Synthesis and characterization of nitrile ligated transition metal complexes bearing WCAs as catalysts for the homopolymerization of isobutylene:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
München
Verl. Dr. Hut
2010
|
| Ausgabe: | 1. Aufl. |
| Schriftenreihe: | Anorganische Chemie
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | 160 S. Ill., graph. Darst. 210 mm x 148 mm, 286 g |
| ISBN: | 9783868536638 |
Internformat
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| 100 | 1 | |a Diebl, Bernd Eduard |d 1981- |e Verfasser |0 (DE-588)143151932 |4 aut | |
| 245 | 1 | 0 | |a Synthesis and characterization of nitrile ligated transition metal complexes bearing WCAs as catalysts for the homopolymerization of isobutylene |c Bernd E. Diebl |
| 250 | |a 1. Aufl. | ||
| 264 | 1 | |a München |b Verl. Dr. Hut |c 2010 | |
| 300 | |a 160 S. |b Ill., graph. Darst. |c 210 mm x 148 mm, 286 g | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
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| 490 | 0 | |a Anorganische Chemie | |
| 502 | |a Zugl.: München, Techn. Univ., Diss., 2010 | ||
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Datensatz im Suchindex
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|---|---|
| adam_text | IMAGE 1
INDEX
INDEX
CHAPTER I: INTRODUCTION 1
1. CATEGORISATION OF POLYISOBUTYLENES AND THEIR COMMERCIAL APPLICATIONS
1
1.2 METHODS FOR ISOBUTYLENE POLYMERIZATION 2
1.2.1 CARBOCATIONIC POLYMERIZATION OF ISOBUTYLENE 2
1.2.2 NITRILE LIGATED TRANSITION METAL COMPLEXES BEARING WCAS FOR
ISOBUTYLENE
POLYMERIZATION 5
2. SYNTHESIS AND CHARACTERIZATION OF NITRILE LIGATED TRANSITION METAL
COMPLEXES
BEARING WCAS 8
2.1 CANDIDATES - AN OVERVIEW 8
2.2 SYNTHETIC STRATEGIES FOR INTRODUCING WCAS TO NITRILE LIGATED
TRANSITION METAL
COMPLEXES 12
2.3 VIBRATIONAL SPECTROSCOPIC PROPERTIES OF ACETONITRILE LIGATED
TRANSITION METAL
COMPLEXES IN COMPARISON TO STRUCTURAL CHARACTERIZATION BY X-RAY
STRUCTURE
ANALYSIS 14
2.3.1 SPECIFIC VIBRATIONAL SPECTROSCOPIC PROPERTIES OF ACETONITRILE
LIGATED TRANSITION
METAL COMPLEXES 14
2.3.2 OCTAHEDRAL ACETONITRILE LIGATED TRANSITION METAL COMPLEXES 14
2.3.3 TETRAHEDRAL ACETONITRILE LIGATED TRANSITION METAL COMPLEXES 19
2.3.4 SQUARE-PLANAR ACETONITRILE LIGATED TRANSITION METAL COMPLEXES 23
2.3.5 EXCURSUS: DISCUSSION ABOUT VIBRATIONAL SPECTRA OF MECN AND D
3-MECN 26
3. OBJECTIVES OF THIS WORK 28
4. REFERENCES 29
CHAPTER II: SYNTHESIS OF MOLYBDENUM(LTI) COMPLEXES BEARING WEAKLY
COORDINATING
ANIONS AND THEIR APPLICATION AS CATALYSTS OF ISOBUTYLENE POLYMERIZATION
35
1. BACKGROUND 37
2. RESULTS AND DISCUSSION 38
2.1 SYNTHESIS AND CHARACTERIZATION OF MOLYBDENUM(IN) COMPLEXES 38
2.2 HOMOPOLYMERIZATION OF ISOBUTYLENE 41
2.2.1 INFLUENCE OF CATALYST CONCENTRATION 41
2.2.2 CONVERSION OF ISOBUTYLENE WITH MOLYBDENUM(IH) CATALYSTS 1-3 44
BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/1008935565
DIGITALISIERT DURCH
IMAGE 2
INDEX
2.2.3 INFLUENCE OF PROTON TRAPS 48
2.2.4 POLYMERIZATION IN NON-POLAR SOLVENTS 49
2.2.5 ONLINE MONITORING OF ISOBUTYLENE POLYMERIZATION B Y H - N MR 52
3. CONCLUSIONS 53
4. EXPERIMENTAL 54
4.1 MEASUREMENTS AND PREPARATIONS 54
4.2 GENERAL PROCEDURES FOR THE SYNTHESIS OF COMPOUNDS 1-3 55
4.3 TUBE POLYMERIZATION 57
5. REFERENCES 57
CHAPTER HI: SYNTHESIS AND CHARACTERIZATION OF THE MOLYBDENUM(TV)
COMPLEXES
[MOO(MECN) 4(AX-MECN)][B(C6FS)4]2 AND [MOO(PHCN)4][B(C6F5)4]2 AS
CATALYSTS FOR
THE HOMOPOLJ MERIZATION OF ISOBUTYLENE 61
1. INTRODUCTION 63
