Electrocatalysis of direct methanol fuel cells: from fundamentals to applications
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Weinheim
WILEY-VCH
2009
|
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | XXII, 582 S. Ill., graph. Darst. |
| ISBN: | 9783527323777 |
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| 650 | 4 | |a Fuel cells | |
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Datensatz im Suchindex
| _version_ | 1805093140429799424 |
|---|---|
| adam_text |
CONTENTS PREFACE XV LIST OF CONTRIBUTORS XIX 1 DIRECT METHANOL FUEL
CELLS: HISTORY, STATUS AND PERSPECTIVES 1 ANTONINO SALVATORE ARICO,
VINCENZO BAGLIO, AND VINCENZO ANTONUCCI 1.1 INTRODUCTION 1 1.2 CONCEPT
OF DIRECT METHANOL FUEL CELLS 2 1.2.1 PRINCIPLES OF OPERATION 2 1.2.1.1
DMFC COMPONENTS 2 1.2.1.2 DMFC OPERATION MODE 3 1.2.1.3 FUEL CELL
PROCESS 3 1.2.2 PERFORMANCE, EFFICIENCY AND ENERGY DENSITY 4 1.2.2.1
POLARIZATION CURVES AND PERFORMANCE 4 1.2.2.2 FUEL UTILIZATION 5 1.2.2.3
CATHODE OPERATING CONDITIONS 7 1.2.2.4 HEAT PRODUCTION 8 1.2.2.5 CELL
EFFICIENCY 9 1.2.2.6 ENERGY DENSITY 9 1.3 HISTORICAL ASPECTS OF DIRECT
METHANOL FUEL CELL DEVELOPMENT AND STATE-OF-THE-ART 10 1.3.1 HISTORICAL
DEVELOPMENT OF METHANOL OXIDATION CATALYSTS 10 1.3.2 STATUS OF KNOWLEDGE
OF METHANOL OXIDATION PROCESS AND STATE-OF-THE-ART ANODE CATALYSTS 14
1.3.2.1 OXIDATION MECHANISM 14 1.3.2.2 PT-RU CATALYSTS 25 1.3.2.3
ALTERNATIVE ANODE FORMULATIONS 19 1.3.2.4 PRACTICAL ANODE CATALYSTS 19
1.3.2.5 ANODE CATALYSTS FOR ALKALINE DMFC SYSTEMS 20 BIBLIOGRAFISCHE
INFORMATIONEN HTTP://D-NB.INFO/993261299 DIGITALISIERT DURCH VI CONTENTS
1.3.4.2 PROTON CONDUCTING MEMBRANES 24 1.3.4.3 MEMBRANES FOR HIGH
TEMPERATURE APPLICATIONS 26 1.3.4.4 ALKALINE MEMBRANES 29 1.3.4.5
EFFECTS OF CROSSOVER ON DMFC PERFORMANCE AND EFFICIENCY 32 1.3.5
HISTORICA! DEVELOPMENT OF OXYGEN ELECTROREDUCTION IN DMFCS 33 1.3.6
STATUS OF KNOWLEDGE OF OXYGEN REDUCTION ELECTROCATALYSIS AND
STATE-OF-THE-ART CATHODE CATALYSTS 33 1.3.6.1 OXYGEN REDUCTION PROCESS
33 1.3.6.2 PT-BASED CATALYSTS AND NON-NOBLE METAL ELECTROCATALYSTS 35
1.3.6.3 ALTERNATIVE CATHODE CATALYSTS 37 1.3.7 DMFC POWER SOURCES IN THE
'PRE-1990 ERA' 39 1.4 CURRENT STATUS OF DMFC TECHNOLOGY FOR DIFFERENT
FIELDS OF APPLICATION 40 1.4.1 PORTABLE POWER SOURCES 40 1.4.2
