Immobilization of Rh-diphosphine complexes on mesostructured materials and their application to asymmetric hydrogenation and hydroboration:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Aachen
Shaker
2009
|
| Schriftenreihe: | Berichte aus der Chemie
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | IV, 152 S. graph. Darst. |
| ISBN: | 9783832287580 |
Internformat
MARC
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| 245 | 1 | 0 | |a Immobilization of Rh-diphosphine complexes on mesostructured materials and their application to asymmetric hydrogenation and hydroboration |c George Adrian Crosman |
| 264 | 1 | |a Aachen |b Shaker |c 2009 | |
| 300 | |a IV, 152 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
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| 490 | 0 | |a Berichte aus der Chemie | |
| 502 | |a Zugl.: Aachen, Techn. Hochsch., Diss., 2009 | ||
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| 650 | 7 | |a Festphasentechnik |2 swd | |
| 650 | 7 | |a Hydroborierung |2 swd | |
| 650 | 7 | |a Immobilisierung |2 swd | |
| 650 | 7 | |a Katalytische Hydrierung |2 swd | |
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Datensatz im Suchindex
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| adam_text |
CONTENT 1. SCOPE AND PREMISES 1 2. ASYMMETRIC SYNTHESIS AND
STEREOCHEMISTRY 4 2.1. GENERALITIES 4 2.2. COMMON DEFINITIONS 7 2.3.
GENERAL METHODS FOR THE SYNTHESIS OF OPTICALLY ACTIVE COMPOUNDS 9 2.4.
ASYMMETRIC CATALYTIC REACTIONS 11 2.4.1. HOMOGENEOUS ASYMMETRIC
HYDROGENATION 12 2.4.1.1. CHIRAL PHOSPHORUS LIGANDS 14 2.4.2. ASYMMETRIC
HYDROBORATION AND RELATED REACTIONS 18 2.5. IMMOBILIZATION OF CHIRAL
HOMOGENEOUS CATALYSTS 23 2.5.1. SUPPORT MATERIALS 26 2.5.1.1. POLYMERS,
ZEOLITES AND SILICA GELS 26 2.5.1.2. MESOPOROUS MATERIALS 27 2.5.1.2.1.
M41S FAMILY 28 2.5.1.2.2. SBA FAMILY 30 2.5.2. COVALENT IMMOBILIZATION
31 2.5.3. NON-COVALENT IMMOBILIZATION 37 3. RESULTS AND DISCUSSION 48
3.1. HETEROGENIZATLON OF RHODIUM DLPHOSPHLNE COMPLEXES 48 3.1.1. CHOICE
OF RHODIUM PRECURSOR 48 3.1.2. CHOICE OF CHIRAL DIPHOSPHINES 51 3.1.3.
CHOICE OF SUPPORT MATERIALS 51 3.2. CHARACTERIZATION OF THE NEW
HETEROGENLZED CATALYST. 55 3.2.1. COMPUTER SIMULATION OF THE IMMOBILIZED
CATALYSTS 55 3.2.2 BIBLIOGRAFISCHE INFORMATIONEN
HTTP://D-NB.INFO/999464981 DIGITALISIERT DURCH 5.1.1.1. SYNTHESIS
OFAI-MCM-41 (DIRECT SYNTHESIS) 124 5.1.1.2. SYNTHESIS OF SILICEOUS
MCM-41 125 5. 1.1.3. SYNTHESIS OFAI-MCM-48 (DIRECT SYNTHESIS) 125
5.1.1.4. SYNTHESIS OF SILICEOUS SBA-15 125 5.1.1.5. POST-ALUMINATION OF
SILICEOUS MESOSTRUCTURED MATERIALS 126 5.1.2. PREPARATION AND
IMMOBILIZATION OF RHODIUM DIPHOSPHINE COMPLEXES 126 5.2. CATALYST
CHARACTERIZATION 127 5.2.1. ICP-AES 127 5.2.2. XRD 127 5.2.3. N2
SORPTION EXPERIMENTS 127 5.2.4. FT-IR 127 5.2.5. THERMOGRAVLMETRIC
ANALYSIS 128 5.2.6. THERMOPROGRAMMED DESORPTION OF AMMONIA (NH3-TPD) 128
5.2.7. MAS-NMR 129 5.3. SYNTHESIS OF A-1-ARY/A/FCYFENAM/CTES 129 5.4.
CATALYTIC TESTS 130 5.4.1. HOMOGENEOUS HYDROGENATLONS 130 5.4.2.
