Rhenium, molybdenum and tungsten organometallic homogeneous catalysts: synthesis, characterisation and application in olefin epoxidation
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
München
Verl. Dr. Hut
2009
|
| Ausgabe: | 1. Aufl. |
| Schriftenreihe: | Anorganische Chemie
|
| Schlagworte: | |
| Online-Zugang: | Volltext https://nbn-resolving.org/urn:nbn:de:bvb:91-diss-20090804-806954-1-2 Inhaltsverzeichnis |
| Beschreibung: | 199 S. graph. Darst. |
| ISBN: | 9783868531718 |
Internformat
MARC
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| 245 | 1 | 0 | |a Rhenium, molybdenum and tungsten organometallic homogeneous catalysts |b synthesis, characterisation and application in olefin epoxidation |c Alejandro Capapé Miralles |
| 250 | |a 1. Aufl. | ||
| 264 | 1 | |a München |b Verl. Dr. Hut |c 2009 | |
| 300 | |a 199 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a Anorganische Chemie | |
| 502 | |a Zugl.: München, Techn. Univ., Diss., 2009 | ||
| 650 | 0 | 7 | |a Wolframkomplexe |0 (DE-588)4223114-0 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Katalytische Oxidation |0 (DE-588)4163425-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Rheniumkomplexe |0 (DE-588)4223129-2 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Epoxidation |0 (DE-588)4152560-7 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Molybdänkomplexe |0 (DE-588)4223139-5 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Epoxidation |0 (DE-588)4152560-7 |D s |
| 689 | 0 | 1 | |a Katalytische Oxidation |0 (DE-588)4163425-1 |D s |
| 689 | 0 | 2 | |a Rheniumkomplexe |0 (DE-588)4223129-2 |D s |
| 689 | 0 | 3 | |a Molybdänkomplexe |0 (DE-588)4223139-5 |D s |
| 689 | 0 | 4 | |a Wolframkomplexe |0 (DE-588)4223114-0 |D s |
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| 912 | |a ebook | ||
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Datensatz im Suchindex
| _version_ | 1804139431577255936 |
|---|---|
| adam_text | INDEX I. INTRODUCTION 1 1. OXIDATION CATALYSIS: AN OVERVIEW 2 1.1 SCOPE
OF THE PRESENT WORK 2 2. THE EPOXIDATION REACTION. INDUSTRIAL
SIGNIFICANCE 4 2.1 EPOXIDES: A KEY INDUSTRIAL INTERMEDIATE 5 2.1.1
SIGNIFICANT EPOXIDES IN THE INDUSTRIAL WORLD 7 2.2 CATALYTIC EPOXIDATION
9 2.2.1 THE OXIDANT POINT OF VIEW. INTRODUCTION OF CATALYTIC PROCESSES
IN THE EPOXIDATION INDUSTRY 9 2.2.2 CURRENT INDUSTRIAL ADVANCES IN
CATALYSIS. PROPYLENE OXIDE 11 3. OLEFIN EPOXIDATION FROM A CATALYST
POINT OF VIEW 18 3.1 HOMOGENEOUS CATALYSIS 18 3.1.1 HOMOGENEOUS
EPOXIDATION CATALYSIS. TRANSITION METAL OXIDES 19 3.2 ASYMMETRIC
EPOXIDATION 23 3.2.1 ASYMMETRIC HOMOGENEOUS EPOXIDATION CATALYSTS 24 4
OBJECTIVES OF THIS WORK 27 REFERENCES CITED IN THIS CHAPTER 29 II.