TRANSPORTATION 53 1.4.3 TECHNOLOGY DEVELOPMENT 60 1.4.3.1 DMFC
TECHNOLOGY 60 1.4.3.2 CATALYST PREPARATION 61 1.4.3.3 ELECTRODE
MANUFACTURING AND MEMBRANE ELECTRODE ASSEMBLIES MEMBRANE ELECTRODE
ASSEMBLY (MEAS) 61 1.4.3.4 STACK HARDWARE AND DESIGN 62 1.4.3.5 DMFC
SYSTEMS 64 1.5 PERSPECTIVES OF DIRECT METHANOL FUEL CELLS AND
TECHNO-ECONOMICA CONTENTS VII 2.4.2.3 NANOPOROUS PLATINUM I02 2.4.2.4
HOLLOW PLATINUM NANOCHANNELS 102 2.4.2.5 BIMETALLIC CLUSTERS 103 2.4.3
ELECTROCHEMICAL SYNTHESIS 104 2.4.3.1 SPHERICAL PLATINUM CLUSTERS 204
2.4.3.2 NANOPOROUS PLATINUM 205 2.4.3.3 TETRAHEXAHEDRAL PLATINUM
NANOSTRUCTURES 206 2.5 CONCLUSIONS 208 REFERENCES 220 3 ELECTROCATALYST
CHARACTERIZATION AND ACTIVITY VALIDATION - FUNDAMENTALS AND METHODS 115
LOKA SUBRAMANYAM SARMA, FADLILATUL TAUFANY, AND BING-JOE HWANG 3.1
INTRODUCTION 2 25 3.2 DIRECT METHANOL FUEL CELLS - ROLE OF
ELECTROCATALYSTS 2 27 3.2.1 ROLE OF ANODE ELECTROCATALYSTS - METHANOL
OXIDATION REACTION (MOR) 228 3.2.2 ROLE OF CATHODE ELECTROCATALYSTS -
OXYGEN REDUCTION REACTION (ORR) 2 29 3.3 CHARACTERIZATION TECHNIQUES FOR
ANODE AND CATHODE CATALYSTS 221 3.3.1 FUNDAMENTAL ASPECTS 222 3.3.2
EVALUATION OF CATALYST CRYSTALLITE SIZE, ELEMENTAL COMPOSITION,
MORPHOLOGY, DISPERSION 122 3.3.2.1 X-RAY DIFFRACTION (XRD) 222 3.3.2.2
TRANSMISSION ELECTRON MICROSCOPY (TEM) 224 3.3.2.3 SCANNING ELECTRON
MICROSCOPY (SEM) 125 3.3.2.4 ATOMIC FORCE MICROSCOPY (AFM) 225 3.3.2.5
ENERGY DISPERSIVE X-RAY SPECTROSCOPY (EDS/EDX) 125 3.3.3 ELUCIDATION OF
NANOSTRUCTURAL CHARACTERISTICS OF ELECTROCATALYSTS - ALLOYIN VILI
CONTENTS 3.4.1.2 STATE OF THE PT-BASED CATALYSTS 137 3.4.1.3 QUALITATIVE
INDICATOR FOR THE ACTIVITY OF PT-BASED CATALYSTS TOWARDS ORR 139 3.4.1.4
QUALITATIVE INDICATOR FOR THE ACTIVITY OF PT-BASED CATALYSTS TOWARDS MOR
139 3.4.1.5 REVERSIBILITY OF H A D S /DES REACTION AND ROUGHNESS FACTOR
(RF) OF PT-BASED CATALYSTS 140 3.4.1.6 ELECTROCHEMICAL ACTIVE SURFACE
AREA (ECASA) AND PARTICLE SIZE OF PT-BASED CATALYSTS 240 3.4.2
ADSORPTIVE CO-STRIPPING VOLTAMMETRY (CO ADS -SV) 141 3.4.3
UNDERPOTENTIAL DEPOSITION (UPD) 143 3.4.3.1 SURFACE COMPOSITION OF
PT-BASED CATALYSTS THROUGH THE CU-UPD METHOD 145 3.4.4 ROTATING DISK
ELECTRODE (RDE) 146 3.4.5 ROTATING RING-DISK ELECTRODE (RRDE) METHOD 148