HETEROGENEOUS HYDROGENATIONS 130 5.4.3. HOMOGENEOUS
HYDROBORATION/OXIDATION REACTIONS 131 5.4.4. HETEROGENEOUS
HYDROBORATION/OXIDATION REACTIONS 132 5.5 5.1.1.1. SYNTHESIS OFAI-MCM-41
(DIRECT SYNTHESIS) 124 5.1.1.2. SYNTHESIS OF SILICEOUS MCM-41 125 5.
1.1.3. SYNTHESIS OFAI-MCM-48 (DIRECT SYNTHESIS) 125 5.1.1.4. SYNTHESIS
OF SILICEOUS SBA-15 125 5.1.1.5. POST-ALUMINATION OF SILICEOUS
MESOSTRUCTURED MATERIALS 126 5.1.2. PREPARATION AND IMMOBILIZATION OF
RHODIUM DIPHOSPHINE COMPLEXES 126 5.2. CATALYST CHARACTERIZATION 127
5.2.1. ICP-AES 127 5.2.2. XRD 127 5.2.3. N 2 SORPTION EXPERIMENTS 127
5.2.4. FT-IR 127 5.2.5. THERMOGRAVIMETRIC ANALYSIS 128 5.2.6.
THERMOPROGRAMMED DESORPTION OF AMMONIA (NH3-TPO) 128 5.2.7. MAS-NMR 129
5.3. SYNTHESIS OF A-1-ARYLALKYLENAMIDES 129 5.4. CATALYTIC TESTS 130
5.4.1. HOMOGENEOUS HYDROGENATIONS 130 5.4.2. HETEROGENEOUS
HYDROGENATIONS 130 5.4.3. HOMOGENEOUS HYDROBORATION/OXIDATION REACTIONS
131 5.4.4. HETEROGENEOUS HYDROBORATION/OXIDATION REACTIONS 132 5.5.
EVALUATION OF THE CATALYTIC PROPERTIES BY GAS CHROMATOGRAPHY 13 |
| any_adam_object | 1 |
| author | Crosman, George Adrian 1976- |
| author_GND | (DE-588)140124160 |
| author_facet | Crosman, George Adrian 1976- |
| author_role | aut |
| author_sort | Crosman, George Adrian 1976- |
| author_variant | g a c ga gac |
| building | Verbundindex |
| bvnumber | BV036119966 |
| ctrlnum | (OCoLC)506488632 (DE-599)BVBBV036119966 |
| dewey-full | 547.215 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 547 - Organic chemistry |
| dewey-raw | 547.215 |
| dewey-search | 547.215 |
| dewey-sort | 3547.215 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV036119966 |
| illustrated | Illustrated |
| indexdate | 2025-02-11T15:00:39Z |
| institution | BVB |
| isbn | 9783832287580 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-019009974 |
| oclc_num | 506488632 |
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| owner_facet | DE-91 DE-BY-TUM |
| physical | IV, 152 S. graph. Darst. |
| publishDate | 2009 |
| publishDateSearch | 2009 |
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| publisher | Shaker |
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| series2 | Berichte aus der Chemie |
| spelling | Crosman, George Adrian 1976- Verfasser (DE-588)140124160 aut Immobilization of Rh-diphosphine complexes on mesostructured materials and their application to asymmetric hydrogenation and hydroboration George Adrian Crosman Aachen Shaker 2009 IV, 152 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Berichte aus der Chemie Zugl.: Aachen, Techn. Hochsch., Diss., 2009 Asymmetrische Synthese swd Chirale Verbindungen swd Festphasentechnik swd Hydroborierung swd Immobilisierung swd Katalytische Hydrierung swd Phosphine swd Rhodiumkomplexe swd Silicate swd Silicate (DE-588)4077444-2 gnd rswk-swf Immobilisierung (DE-588)4123417-0 gnd rswk-swf Hydroborierung (DE-588)4160898-7 gnd rswk-swf Festphasentechnik (DE-588)4154192-3 gnd rswk-swf Asymmetrische Synthese (DE-588)4135603-2 gnd rswk-swf Chirale Verbindungen (DE-588)4348527-3 gnd rswk-swf Katalytische Hydrierung (DE-588)4163422-6 gnd rswk-swf Phosphine (DE-588)4174379-9 gnd rswk-swf Rhodiumkomplexe (DE-588)4314155-9 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Rhodiumkomplexe (DE-588)4314155-9 s Phosphine (DE-588)4174379-9 s Chirale Verbindungen (DE-588)4348527-3 s Immobilisierung (DE-588)4123417-0 s Silicate (DE-588)4077444-2 s DE-604 Katalytische Hydrierung (DE-588)4163422-6 s Asymmetrische Synthese (DE-588)4135603-2 s Festphasentechnik (DE-588)4154192-3 s Hydroborierung (DE-588)4160898-7 s DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=019009974&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Crosman, George Adrian 1976- Immobilization of Rh-diphosphine complexes on mesostructured materials and their application to asymmetric hydrogenation and hydroboration Asymmetrische Synthese swd Chirale Verbindungen swd Festphasentechnik swd Hydroborierung swd Immobilisierung swd Katalytische Hydrierung swd Phosphine swd Rhodiumkomplexe swd Silicate swd Silicate (DE-588)4077444-2 gnd Immobilisierung (DE-588)4123417-0 gnd Hydroborierung (DE-588)4160898-7 gnd Festphasentechnik (DE-588)4154192-3 gnd Asymmetrische Synthese (DE-588)4135603-2 gnd Chirale Verbindungen (DE-588)4348527-3 gnd Katalytische Hydrierung (DE-588)4163422-6 gnd Phosphine (DE-588)4174379-9 gnd Rhodiumkomplexe (DE-588)4314155-9 gnd |
| subject_GND | (DE-588)4077444-2 (DE-588)4123417-0 (DE-588)4160898-7 (DE-588)4154192-3 (DE-588)4135603-2 (DE-588)4348527-3 (DE-588)4163422-6 (DE-588)4174379-9 (DE-588)4314155-9 (DE-588)4113937-9 |
| title | Immobilization of Rh-diphosphine complexes on mesostructured materials and their application to asymmetric hydrogenation and hydroboration |
| title_auth | Immobilization of Rh-diphosphine complexes on mesostructured materials and their application to asymmetric hydrogenation and hydroboration |
| title_exact_search | Immobilization of Rh-diphosphine complexes on mesostructured materials and their application to asymmetric hydrogenation and hydroboration |
| title_full | Immobilization of Rh-diphosphine complexes on mesostructured materials and their application to asymmetric hydrogenation and hydroboration George Adrian Crosman |
| title_fullStr | Immobilization of Rh-diphosphine complexes on mesostructured materials and their application to asymmetric hydrogenation and hydroboration George Adrian Crosman |
| title_full_unstemmed | Immobilization of Rh-diphosphine complexes on mesostructured materials and their application to asymmetric hydrogenation and hydroboration George Adrian Crosman |
| title_short | Immobilization of Rh-diphosphine complexes on mesostructured materials and their application to asymmetric hydrogenation and hydroboration |
| title_sort | immobilization of rh diphosphine complexes on mesostructured materials and their application to asymmetric hydrogenation and hydroboration |
| topic | Asymmetrische Synthese swd Chirale Verbindungen swd Festphasentechnik swd Hydroborierung swd Immobilisierung swd Katalytische Hydrierung swd Phosphine swd Rhodiumkomplexe swd Silicate swd Silicate (DE-588)4077444-2 gnd Immobilisierung (DE-588)4123417-0 gnd Hydroborierung (DE-588)4160898-7 gnd Festphasentechnik (DE-588)4154192-3 gnd Asymmetrische Synthese (DE-588)4135603-2 gnd Chirale Verbindungen (DE-588)4348527-3 gnd Katalytische Hydrierung (DE-588)4163422-6 gnd Phosphine (DE-588)4174379-9 gnd Rhodiumkomplexe (DE-588)4314155-9 gnd |
| topic_facet | Asymmetrische Synthese Chirale Verbindungen Festphasentechnik Hydroborierung Immobilisierung Katalytische Hydrierung Phosphine Rhodiumkomplexe Silicate Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=019009974&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT crosmangeorgeadrian immobilizationofrhdiphosphinecomplexesonmesostructuredmaterialsandtheirapplicationtoasymmetrichydrogenationandhydroboration |