXTRACTION TECHNOLOGY 181 ANDREAS PFENNIG, DIRK DELINSKI, WILHELM
JOHANNISBAUER AND HORST JOSTEN 6.1 INTRODUCTION 181
6.2 EXTRACTION PROCESS BASICS 181 6.2.1 INTRODUCTION 181 6.2.2
EXTRACTION TECHNIQUES 183 6.2.2.1 SOLID-LIQUID EXTRACTION 183
6.2.2.2 PROCESS ALTERNATIVES 185 6.2.2.3 CONTINUOUS OR DISCONTINUOUS
EXTRACTION 186 6.2.3 FURTHER CONSIDERATIONS 186 6.3 EXPERIMENTAL
PROCEDURES 187
6.3.1 EXTRACTION CURVES 187 6.3.2 DETERMINATION OF EQUILIBRIUM AND
KINETICS 187 6.3.3 STANDARD LABORATORY EXPERIMENT 190 6.3.4 EXAMPLE
EXTRACTION OF PEPPER 191 6.3.4.1 CALIBRATION WITH PURE COMPONENT 191
6.3.4.2 PRE-TREATMENT OF SOLID RAW MATERIAL 191 6.3.4.3 EXTRACTION
KINETICS 192
6.4 THEORETICAL MODELING AND SCALE-UP 193
IMAGE 5
CONTENTS IX
6.4.1 MACRO-MODEL 194
6.4.1.1 IDEAL STIRRED TANK 194 6.4.1.2 IDEAL PLUG-FLOW EXTRACTOR 195
6.4.1.3 OTHER MACRO-MODELS 195 6.4.2 MICRO-MODELS 196 6.4.2.1 OTHER
MICRO-MODELS 197 6.4.3 FITTING TO EXPERIMENTAL DATA AND MODEL-BASED
EXPERIMENTAL DESIGN 199 6.4.4 SCALE-UP DESIGN 199 6.5 INDUSTRIAL
EXTRACTION EQUIPMENT 200 6.5.1 PRE-PROCESSING OF PLANT MATERIAL 200
6.5.2 SELECTION OF EXTRACTION SOLVENTS 201 6.5.3 SOLID-LIQUID EXTRACTION
PROCESSES 202 6.5.3.1 BATCH PROCESSES 202 6.5.3.2 CONTINUOUS PROCESSES
204
6.5.4 EXTRACTOR DESIGN 205 6.5.4.1 BATCH EQUIPMENT 206 6.5.4.2
CONTINUOUS EXTRACTORS 208 6.5.5 FUTURE DEVELOPMENTS 212
6.5.6 EXTRACT TREATMENT 235 6.5.7 DEPLETED PLANT TREATMENT 236 SYMBOLS
217 LATIN SYMBOLS 217
GREEK SYMBOLS AND SPECIAL CHARACTERS 218 SUBSCRIPTS 218 REFERENCES 218
7 EXTRACTION OF LIGNOCELLULOSE AND ALGAE FOR THE PRODUCTION OF BULK AND
FINE CHEMICALS 221 THOMAS HAHN, SVENJA KELLY, KAI MUFFER, NILS
TIPPKOETTER AND ROLAND ULBER
7.1 INTRODUCTION 221
7.2 PRODUCTS FROM LIGNOCELLULOSE 222 7.2.1 CELLULOSE FRACTION 222 7.2.2
HEMICELLULOSE FRACTION 224 7.2.3 EXTRACTION OF FERMENTATION INHIBITORS
225
7.2.4 LIGNIN FRACTION 226 7.2.5 CONTINUOUS EXTRACTION OF LIGNOCELLULOSE
227 7.3 POLYSACCHARIDES AND SPOROPOLLENIN FROM MARINE ALGAE 227 7.3.1
AGAR 227
7.3.2 CARRAGEENAN 230 7.3.3 ALGINIC ACID 232 7.3.4 FUCOIDAN 235 7.3.5
SPOROPOLLENIN/ALGAENAN 238
REFERENCES 242
IMAGE 6
X CONTENTS
8 NATURAL PRODUCTS-MARKET DEVELOPMENT AND POTENTIALS 247
SYBILLE BUCHWALD-WERNER AND FRIEDRICH BISCHOFF 8.1 INTRODUCTION 247
8.2 NATURAL PRODUCT MARKET OVERVIEW 247 8.2.1 MARKET FOR EXTRACTS 248
8.3 NATURAL PRODUCTS IN FOOD AND FUNCTIONAL FOOD 249 8.3.1 FUNCTIONAL
FOOD CONCEPT BASED ON NATURAL PRODUCTS 249 8.3.2 NATURAL PRODUCT
DEVELOPMENT 250 8.3.3 FOOD APPLICATIONS OF NATURAL PRODUCTS 252
8.3.4 SUCCESS STORY PLANT STEROLS FOR HEART HEALTH 256 8.3.5 BAOBAB-THE
NEW SUPERFRUIT 257 8.4 NATURAL PRODUCTS FOR PHARMACEUTICAL APPLICATIONS
259 8.4.1 EXISTING PRODUCTS AND INNOVATION 259 8.4.2 TERPENES: PADITAXEL
(TAXOL) -THE POSTERCHILD 262 8.4.3 ALKALOIDS: A GROUP OF POTENT APIS 263
8.4.3.1 CAMPTOTHECIN-DERIVED APIS 263 8.4.3.2 OMACETAXINE
(HOMOHARRINGTONINE) 264 8.4.3.3 OPIATE ALKALOIDS 264 8.5 SUMMARY 266
REFERENCES 267
9 REGULATIONS AND REQUIREMENTS 269 CUIDO RITTER AND ALWINE KRAATZ 9.1
INTRODUCTION 269
9.2 DEFINITION OF PLANT EXTRACTS AS MEDICINES OR FOODS- A BORDERLINE