3.4.6 LINEAR SWEEP VOLTAMMETRY (LSV) 149 3.5 CONCLUSIONS AND OUTLOOK 155
REFERENCES 256 4 COMBINATORIAL AND HIGH THROUGHPUT SCREENING OF DMFC
ELECTROCATALYSTS 165 RONGZHONG JIANG AND DERYN CHU 4.1 INTRODUCTION 165
4.2 COMMON PROCEDURES FOR THE DEVELOPMENT OF DMFC CATALYSTS 268 4.
CONTENTS IX 4.8 CHALLENGE AND PERSPECTIVE 1 90 REFERENCES 2 93 5
STATE-OF-THE-ART ELECTROCATALYSTS FOR DIRECT METHANOL FUEL CELLS 297
HANWEI LEI, PAOLINA ATANASSOVA, YIPENG SUN, AND BERISLAV BLIZANAC 5.1
INTRODUCTION 297 5.2 ELECTROCATALYSIS AND ELECTROCATALYSTS FOR DMFC 298
5.2.1 ELECTROCATALYSIS FOR METHANOL OXIDATION 298 5.2.2 ELECTROCATALYST
DEVELOPMENT 199 5.2.3 SPRAY CONVERSION REACTION PLATFORM FOR
ELECTROCATALYST MANUFACTURING 202 5.3 DMFC ELECTROCATALYST
CHARACTERIZATION AND EVALUATION 203 5.3.1 PHYSICAL CHARACTERIZATION 204
5.3.2 ELECTROCHEMICAL EVALUATION 208 5.3.2.1 THIN FILM ROTATING DISC
ELECTRODE (TFRDE) CATALYST CHARACTERIZATION 208 5.3.2.2 FUEL CELL
EVALUATION 210 5.3.3 DURABILITY STUDY 212 5.4 DMFC PERFORMANCE
ADVANCEMENT VIA MEA DESIGN 215 5.4.1 ELECTROCATALYST LAYER DESIGN 225
5.4.2 HYDROCARBON MEMBRANE FOR DMFC PERFORMANCE IMPROVEMENT 227 5.4.3
OTHER ASPECTS OF DMFC CATALYST DEVELOPMENT 220 5.5 PROSPECTS FOR DMFC
222 5.6 CONCLUSIONS 222 REFERENCE CONTENTS 6.5 STABILITY OF PT-RU
CATALYSTS IN DMFC ENVIRONMENT 248 6.6 CONCLUSIONS 250 REFERENCES 251 7
METHANOL-TOLERANT CATHODE CATALYSTS FOR DMFC 257 CLAUDE LAMY, CHRISTOPHE
COUTANCEAU, AND NICOLAS ALONSO-VANTE 7.1 INTRODUCTION 257 7.2
THERMODYNAMICS AND KINETICS OF THE OXYGEN REDUCTION REACTION (ORR) 258
7.2.1 THE ORR AT A PLATINUM ELECTRODE IN A DMFC 258 7.2.2 CONCEPTS FOR
NOVEL OXYGEN REDUCTION ELECTROCATALYSTS 261 7.3 EXPERIMENTAL DETAILS 264
7.3.1 DETERMINATION OF THE METHANOL CROSSOVER OF PROTON EXCHANGE
MEMBRANES 264 7.3.1.1 EXPERIMENTAL PROCEDURES 264 7.3.1.2 RESULTS 266
7.3.2 ELECTROCHEMICAL MEASUREMENTS (VOLTAMMETRY, RDE, RRDE, ETC.) 269
7.3.2.1 EXPERIMENTAL SET-UP 269 7.3.2.2 ANALYSIS OF THE DATA 269 7.4
SYNTHESIS AND CHARACTERIZATIONS OF NANOSTRUCTURED CATALYSTS FOR THE ORR
272 7A.I PLATINUM-BASED CATALYSTS AND ELECTRODES 272 7.4.1.1 SYNTHESIS
OF PLATINUM-BASED CATALYSTS BY THE CARBONYL COMPLEX ROUTE 273 7.4.1.2
SYNTHESIS OF PLATINUM-BASED CATALYSTS BY THE COLLOIDAL ROUTE 273 7.4.1.