2. RESULTS AND DISCUSSION 64
2.1 SYNTHESIS OF COMPOUNDS [MOO(MECN) 4(*C-MECN)][B(C6F5)4]2 (4) AND
[MOO(PHCN) 4][B(C6F5)4]2(5) 64
2.2 CHARACTERIZATION OF COMPOUNDS [MOO(MECN) 4(*C-MECN)] [B(C6F5)4]2 (4)
AND
[MOO(PHCN)4][B(C6F 5)4]2 (5) 65
2.2.1 VIBRATIONAL SPECTROSCOPY 65
2.2.2 9SMO-NMR SPECTROSCOPY 67
2.2.3 THERMOGRAVIMETIC ANALYSIS 67
2.2.4 X-RAY STRUCTURE ANALYSIS 68
3. APPLICATION OF COMPOUND 4 AND 5 FOR THE POLYMERIZATION OF ISOBUTENE
70
4. CONCLUSIONS 70
5. EXPERIMENTAL 71
5.1 MEASUREMENTS AND PREPARATIONS 71
5.2 PREPARATION OF THE CATALYSTS 71
5.3 SINGLE-CRYSTAL X-RAY STRUCTURE DETERMINATION OF COMPOUND 4 73
5.4 POLYMERIZATION REACTIONS 73
6. REFERENCE 74
CHAPTER IV: SYNTHESIS AND CHARACTERIZATION OF BENZONITRILE LIGATED
TRANSITION METAL
COMPLEXES [M(PHCN) 6][B(C6F5)4]2 (M= MN-CO) AND [M(PHCN)5][B(C6F5)4]2
(M= NI-ZN)
AS CATALYSTS FOR THE HOMOPOLY MERIZATION OF ISOBUTYLENE 77
IMAGE 3
INDEX
1. BACKGROUND 79
2. RESULTS AND DISCUSSION 80
2.1 SYNTHESIS OF COMPOUNDS [M(PHCN) 6] [B(C6F5)4]2 (M= MN (6), FE (7),
CO (8)) AND
[M(PHCN) 5][B(C6F5)4]2 (M= NI (9), ZN (10), CU(LL)) 80
2.2 SPECTROSCOPIC ANALYSIS 80
2.3 THERMOGRAVIMETRIC ANALYSIS 82
2.4 X-RAY STRUCTURE ANALYSIS OF [CU(PHCN) 5] [B(C6FS)4]2 (11) 83
3. HOMOPOLYMERIZATION OF ISOBUTYLENE CATALYSTS 6-11 84
4. CONCLUSIONS 86
5. OUTLOOK 88
6. EXPERIMENTAL 89
6.1 MEASUREMENTS AND PREPARATIONS 89
6.2 GENERAL SYNTHESIS OF COMPOUNDS [M(PHCN)6][B(C 6F5)4]2 (M= MN (6), FE
(7),
CO (8)) AND [M(PHCN)5][B(C 6F5)4]2 (M= NI (9), ZN (10)) 90
7. REFERENCES 92
CHAPTER V: SYNTHESIS OF ACETONITRILE LIGATED COPPER COMPLEXES WITH
PERFLUOROALKOXY
ALUMINATE AS ANION AND THEIR CATALYTIC APPLICATION FOR OLEFIN
AZIRIDINATION 95
1. BACKGROUND 97
2. RESULTS AND DISCUSSION 98
2.1 SYNTHESIS AND SPECTROSCOPIC CHARACTERIZATION OF COMPOUNDS
[CU(MECN) 4][AL{OC(CF3)3}4] (12) AND [CU(MECN)6][AL{OC(CF3)3}4]2(13) 98
2.2 CATALYTIC AZIRIDINATION OF OLEFINS 99
3. CONCLUSIONS 102
4. EXPERIMENTAL 103
4.1 MEASUREMENTS AND PREPARATIONS 103
4.2 SYNTHESIS OF COMPOUNDS [CU(MECN) 4][AL{OC(CF3)3}4] (12) AND
[CU(MECN) 6][AL{OC(CF3)3}4]2 (13) 103
4.3 GENERAL PROCEDURE FOR THE OLEFIN AZIRIDINATION REACTION 104
5. REFERENCES 105
CHAPTER VI: SYNTHESIS OF MCM-41 SUPPORTED DIOXOMOLYBDENUM(VI) COMPLEXES
BEARING ETHOXYCARBONYL BIPYRIDINE LIGANDS AND THEIR CATALYTIC PROPERTIES
IN THE
EPOXIDATION OF 1-OCTENE 107
1. INTRODUCTION 109
IMAGE 4
INDEX
2. RESULTS AND DISCUSSIONS 110
2.1 SYNTHESIS AND CHARACTERIZATION OF THE HOMOGENEOUS CATALYSTS 14A-18A
110
2.2 SYNTHESIS AND CHARACTERIZATION OF THE HETEROGENEOUS CATALYSTS
14B-18B 111
2.3 CATALYTIC RESULTS OF CATALYSTS 14A-18A AND 14B-18B FOR THE
EPOXIDATION OR
1-OCTENE 114
2.4 NMR-STUDIES OF CATALYSTS 14A AND 14B 117
3. CONCLUSIONS 118
4. EXPERIMENTAL 119
4.1 MEASUREMENTS AND PREPARATION 119
4.2 SYNTHESIS OF THE HOMOGENEOUS COMPLEXES 14A-18A 120
4.3 IMMOBILIZATION OF THE HOMOGENEOUS COMPLEXES 14A-18A ONTO MCM-41 121
4.4 CATALYTIC OXIDATION REACTIONS 122
5. REFERENCES 122
CHAPTER V U: SUMMARY 125
CHAPTER VIII: ZUSAMMENFASSUNG 135
CHAPTER IX: APPENDIX 145
|
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| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Chemie |
| edition | 1. Aufl. |
| format | Thesis Book |
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| id | DE-604.BV036882668 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T22:50:06Z |
| institution | BVB |
| isbn | 9783868536638 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-020798010 |
