Conducting polymers for interfacial modification of heterogeneous polymer blends:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
München
Verl. Dr. Hut
2009
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| Ausgabe: | 1. Aufl. |
| Schriftenreihe: | Makromolekulare Chemie
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Zugl.: Dresden, Techn. Univ., Diss., 2009 |
| Beschreibung: | 202, 13 S. Ill., graph. Darst. 210 mm x 148 mm, 337 gr. |
| ISBN: | 9783868531954 |
Internformat
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Datensatz im Suchindex
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|---|---|
| adam_text | CONDUCTING POLYMERS FOR INTERFACIAL MODIFICATION OF HETEROGENEOUS
POLYMER BLENDS DISSERTATION ZUR ERLANGUNG DES AKADEMISCHEN GRADES DOCTOR
RERAM NATURALIUM (DR. RER. NAT) VORGELEGT DER FAKULTAET MATHEMATIK UND
NATURWISSENSCHAFTEN DER TECHNISCHEN UNIVERSITAET DRESDEN VON DIPL.-CHEM.
JAN HEGEWALD, GEBOREN AM 20.04.1979 IN DOHNA EINGEREICHT AM: 29.05.2009
DIE DISSERTATION WURDE IN DER ZEIT VON NOVEMBER 2005 BIS MAI 2009 IM
INSTITUT FUER POLYMERFORSCHUNG DRESDEN E.V. ANGEFERTIGT. TABLE OF CONTENT
GENERAL
INTRODUCTION....................................................................................................
1 MOTIVATION TO THE WORK 1 STATE OF THE ART 2 STRATEGY AND RESULTANT
OBJECTIVES 10 MATERIALS AND CHARACTERIZATION METHODS 13 A. SYNTHESIS OF
AMINO AND CARBOXY END-FUNCTIONALIZED MATRIX
POLYMERS...................... 19 *.1. ATOM TRANSFER RADICAL
POLYMERIZATION (ATRP) 19 A.1.1. INTRODUCTION 19 A.1.2. EXPERIMENTAL 22
A.1.3. RESULTS AND DISCUSSION 26 A.1.4. ATRP CONCLUSION 40 A.2.
REVERSIBLE ADDITION-FRAGMENTATION CHAIN TRANSFER POLYMERIZATION (RAPT)
41 A.2.1. INTRODUCTION 41 A.2.2. EXPERIMENTAL 43 A.2.3. RESULTS AND
DISCUSSION 48 A.2.4. RAFT CONCLUSION 71 A.3. CONCLUSIONS 71 B. SYNTHESIS
AND CHARACTERIZATION OF CONDUCTING POLYPYRROLE (PPY) ........ 74 B.L.
INTRODUCTION 74 B.2. SYNTHESIS OF REACTIVE PYRROLE MONOMERS 76 B.2.1.
EXPERIMENTAL 76 B.2.2. DISCUSSION 79 B.3. PRELIMINARY CONSIDERATIONS TO
THE (CO-)POLYMERIZATION OF (FUNCTIONAL) PYRROLES 80 B.3.1. THE PYRROLE
POLYMERIZATION MECHANISM 81 B.3.2. DETERMINING THE OXIDATION POTENTIAL
OF THE SYNTHESIZED PYRROLE DERIVATIVES.... 83 B.4. CHEMICAL
(CO-)POLYMERIZATION OF PYRROLE AND PYRROLE DERIVATIVES 92 B.4.1.
EXPERIMENTAL 92 B.4.2. RESULTS AND DISCUSSION 93 B.5. VERIFYING THE
REACTIVITY OF THE FUNCTIONAL SITES IN THE CONDUCTING POLYMER 110 B.6.
THERMAL STABILITY AND THERMAL AGING OF POLYPYRROLES 112 B.7. CONCLUSIONS
125 TABLE OF CONTENT *. POLYMER (REACTIVE) BLENDING ............
............ ..................... ....... ...... 128 C.L. INTRODUCTION
128 C.2. EXPERIMENTAL 131 C.3. MECHANICAL MELT MIXING OF PS/PMMA BLENDS
WITH AND WITHOUT PPY FILLER 134 C.4. TWO-STEP MIXING PROCEDURE 146 C.5.
EXTRACTION EXPERIMENTS TO ELUCIDATE THE ENVISAGED COUPLING REACTION 149
C.6. DSC MEASUREMENTS 152 C.7. MECHANICAL AND RHEOLOGICAL TESTING 153
C.7.1. RHEOLOGICAL STUDIES 154 C.7.2. MECHANICAL TESTING 156 C.8.
ELECTRICAL CONDUCTIVITY AND DIELECTRIC MEASUREMENTS 160 C.9. PS/PPY
CORE-SHELL-PARTICLES FOR POLYMER BLENDING 163 CIO. TWO-STEP REACTIVE
BLENDING 168 **. COMPRESSION MOLDED PS/PMMA/PPY COMPOSITES 172 C.12.
CONCLUSIONS 182 SUMMARY AND OUTLOOK. . .... .......... ........ ...
...........* 185 REFERENCES 192 APPENDIX ....... ........... .......
............. ....... .. ............ AL *H AND 13 C DATA AND SPECTRA AL
SUPPLEMENTARY TABLES A8 CHEMICALS AND SUPPLIERS A9 ABBREVIATIONS ALL
|
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| indexdate | 2024-07-09T22:05:58Z |
| institution | BVB |
| isbn | 9783868531954 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-018703100 |
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| physical | 202, 13 S. Ill., graph. Darst. 210 mm x 148 mm, 337 gr. |
| publishDate | 2009 |
| publishDateSearch | 2009 |
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| publisher | Verl. Dr. Hut |
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| series2 | Makromolekulare Chemie |
| spelling | Hegewald, Jan 1979- Verfasser (DE-588)139770607 aut Conducting polymers for interfacial modification of heterogeneous polymer blends Jan Hegewald 1. Aufl. München Verl. Dr. Hut 2009 202, 13 S. Ill., graph. Darst. 210 mm x 148 mm, 337 gr. txt rdacontent n rdamedia nc rdacarrier Makromolekulare Chemie Zugl.: Dresden, Techn. Univ., Diss., 2009 (DE-588)4113937-9 Hochschulschrift gnd-content GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018703100&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Hegewald, Jan 1979- Conducting polymers for interfacial modification of heterogeneous polymer blends |
| subject_GND | (DE-588)4113937-9 |
| title | Conducting polymers for interfacial modification of heterogeneous polymer blends |
| title_auth | Conducting polymers for interfacial modification of heterogeneous polymer blends |
| title_exact_search | Conducting polymers for interfacial modification of heterogeneous polymer blends |
| title_full | Conducting polymers for interfacial modification of heterogeneous polymer blends Jan Hegewald |
| title_fullStr | Conducting polymers for interfacial modification of heterogeneous polymer blends Jan Hegewald |
| title_full_unstemmed | Conducting polymers for interfacial modification of heterogeneous polymer blends Jan Hegewald |
| title_short | Conducting polymers for interfacial modification of heterogeneous polymer blends |
| title_sort | conducting polymers for interfacial modification of heterogeneous polymer blends |
| topic_facet | Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018703100&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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