SCHIFF BASE ADDUCTS OF METHYLTRIOXORHENIUM 33 5. RHENIUM OXIDES AS
EPOXIDATION CATALYSTS 36 5.1 ALKYL- AND ARYL-TRIOXORHENIUM COMPOUNDS 36
5.2 METHYLTRIOXORHENIUM: AN OVERVIEW 37 5.2.1 PROPERTIES 37 5.2.2
SYNTHESIS 38 5.3 CATALYTIC APPLICATIONS OF MTO 39 5.3.1
METHYLTRIOXORHENIUM AS A HOMOGENEOUS OXIDATION CATALYST 40 5.3.2
MECHANISTIC IMPLICATIONS IN THE EPOXIDATION REACTION 41 5.3.3
HETEROGENEOUS DERIVATIVES OF MTO 42 5.4 BASE ADDUCTS OF
METHYLTRIOXORHENIUM AND THEIR EFFECT IN EPOXIDATION CATALYSIS43 5.4.1
NITROGEN DONOR ADDUCTS 44 5.4. BIBLIOGRAFISCHE INFORMATIONEN
HTTP://D-NB.INFO/997426489 DIGITALISIERT DURCH 5.4.3 SCHIFF BASES AND
ITS ROLE IN SYNTHESIS AND CATALYSIS 47 6. SYNTHESIS AND CATALYTIC
APPLICATIONS OF MTO SCHIFF BASE COMPLEXES 49 6.1 ABSTRACT 50 6.2 RESULTS
AND DISCUSSION 50 6.2.1 SYNTHESIS AND SPECTROSCOPIC CHARACTERISATION 50
6.2.2 SCHIFF BASE ADDUCTS OF MTO: A COMPARATIVE STUDY OF THEIR STABILITY
56 6.2.3 X-RAY STRUCTURES OF COMPOUNDS 5-10 58 6.2.4 APPLICATION IN
EPOXIDATION CATALYSIS 64 6.3 CONCLUSIONS 66 REFERENCES CITED IN THIS
CHAPTER 68 III. SYNTHESIS AND CATALYTIC APPLICATIONS OF CYCLOPENTADIENYL
MOLYBDENUM AND TUNGSTEN ALKYL COMPOUNDS 73 7. HIGH VALENT ORGANOMETALLIC
OXIDES OF MOLYBDENUM AND TUNGSTEN AS EPOXIDATION CATALYSTS 76 7.1
DIOXOMOLYBDENUM COMPLEXES 77 7.1.1 NON-ORGANOMETALLIC MOLYBDENUM DIOXO
COMPOUNDS. ADDUCTS WITH DONOR LIGANDS 77 7.1.2 ORGANOMETALLIC
DERIVATIVES WITH M-C A BONDS 78 7.1.3 CHIRAL DERIVATIVES 79 7.1.4
APPLICATION IN EPOXIDATION CATALYSIS 80 7.1.5 TUNGSTEN DERIVATIVES 81
7.2 IF-CYCLOPENTADIENYL COMPOUNDS 82 7.2.1 CYCLOPENTADIENYL CARBONYL
METAL DERIVATIVES 83 7.2.2 CYCLOPENTADIENYL OXO-METAL DERIVATIVES 84
7.2.3 CHIRAL DERIVATIVES 85 7.2.4 APPLICATION IN EPOXIDATION CATALYSIS
86 7.2.5 HETEROGENISATION OF CYCLOPENTADIENYL MOLYBDENUM COMPOUNDS.
APPLICATIONS IN IONIC LIQUIDS 87 7.3 MECHANISTIC IMPLICATIONS IN THE
EPOXIDATION REACTION. A COMPARATIVE 87 7.3. 8. KINETIC STUDIES ON THE
OXIDATION OF H^CYCLOPENTADIENYL METHYL TRICARBONYL MOLYBDENUM(II) AND
THE USE OF ITS OXIDATION PRODUCTS AS OLEFIN EPOXIDATION CATALYSTS 92 8.1
ABSTRACT 92 8.2 RESULTS AND DISCUSSION 93 8.2.1 KINETIC STUDIES 94 8.2.2
CATALYTIC EPOXIDATION 100 8.3 CONCLUSIONS 107 9. ANSA COMPOUNDS 108 9.1
CLASSIFICATION 108 9.1.1 ANSA BRIDGED BENT METALLOCENES 109 9.1.2
HETEROATOMIC HALF-SANDWICH ANSA COMPOUNDS. CONSTRAINED GEOMETRY
CATALYSTS 109 9.1.3 M-C ANSA COMPOUNDS 110 9.2 ANSA COMPOUNDS OF MO AND
W AS OXIDATION CATALYSTS 110 10. STABLE AND CATALYTICALLY ACTIVE ANSA
COMPOUNDS WITH CYCLOALKYL MOIETIES AS BRIDGING UNITS 112 10.1 ABSTRACT
113 10.2 RESULTS AND DISCUSSION 113 10.2.1 SYNTHESIS AND
CHARACTERISATION OF THE SPIROLIGANDS 1A-D 113 10.2.2 SYNTHESIS OF THE
ANSA COMPOUNDS 2A-D 114 10.2.3 PROPERTIES AND CHARACTERISATION 117
10.2.4 X-RAY STRUCTURES OF COMPOUNDS 2A, 3A AND 2B 122 10.2.5
APPLICATION IN EPOXIDATION CATALYSIS 126 10.3 CONCLUSIONS 130 11.