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| physical | 160 S. Ill., graph. Darst. 210 mm x 148 mm, 286 g |
| publishDate | 2010 |
| publishDateSearch | 2010 |
| publishDateSort | 2010 |
| publisher | Verl. Dr. Hut |
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| series2 | Anorganische Chemie |
| spelling | Diebl, Bernd Eduard 1981- Verfasser (DE-588)143151932 aut Synthesis and characterization of nitrile ligated transition metal complexes bearing WCAs as catalysts for the homopolymerization of isobutylene Bernd E. Diebl 1. Aufl. München Verl. Dr. Hut 2010 160 S. Ill., graph. Darst. 210 mm x 148 mm, 286 g txt rdacontent n rdamedia nc rdacarrier Anorganische Chemie Zugl.: München, Techn. Univ., Diss., 2010 Übergangsmetallkomplexe (DE-588)4131837-7 gnd rswk-swf Katalysator (DE-588)4029919-3 gnd rswk-swf Polymerisation (DE-588)4046704-1 gnd rswk-swf Isobuten (DE-588)4162474-9 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Übergangsmetallkomplexe (DE-588)4131837-7 s Katalysator (DE-588)4029919-3 s Polymerisation (DE-588)4046704-1 s Isobuten (DE-588)4162474-9 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020798010&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Diebl, Bernd Eduard 1981- Synthesis and characterization of nitrile ligated transition metal complexes bearing WCAs as catalysts for the homopolymerization of isobutylene Übergangsmetallkomplexe (DE-588)4131837-7 gnd Katalysator (DE-588)4029919-3 gnd Polymerisation (DE-588)4046704-1 gnd Isobuten (DE-588)4162474-9 gnd |
| subject_GND | (DE-588)4131837-7 (DE-588)4029919-3 (DE-588)4046704-1 (DE-588)4162474-9 (DE-588)4113937-9 |
| title | Synthesis and characterization of nitrile ligated transition metal complexes bearing WCAs as catalysts for the homopolymerization of isobutylene |
| title_auth | Synthesis and characterization of nitrile ligated transition metal complexes bearing WCAs as catalysts for the homopolymerization of isobutylene |
| title_exact_search | Synthesis and characterization of nitrile ligated transition metal complexes bearing WCAs as catalysts for the homopolymerization of isobutylene |
| title_full | Synthesis and characterization of nitrile ligated transition metal complexes bearing WCAs as catalysts for the homopolymerization of isobutylene Bernd E. Diebl |
| title_fullStr | Synthesis and characterization of nitrile ligated transition metal complexes bearing WCAs as catalysts for the homopolymerization of isobutylene Bernd E. Diebl |
| title_full_unstemmed | Synthesis and characterization of nitrile ligated transition metal complexes bearing WCAs as catalysts for the homopolymerization of isobutylene Bernd E. Diebl |
| title_short | Synthesis and characterization of nitrile ligated transition metal complexes bearing WCAs as catalysts for the homopolymerization of isobutylene |
| title_sort | synthesis and characterization of nitrile ligated transition metal complexes bearing wcas as catalysts for the homopolymerization of isobutylene |
| topic | Übergangsmetallkomplexe (DE-588)4131837-7 gnd Katalysator (DE-588)4029919-3 gnd Polymerisation (DE-588)4046704-1 gnd Isobuten (DE-588)4162474-9 gnd |
| topic_facet | Übergangsmetallkomplexe Katalysator Polymerisation Isobuten Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020798010&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT dieblberndeduard synthesisandcharacterizationofnitrileligatedtransitionmetalcomplexesbearingwcasascatalystsforthehomopolymerizationofisobutylene |