STM investigation of molecular architectures of porphyrinoids on a Ag(111) surface -: supramolecular ordering, electronic properties and reactivity = STM-Untersuchung von Porphyrinoiden auf einer Ag(111)-Oberfläche
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
2010
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| Schlagworte: | |
| Online-Zugang: | kostenfrei https://nbn-resolving.org/urn:nbn:de:bvb:29-opus-16445 http://d-nb.info/1000613143/34 Inhaltsverzeichnis |
| Beschreibung: | IV, 233 S. Ill., graph. Darst. |
| Format: | Langzeitarchivierung Nationalbibliothek gewährleistet |
Internformat
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| 245 | 1 | 0 | |a STM investigation of molecular architectures of porphyrinoids on a Ag(111) surface - |b supramolecular ordering, electronic properties and reactivity = STM-Untersuchung von Porphyrinoiden auf einer Ag(111)-Oberfläche |c von Florian Buchner |
| 246 | 1 | 1 | |a STM-Untersuchung von Porphyrinoiden auf einer Ag(111)-Oberfläche |
| 264 | 1 | |c 2010 | |
| 300 | |a IV, 233 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
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Datensatz im Suchindex
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|---|---|
| adam_text | IMAGE 1
CONTENTS
1 INTRODUCTION 1
REFERENCES 2
2 FUNDAMENTALS 5
2.1 PRINCIPLE OF THE STM 5
2.2 ORIGIN OF THE TUNNELING CURRENT 7
2.3 SCANNING TUNNELING SPECTROSCOPY 9
2.4 CONTRAST MECHANISM OF MOLECULAR ADSORBATES 10
2.5 TEMPERATURE PROGRAMMED DESORPTION 12
2.6 LOW ENERGY ELECTRON DIFFRACTION 14
REFERENCES 15
3 EXPERIMENTAL SETUP 17
3.1 UHV SYSTEM 17
3.2 SCANNING TUNNELING MICROSCOPE 18
3.3 CONTROL ELECTRONICS AND VIBRATION ISOLATION 21
3.4 AG(LLL) 22
3.5 PORPHYRINOIDS 24
3.6 PREPARATION OF THIN PORPHYRINOID LAYERS 25
3.7 VAPOR-DEPOSITION OF COBALT AND IRON 27
REFERENCES 28
PART I RESULTS
4 SELF-ASSEMBLY AND INDIVIDUAL APPEARANCE OF TETRAPHENYLPORPHYRINS ON
AG(LLL) 31
4.1 INTRODUCTION 31
4.2 EPITAXIAL GROWTH 32
4.3 APPEARANCE AND INTRAMOLECULAR CONFORMATION 36
BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/100407123X
DIGITALISIERT DURCH
IMAGE 2
XII CONTENTS
4.4 ORDERING ASPECTS 37
4.5 CONCLUSION 43
REFERENCES 44
5 SELF-ASSEMBLY AND INDIVIDUAL APPEARANCE OF
COBALT(II)-TETRAKISDITERTBUTYLPHENYLPORPHYRINS ON AG(LLL) 47 5.1
POLYMORPHISM OF COTTBPP 47
5.1.1 CONCLUSION 59
5.2 POLARITY-DEPENDENT APPEARANCE 60
5.2.1 CONCLUSION 61
REFERENCES 62
6 COORDINATION OF IRON AND COBALT ATOMS BY TETRAPHENYLPORPHYRIN
MONOLAYERS ON AG(LLL) AND FORMATION OF METAL(II)-TETRAPHENYLPORPHYRIN 63
6.1 INTRODUCTION 63
6.2 COORDINATION OF POST-DEPOSITED IRON ATOMS BY TETRAPHENYLPORPHYRIN
MONOLAYERS 64
6.2.1 CONCLUSION 68
6.3 COORDINATION OF PRE-DEPOSITED IRON ATOMS BY TETRAPHENYLPORPHYRIN
MONOLAYERS 68
6.3.1 CONCLUSION 71
6.4 COORDINATION OF POST-DEPOSITED COBALT ATOMS BY TETRAPHENYLPORPHYRIN
MONOLAYERS 71
6.4.1 CONCLUSION 75
6.5 DISCUSSION OF THE METALATION REACTION 75
REFERENCES 77
7 DIFFERENT ASPECTS OF 2H-TETRAKIS-DI-TERT-BUTYLPHENYIPORPHYRIN ON
AG(LLL) 79
7.1 INTRODUCTION . . 79
7.2 MONOLAYER PREPARATION 80
7.3 ARRANGEMENT OF 2HTTBPP 82
7.3.1 CONCLUSION 85
7.4 VOLTAGE-DEPENDENT APPEARANCE 86
7.4.1 CONCLUSION 87
7.5 DIRECT METALATION OF 2HTTBPP WITH CO-ADSORBED IRON 87 7.5.1
CONCLUSION 88
REFERENCES 89
8 DIRECT METALATION OF A PHTHALOCYANINE MONOLAYER ON AG(LLL) WITH
CO-ADSORBED IRON ATOMS 91
8.1 INTRODUCTION 91
8.2 RESULTS 92
IMAGE 3
CONTENTS XIII
8.3 CONCLUSION 98
REFERENCES 98
9 MULTICOMPONENT ADLAYERS OF TETRAPHENYLPORPHYRINS ON AG(LLL). . 101 9.1