CURRENT RESEARCH. NEW ANSA DERIVATIVES 132 11.1 ANSA-C4 COMPOUNDS. DIMER
FORMATION 132 11.2 SYNTHESIS AND CATALYTIC APPLICATIONS OF HIGHLY
ENANTIOSELECTIVE ANSA COMPOUND IV. EXPERIMENTAL SECTION 147 12.
SYNTHESIS AND CATALYTIC APPLICATIONS OF MTO SCHIFF BASE COMPLEXES
(CHAPTER 6) 149 12.1 MATERIALSAND METHODS 149 12.2 SYNTHESIS OF THE
SCHIFF BASE ADDUCTS 149 12.3 X-RAY CRYSTAL DETERMINATION OF COMPOUNDS
5-9 152 12.4 CATALYTIC REACTIONS 153 13. KINETIC STUDIES ON THE
OXIDATION OF TI 5 -CYCLOPENTADIENYL METHYL TRICARBONYL MOLYBDENUM(II)
AND THE USE OF ITS OXIDATION PRODUCTS AS OLEFIN EPOXIDATION CATALYSTS
(CHAPTER 8) 154 13.1 MATERIALSAND METHODS 154 13.2 SYNTHESIS OF CPMO(O 2
)OCH 3 154 13.3 KINETIC STUDIES 155 13.4 CRYSTAL DATA OF COMPOUND 3 156
14. STABLE AND CATALYTICALLY ACTIVE ANSA COMPOUNDS WITH CYCLOALKYL
MOIETIES AS BRIDGING UNITS (CHAPTER 10) 158 14.1 MATERIALS AND METHODS
158 14.2 SYNTHESIS OF THE SPIRO LIGANDS 159 14.3 SYNTHESIS OF THE MO
DERIVATIVES 160 14.4 SYNTHESIS OF THE W DERIVATIVES 162 14.5 APPLICATION
IN EPOXIDATION CATALYSIS 163 14.6 CRYSTAL DATA OF COMPOUND 2A 164 14.6.1
BOND DISTANCES (IN A) 164 14.6.2 BOND ANGLES (IN 0 ) 165 14.7 CRYSTAL
DATA OF COMPOUND 2B 166 14.7.1 BOND DISTANCES (IN A) 166 14.7.2 BOND
ANGLES (IN ) 167 14.8 CRYSTAL DATA OF COMPOUND 3A 168 14.8.1 BOND
DISTANCES (IN A) 168 14.8.2 BOND ANGLES (IN ) 169 14. A.1 : DERIVATION
OF EQUATION 1 177 A.2: DERIVATION OF EQUATION 4 178 APPENDIX B: NMR
SPECTRA OF COMPOUNDS FROM CHAPTER 10 180 B.1 COMPOUNDS 1A-1E 180 B.2
COMPOUNDS 2A-2F 185 B.3 COMPOUNDS 3A-3E 193 APPENDIX C: PUBLICATIONS
RESULTED FROM THIS WORK 198 C. 1 : PUBLICATIONS AS FIRST AUTHOR 198 C.2:
CONTRIBUTIONS TO OTHER PUBLICATIONS 198 C.3: COMMUNICATIONS 199
|
| any_adam_object | 1 |
| author | Capapé Miralles, Alejandro 1979- |
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| dewey-full | 547.215 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 547 - Organic chemistry |
| dewey-raw | 547.215 |
| dewey-search | 547.215 |
| dewey-sort | 3547.215 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik Chemie |
| edition | 1. Aufl. |
| format | Thesis Book |
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| spelling | Capapé Miralles, Alejandro 1979- Verfasser (DE-588)139069119 aut Rhenium, molybdenum and tungsten organometallic homogeneous catalysts synthesis, characterisation and application in olefin epoxidation Alejandro Capapé Miralles 1. Aufl. München Verl. Dr. Hut 2009 199 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Anorganische Chemie Zugl.: München, Techn. Univ., Diss., 2009 Wolframkomplexe (DE-588)4223114-0 gnd rswk-swf Katalytische Oxidation (DE-588)4163425-1 gnd rswk-swf Rheniumkomplexe (DE-588)4223129-2 gnd rswk-swf Epoxidation (DE-588)4152560-7 gnd rswk-swf Molybdänkomplexe (DE-588)4223139-5 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Epoxidation (DE-588)4152560-7 s Katalytische Oxidation (DE-588)4163425-1 s Rheniumkomplexe (DE-588)4223129-2 s Molybdänkomplexe (DE-588)4223139-5 s Wolframkomplexe (DE-588)4223114-0 s DE-604 Erscheint auch als Online-Ausgabe urn:nbn:de:bvb:91-diss-20090804-806954-1-2 http://mediatum.ub.tum.de/node?id=806954 Verlag kostenfrei Volltext https://nbn-resolving.org/urn:nbn:de:bvb:91-diss-20090804-806954-1-2 Resolving-System DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017764614&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Capapé Miralles, Alejandro 1979- Rhenium, molybdenum and tungsten organometallic homogeneous catalysts synthesis, characterisation and application in olefin epoxidation Wolframkomplexe (DE-588)4223114-0 gnd Katalytische Oxidation (DE-588)4163425-1 gnd Rheniumkomplexe (DE-588)4223129-2 gnd Epoxidation (DE-588)4152560-7 gnd Molybdänkomplexe (DE-588)4223139-5 gnd |
| subject_GND | (DE-588)4223114-0 (DE-588)4163425-1 (DE-588)4223129-2 (DE-588)4152560-7 (DE-588)4223139-5 (DE-588)4113937-9 |
| title | Rhenium, molybdenum and tungsten organometallic homogeneous catalysts synthesis, characterisation and application in olefin epoxidation |
| title_auth | Rhenium, molybdenum and tungsten organometallic homogeneous catalysts synthesis, characterisation and application in olefin epoxidation |
| title_exact_search | Rhenium, molybdenum and tungsten organometallic homogeneous catalysts synthesis, characterisation and application in olefin epoxidation |
| title_full | Rhenium, molybdenum and tungsten organometallic homogeneous catalysts synthesis, characterisation and application in olefin epoxidation Alejandro Capapé Miralles |
| title_fullStr | Rhenium, molybdenum and tungsten organometallic homogeneous catalysts synthesis, characterisation and application in olefin epoxidation Alejandro Capapé Miralles |
| title_full_unstemmed | Rhenium, molybdenum and tungsten organometallic homogeneous catalysts synthesis, characterisation and application in olefin epoxidation Alejandro Capapé Miralles |
| title_short | Rhenium, molybdenum and tungsten organometallic homogeneous catalysts |
| title_sort | rhenium molybdenum and tungsten organometallic homogeneous catalysts synthesis characterisation and application in olefin epoxidation |
| title_sub | synthesis, characterisation and application in olefin epoxidation |
| topic | Wolframkomplexe (DE-588)4223114-0 gnd Katalytische Oxidation (DE-588)4163425-1 gnd Rheniumkomplexe (DE-588)4223129-2 gnd Epoxidation (DE-588)4152560-7 gnd Molybdänkomplexe (DE-588)4223139-5 gnd |
| topic_facet | Wolframkomplexe Katalytische Oxidation Rheniumkomplexe Epoxidation Molybdänkomplexe Hochschulschrift |
| url | http://mediatum.ub.tum.de/node?id=806954 https://nbn-resolving.org/urn:nbn:de:bvb:91-diss-20090804-806954-1-2 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017764614&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT capapemirallesalejandro rheniummolybdenumandtungstenorganometallichomogeneouscatalystssynthesischaracterisationandapplicationinolefinepoxidation |