CONTENTS XI 7.6 SUMMARY AND OUTLOOK 306 REFERENCES 308 8 CARBON
NANOTUBE-SUPPORTED CATALYSTS FOR THE DIRECT METHANOL FUEL CELL 315
CHEN-HAO WANG, LI-CHYONG CHEN, AND KUEI-HSIEN CHEN 8.1 INTRODUCTION 325
8.2 PREPARATION OF CARBON NANOTUBE-SUPPORTED CATALYSTS 316 8.2.1
FUNCTIONALIZATION OF CARBON NANOTUBES 316 8.2.2 POLYMER-MODIFIED CNTS
317 8.2.3 IMPREGNATION METHOD 318 8.2.4 COLLOIDAL METHOD 322 8.2.5
ELECTRODEPOSITION METHOD 323 8.3 CHARACTERISTICS OF THE CARBON NANOTUBE
ELECTRODE 325 8.3.1 ELECTROCHEMICAL BEHAVIOR OF THE CNT ELECTRODE 325
8.3.2 DURABILITY OF THE CNT ELECTRODE 329 8.4 ELECTROCHEMICAL BEHAVIOR
OF CARBON NANOTUBE-SUPPORTED CATALYSTS 332 8.4.1 METHANOL OXIDATION
REACTION 331 8.4.2 OXYGEN REDUCTION REACTION 337 8.4.3 ELECTROCHEMICAL
IMPEDANCE ANALYSIS 340 8.5 DIRECT GROWTH OF CARBON NANOTUBES AS CATALYST
SUPPORTS 341 8.5.1 DIRECT GROWTH OF CNTS ON CARBON CLOTH (CNT-CC) 342
8.5.2 APPEARANCE OF CNT-CC-SUPPORTED CATALYSTS 344 8.5. XII CONTENTS 9.5
SUMMARY AND PROSPECT 373 REFERENCES 375 10 PROTON EXCHANGE MEMBRANES FOR
DIRECT METHANOL FUEL CELLS 379 DAE SIK KIM, MICHAEL D. CUIVER, AND YU
SEUNG KIM 10.1 INTRODUCTION 379 10.2 SYNTHESIS OF POLYMER ELECTROLYTE
MEMBRANES FOR DMFC 380 10.2.1 SYNTHESIS AND PROPERTIES OF PEMS
CONTAINING ALIPHATIC POLYMERS 380 10.2.2 SYNTHESIS OF SULFONATED
POLY(ARYL ETHER) COPOLYMERS 385 10.2.2.1 POST-SULFONATION OF POLYMERS
385 10.2.2.2 DIRECT COPOLYMERIZATION OF SULFONATED MONOMERS 388 10.2.2.3
OTHER SYNTHETIC STRATEGIES: INTRODUCING SULFONIC ACID GROUPS 397
10.2.2.4 PROPERTIES OF SULFONATED POLY(ARYLENE ETHER) COPOLYMERS 402
10.2.3 SINGLE CELL PERFORMANCES 403 10.3 CONCLUSIONS 412 REFERENCES 412
11 FABRICATION AND OPTIMIZATION OF DMFC CATALYST LAYERS AND MEMBRANE
ELECTRODE ASSEMBLIES 417 LIANG MA, YUNJIE HUANG, LIGANG FENG, WEI XING,
ANDJIUJUN ZHANG 11.1 INTRODUCTION 417 11.2 COMPONENTS FOR DMFC CATALYST
LAYER OPTIMIZATION 419 CONTENTS XIII 12.2.2 BASIC ASSUMPTIONS 452 12.2.3
THROUGH-PLANE RELATIONS 453 12.2.4 EQUATIONS ALONG THE CHANNEL 454
12.2.5 LARGE METHANOL STOICHIOMETRY, SMALL CURRENT 456 12.3 THE
BIFUNCTIONAL REGIME OF DMFC OPERATION 459 12.3.1 EXPERIMENTAL 459 12.3.2
EXPERIMENTAL RESULTS 461 12.3.3 POLARIZATION CURVES AT CONSTANT OXYGEN
STOICHIOMETRY 462 12.3.4 CRITICAL AIR FLOW RATE 464 12.4 DIRECT
METHANOL-HYDROGEN FUEL CELLS (DMHFCS) 466 12.4.1 EXPERIMENT 466 12.4.2
DMHFC: THE MECHANISM OF FUNCTIONING 470 12.4.2.1 POTENTIALS ACROSS THE
CELL 470 12.4.2.2 POTENTIALS ALONG THE CHANNEL 471 12.4.2.3 POTENTIALS
IN THE GALVANIC DOMAIN 473 12.4.2.4 THE TRANSITION REGION: HYDROGEN CELL
474 12.5 BIFUNCTIONAL ACTIVATION OF DMFC 476 12.5.1 SINGLE CHANNEL CELL
476 12.5.2 ACTIVATION OF SQUARE-SHAPED CELLS 480 12.6 CONCLUSIONS 482
12.7 LIST OF SYMBOLS 483 12.7.1 SUPERSCRIPTS 484 12.7.2 SUBSCRIPTS 484
XIV CONTENTS 13.6.1 ANION EXCHANGE MEMBRANE FOR METHANOL FUEL CELLS 511
13.6.2 DIRECT METHANOL ALKALINE MEMBRANE FUEL CELL PERFORMANCE 523
13.6.3 MEMBRANELESS FUEL CELL 527 13.7 ALKALINE FUEL CELLS WITH OTHER
DIRECT LIQUID FUELS 518 13.8 CONCLUSIONS 520 REFERENCES 521 14
ELECTROCATALYSIS IN OTHER DIRECT LIQUID FUEL CELLS 527 SHARON L. BLAIR
AND WAI LUNG (SIMON) LAW 14.1 INTRODUCTION 527 14.1.1 FUEL
CHARACTERISTICS AND THEORETICAL COMPARISON OF VARIOUS FUELS 527 14.2