ISSUE 270 9.2.1 MEDICINES 270 9.2.2 FOODS 271 9.3 APPLICATION OF PLANT
EXTRACTS IN FLAVORINGS, FUNCTIONAL FOODS,
NOVEL FOODS AND FOOD SUPPLEMENTS 272 9.3.1 FLAVORINGS 272 9.3.2
FUNCTIONAL FOODS 273 9.3.3 REGULATION ON NUTRITION AND HEALTH CLAIMS
MADE ON FOODS 273 9.3.3.1 NUTRITION CLAIM 275 9.3.3.2 HEALTH CLAIM 275
9.3.3.3 REDUCTION OF DISEASE RISK CLAIM 276
9.3.4 REGULATION CONCERNING NOVEL FOODS AND NOVEL FOOD INGREDIENTS 276
9.3.5 REGULATION CONCERNING FOOD SUPPLEMENTS 277 9.3.6 THE HEALTH
BENEFITS OF FOOD PRODUCTS CONTAINING PLANT EXTRACTS 278 9.3.6.1 MODE OF
FUNCTION PLANT EXTRACTS AS ANTIOXIDANTS 278 9.3.7 EXAMPLES OF
APPLICATIONS OF PLANT EXTRACTS IN FUNCTIONAL FOODS AND
DIETARY SUPPLEMENTS 278 9.3.7.1 BLACK AND GREEN TEA 279 9.3.7.2 GINGKO
BILOBA 280 9.3.7.3 SOY PROTEIN 280
IMAGE 7
CONTENTS XI
9.4 REQUIREMENTS CONCERNING QUALITY AND SAFETY ISSUES 281
9.4.1 TECHNICAL DATA 283 9.4.1.1 IDENTITY AND NATURE OF THE SOURCE
MATERIAL 283 9.4.1.2 MANUFACTURING PROCESS 284 9.4.1.3 CHEMICAL
COMPOSITION 284 9.4.1.4 SPECIFICATIONS 284 9.4.1.5 STABILITY OF THE
BOTANICAL OR BOTANICAL PREPARATION USED AS INGREDIENT IN
FOOD SUPPLEMENT 284 9.4.1.6 PROPOSED USES AND USE LEVELS 284 9.4.1.7
INFORMATION ON EXISTING ASSESSMENTS 285 9.4.2 ADDITIONALLY DATA ON
EXPOSURE AND TOXICOLOGICAL EXPOSURE:
EXTENT AND TIME 285 9.4.3 TOXICOLOGICAL DATA 285 9.5 CONCLUSIONS 286
REFERENCES 286
INDEX 293 |
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| language | English |
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| spelling | Industrial scale natural products extraction ed. by Hans-Jörg Bart ... Weinheim Wiley-VCH 2011 XVII, 296 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Destraktion (DE-588)4124778-4 gnd rswk-swf Naturstoff (DE-588)4041418-8 gnd rswk-swf Naturstoff (DE-588)4041418-8 s Destraktion (DE-588)4124778-4 s DE-604 Bart, Hans-Jörg Sonstige oth X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=3620655&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020887502&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Industrial scale natural products extraction Destraktion (DE-588)4124778-4 gnd Naturstoff (DE-588)4041418-8 gnd |
| subject_GND | (DE-588)4124778-4 (DE-588)4041418-8 |
| title | Industrial scale natural products extraction |
| title_auth | Industrial scale natural products extraction |
| title_exact_search | Industrial scale natural products extraction |
| title_full | Industrial scale natural products extraction ed. by Hans-Jörg Bart ... |
| title_fullStr | Industrial scale natural products extraction ed. by Hans-Jörg Bart ... |
| title_full_unstemmed | Industrial scale natural products extraction ed. by Hans-Jörg Bart ... |
| title_short | Industrial scale natural products extraction |
| title_sort | industrial scale natural products extraction |
| topic | Destraktion (DE-588)4124778-4 gnd Naturstoff (DE-588)4041418-8 gnd |
| topic_facet | Destraktion Naturstoff |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=3620655&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020887502&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT barthansjorg industrialscalenaturalproductsextraction |