UNDERSTANDING THE CONTRAST MECHANISM IN STM IMAGES OF COBALT
TETRAPHENYLPORPHYRIN ON AG(LLL) 101
9.1.1 INTRODUCTION 102
9.1.2 RESULTS 102
9.1.3 CONCLUSION 108
9.2 FINGERPRINTS OF DIFFERENT PORPHYRINS 109
9.2.1 INTRODUCTION 109
9.2.2 RESULTS I LL
9.2.3 CONCLUSION 120
9.3 ADDRESSING MOLECULAR ORBITALS OF COBALT- AND
IRON-TETRAPHENYLPORPHYRINS BY CONTINUOUS IMAGING TUNNELING SPECTROSCOPY
121
9.3.1 INTRODUCTION 121
9.3.2 RESULTS 122
9.3.3 CONCLUSION 127
REFERENCES 127
10 MODIFICATION OF THE GROWTH OF IRON ON AG(LLL) BY PREDEPOSITED ORGANIC
MONOLAYERS 129
10.1 INTRODUCTION 129
10.1.1 GROWTH OF FE ON AG(LLL) 130
10.1.2 GROWTH OF FE ON AG(L 11) PRECOVERED WITH DIFFERENT TETRAPYRROLIC
MONOLAYERS 132
10.2 CONCLUSION 139
REFERENCES 139
11 GEOMETRIC AND ELECTRONIC ASPECTS OF COTPP UPON DOSAGE OF NO 141
11.1 INTRODUCTION 141
11.2 IN SITU OBSERVATION OF THE REARRANGEMENT OF COTPP ON AG(LLL) 142
11.3 CONCLUSION 146
11.4 MODIFICATION OF THE APPEARANCE OF COTPP UPON FORMATION OF NO-COTPP
147
11.5 CONCLUSION 150
REFERENCES 151
12 SELF-ASSEMBLY AND VOLTAGE-DEPENDENT APPEARANCE OF OCTAETHYLPORPHYRINS
153
12.1 INTRODUCTION 153
IMAGE 4
XIV CONTENTS
12.2 RESULTS 154
12.3 CONCLUSION 158
REFERENCES 159
13 SUMMARY AND OUTLOOK 161
13.1 MOLECULAR ORDERING AND INTRAMOLECULAR CONFORMATION 161 13.2
COORDINATION OF METAL ATOMS BY FREE BASE PORPHYRINOIDS. . . . 162 13.3
ELECTRONIC PROPERTIES OF PORPHYRINS 163
13.4 INTERACTION WITH SMALL MOLECULES 163
13.5 OUTLOOK 164
|
| any_adam_object | 1 |
| author | Buchner, Florian |
| author_GND | (DE-588)140625488 |
| author_facet | Buchner, Florian |
| author_role | aut |
| author_sort | Buchner, Florian |
| author_variant | f b fb |
| building | Verbundindex |
| bvnumber | BV036053442 |
| classification_rvk | UH 6310 VK 5800 |
| collection | ebook |
| ctrlnum | (OCoLC)608751415 (DE-599)DNB1000613143 |
| dewey-full | 547.704533 547.704426 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 547 - Organic chemistry |
| dewey-raw | 547.704533 547.704426 |
| dewey-search | 547.704533 547.704426 |
| dewey-sort | 3547.704533 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik Allgemeine Naturwissenschaft |
| format | Thesis Book |
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| indexdate | 2024-07-09T22:10:23Z |
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| language | English |
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| spelling | Buchner, Florian Verfasser (DE-588)140625488 aut STM investigation of molecular architectures of porphyrinoids on a Ag(111) surface - supramolecular ordering, electronic properties and reactivity = STM-Untersuchung von Porphyrinoiden auf einer Ag(111)-Oberfläche von Florian Buchner STM-Untersuchung von Porphyrinoiden auf einer Ag(111)-Oberfläche 2010 IV, 233 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Erlangen-Nürnberg, Univ., Diss., 2010 Langzeitarchivierung Nationalbibliothek gewährleistet Metalloporphyrine (DE-588)4343266-9 gnd rswk-swf Silber (DE-588)4133759-1 gnd rswk-swf Adsorption (DE-588)4000536-7 gnd rswk-swf Tetrapyrrole (DE-588)4140190-6 gnd rswk-swf Komplexe (DE-588)4133953-8 gnd rswk-swf Rastertunnelmikroskopie (DE-588)4252995-5 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Tetrapyrrole (DE-588)4140190-6 s Komplexe (DE-588)4133953-8 s Silber (DE-588)4133759-1 s Adsorption (DE-588)4000536-7 s Rastertunnelmikroskopie (DE-588)4252995-5 s DE-604 Metalloporphyrine (DE-588)4343266-9 s Erscheint auch als Online-Ausgabe urn:nbn:de:bvb:29-opus-16445 