ELECTROCATALYSIS OF DIRECT FORMIC ACID FUEL CELLS 528 14.2.2 ANODE
CATALYSTS FOR DFAFCS 530 14.2.2.1 PT-BASED ANODE CATALYSTS 531 14.2.2.2
ALTERNATIVE PT MODIFIERS 536 14.2.2.3 PD-BASED ANODE CATALYSTS 536
14.2.3 CATHODE CATALYSTS FOR DFAFCS 541 14.2.4 DIRECT FORMIC ACID FUEL
CELL PERFORMANCE 541 14.2.5 SUMMARY OF ELECTROCATALYSIS IN DFAFCS 545
14.3 ELECTROCATALYSIS OF DIRECT ETHANOL FUEL CELLS 545 14.3.1 ANODE
CATALYSTS FOR DEFCS 546 14.3.1.1 BINARY CATALYSTS 547 14.3.1.2 TERNARY
CATALYSTS 549 |
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| id | DE-604.BV035803596 |
| illustrated | Illustrated |
| indexdate | 2024-07-20T10:22:46Z |
| institution | BVB |
| isbn | 9783527323777 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-018662681 |
| oclc_num | 432406331 |
| open_access_boolean | |
| owner | DE-29T DE-92 DE-11 |
| owner_facet | DE-29T DE-92 DE-11 |
| physical | XXII, 582 S. Ill., graph. Darst. |
| publishDate | 2009 |
| publishDateSearch | 2009 |
| publishDateSort | 2009 |
| publisher | WILEY-VCH |
| record_format | marc |
| spelling | Electrocatalysis of direct methanol fuel cells from fundamentals to applications ed. by Hansan Liu ... Weinheim WILEY-VCH 2009 XXII, 582 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Electrocatalysis Fuel cells Methanol as fuel Elektrokatalyse (DE-588)4151819-6 gnd rswk-swf Methanolzelle (DE-588)4817944-9 gnd rswk-swf Methanolzelle (DE-588)4817944-9 s Elektrokatalyse (DE-588)4151819-6 s DE-604 Liu, Hansan Sonstige (DE-588)139370234 oth text/html http://deposit.dnb.de/cgi-bin/dokserv?id=3261154&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018662681&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Electrocatalysis of direct methanol fuel cells from fundamentals to applications Electrocatalysis Fuel cells Methanol as fuel Elektrokatalyse (DE-588)4151819-6 gnd Methanolzelle (DE-588)4817944-9 gnd |
| subject_GND | (DE-588)4151819-6 (DE-588)4817944-9 |
| title | Electrocatalysis of direct methanol fuel cells from fundamentals to applications |
| title_auth | Electrocatalysis of direct methanol fuel cells from fundamentals to applications |
| title_exact_search | Electrocatalysis of direct methanol fuel cells from fundamentals to applications |
| title_full | Electrocatalysis of direct methanol fuel cells from fundamentals to applications ed. by Hansan Liu ... |
| title_fullStr | Electrocatalysis of direct methanol fuel cells from fundamentals to applications ed. by Hansan Liu ... |
| title_full_unstemmed | Electrocatalysis of direct methanol fuel cells from fundamentals to applications ed. by Hansan Liu ... |
| title_short | Electrocatalysis of direct methanol fuel cells |
| title_sort | electrocatalysis of direct methanol fuel cells from fundamentals to applications |
| title_sub | from fundamentals to applications |
| topic | Electrocatalysis Fuel cells Methanol as fuel Elektrokatalyse (DE-588)4151819-6 gnd Methanolzelle (DE-588)4817944-9 gnd |
| topic_facet | Electrocatalysis Fuel cells Methanol as fuel Elektrokatalyse Methanolzelle |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=3261154&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018662681&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT liuhansan electrocatalysisofdirectmethanolfuelcellsfromfundamentalstoapplications |