https://open.fau.de/handle/openfau/1093 Verlag kostenfrei Volltext https://nbn-resolving.org/urn:nbn:de:bvb:29-opus-16445 Resolvingsystem http://d-nb.info/1000613143/34 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018945076&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Buchner, Florian STM investigation of molecular architectures of porphyrinoids on a Ag(111) surface - supramolecular ordering, electronic properties and reactivity = STM-Untersuchung von Porphyrinoiden auf einer Ag(111)-Oberfläche Metalloporphyrine (DE-588)4343266-9 gnd Silber (DE-588)4133759-1 gnd Adsorption (DE-588)4000536-7 gnd Tetrapyrrole (DE-588)4140190-6 gnd Komplexe (DE-588)4133953-8 gnd Rastertunnelmikroskopie (DE-588)4252995-5 gnd |
| subject_GND | (DE-588)4343266-9 (DE-588)4133759-1 (DE-588)4000536-7 (DE-588)4140190-6 (DE-588)4133953-8 (DE-588)4252995-5 (DE-588)4113937-9 |
| title | STM investigation of molecular architectures of porphyrinoids on a Ag(111) surface - supramolecular ordering, electronic properties and reactivity = STM-Untersuchung von Porphyrinoiden auf einer Ag(111)-Oberfläche |
| title_alt | STM-Untersuchung von Porphyrinoiden auf einer Ag(111)-Oberfläche |
| title_auth | STM investigation of molecular architectures of porphyrinoids on a Ag(111) surface - supramolecular ordering, electronic properties and reactivity = STM-Untersuchung von Porphyrinoiden auf einer Ag(111)-Oberfläche |
| title_exact_search | STM investigation of molecular architectures of porphyrinoids on a Ag(111) surface - supramolecular ordering, electronic properties and reactivity = STM-Untersuchung von Porphyrinoiden auf einer Ag(111)-Oberfläche |
| title_full | STM investigation of molecular architectures of porphyrinoids on a Ag(111) surface - supramolecular ordering, electronic properties and reactivity = STM-Untersuchung von Porphyrinoiden auf einer Ag(111)-Oberfläche von Florian Buchner |
| title_fullStr | STM investigation of molecular architectures of porphyrinoids on a Ag(111) surface - supramolecular ordering, electronic properties and reactivity = STM-Untersuchung von Porphyrinoiden auf einer Ag(111)-Oberfläche von Florian Buchner |
| title_full_unstemmed | STM investigation of molecular architectures of porphyrinoids on a Ag(111) surface - supramolecular ordering, electronic properties and reactivity = STM-Untersuchung von Porphyrinoiden auf einer Ag(111)-Oberfläche von Florian Buchner |
| title_short | STM investigation of molecular architectures of porphyrinoids on a Ag(111) surface - |
| title_sort | stm investigation of molecular architectures of porphyrinoids on a ag 111 surface supramolecular ordering electronic properties and reactivity stm untersuchung von porphyrinoiden auf einer ag 111 oberflache |
| title_sub | supramolecular ordering, electronic properties and reactivity = STM-Untersuchung von Porphyrinoiden auf einer Ag(111)-Oberfläche |
| topic | Metalloporphyrine (DE-588)4343266-9 gnd Silber (DE-588)4133759-1 gnd Adsorption (DE-588)4000536-7 gnd Tetrapyrrole (DE-588)4140190-6 gnd Komplexe (DE-588)4133953-8 gnd Rastertunnelmikroskopie (DE-588)4252995-5 gnd |
| topic_facet | Metalloporphyrine Silber Adsorption Tetrapyrrole Komplexe Rastertunnelmikroskopie Hochschulschrift |
| url | https://open.fau.de/handle/openfau/1093 https://nbn-resolving.org/urn:nbn:de:bvb:29-opus-16445 http://d-nb.info/1000613143/34 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018945076&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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