Inorganic experiments:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH
2010
|
| Ausgabe: | 3., rev. ed. |
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | XXVI, 456 S. graph. Darst. |
| ISBN: | 9783527324729 |
Internformat
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Datensatz im Suchindex
| _version_ | 1805092734708482048 |
|---|---|
| adam_text |
Titel: Inorganic experiments
Autor: Woollins, John Derek
Jahr: 2010
Contents
1 Introduction 1
1.1 Introduction 3
J. Derek Woollins
1.2 General Spectroscopic Techniques and Report Writing 5
Petr Kilian
2 Introductory Experiments 23
2.1 Preparation and Investigation of Some Coordination Compounds 25
Manfred Bochmann
2.2 Gravimetric Analysis of Hexaamminenickel(ll) Tetrafluoroborate
[Ni(NH3)6](BF4)2 28
Manfred Bochmann
2.3 Analysis of an Iron(lll) Oxalate Complex 33
Manfred Bochmann
2.4 Characterisation of a Copper Oxalate Complex
K?Cufc (C204)c ? dH20 38
Andrew W. C. Piatt
2.5 Synthesis of [NH4][BF4] and Synthesis and Titrimetric Analysis
of(Zn(NH3)4][BF4]2 40
Michael A. Beckett
2.6 Iron(ll) and Lead(ll) Formates 43
Francisco J. Arndiz, Maria R. Pedrosa, and Rafael Aguado
Inorganic Experiments, Third Edition. Edited by (. Derek Woollins
Copyright £ 2010 WILEY-VCH Verlag GmbH Co. KGaA, Weinheim
ISBN: 978-3-527-32472-9
X I Contents
2.7 Ammonium Dichromate, Chromium(lll) Oxide,
Potassium Chromate and Potassium Tetraperoxochromate(V) 47
Antonin Ruzicka and Zdirad Zdk
2.8 Vanadium Alum: An Experiment in Electrosynthesis 51
David T. Richens
2.9 Linkage Isomerism: An Infra-Red Study 54
David T. Richens and Christopher Clidewell
2.10 Preparation of Copper(l) Iodide 56
F.J. Arndiz, M. R. Pedrosa, and S. Arndiz
2.11 Deduction of the Coordination Mode of BH4 in
Bis(triphenylphosphine) Copper(l) Borohydride (Ph3P)2CuBH4 58
Andrew W. C. Piatt
2.12 Preparation and Identification of a Copper(l) Complex 61
Andrew W. C. Piatt
2.13 Synthesis and Characterisation of a Metal Hydride Complex 63
Andrew W. C. Piatt
2.14 Reactivity of Triphenylphosphine and Its Oxide Towards CuCI2 65
Paul F. Kelly and Martin B. Smith
2.15 Synthesis of a Thermochromic Copper Complex 68
lain A. Smellie 68
2.16 Preparation and Complexation of
Tris(3,5-dimethylpyrazoyl)hydroborate 70
Manfred Bochmann
2.17 Tetraiodotin(IV) and its Triphenylphosphine Complex 73
lain A. Smellie and J. Derek Woollins
2.18 Silicon Oxygen Compounds and Siloxane Polymers 75
Paul D. Lickiss
2.19 Preparation and NMR Identification of Two Phosphorus Esters 79
Christopher Clidewell
Contents I XI
2.20 Synthesis of Triphenylphosphine Oxide and
Triphenylphosphine Sulfide 81
lain Smellie
2.21 Preparation of Sodium Trithionate, Na2S306 and
Potassium Trithionate, K2S306 86
Andrew C. Piatt
2.22 The Preparation of Potassium Peroxodisulfate, K2S208 89
Zdirad Zdk and Antonin Ruiicka
2.23 Polyiodides, Me4Nlx 92
Andrew W. C. Piatt
2.24 Interhalogen Compounds 94
Ivan P. Parkin
2.25 Preparation of K[ICI4] 99
lain Smellie
2.26 Synthesis and Infrared Spectroscopic Characterisation
of Boranes and Germanes 101
Ivan P. Parkin
3 Intermediate Experiments
3.1 Metal Acetylacetonate Complexes:
Preparation and Characterisation 109
Christopher Clidewell
3.2 Nickel Dihalide Phosphine Complexes 120
Ivan P. Parkin
3.3 Nickel(ll) Complexes of Some Schiff Base Ligands 124
Christopher J. Jones
3.4 The Synthesis and Coordination Chemistry
of Macrocyclic Complexes 131
Martin Schroder
3.5 [Co(dinosar)]CI3: An Encapsulation Complex
Prepared by a Template Reaction 136
David J. Otway
XII I Contents
3.6 Identification of Stereochemical (Geometrical) Isomers
of [Mo(CO)4(L)2] by Infrared Spectroscopy 139
Michael A. Beckett
3.7 Five Coordinate Complexes:
rVO(acac)2] and [Cr(NH3)6][CuCI5] 142
Christopher P. Morley
3.8 Preparation of tiwis-PtHCl(PPh3)2 and Measurement
ofits'H,31P and 195PtNMR Spectra 145
William P. Griffith
3.9 [Mo02Br2(H20)2] ? (diglyme) and [Mo02Br2(DMF)2] 149
Francisco J. Arndiz, Maria R. Pedrosa, and Rafael Aguado
3.10 Preparation of an Iron Dinitrogen Complex 153
Andrew W. C. Piatt
3.11 Preparation of NitrosyI Complexes of Iron and Nickel 155
Andrew W. C. Piatt
3.12 Synthesis and Characterisation of Two Metal-Metal Bonded
Dimolybdenum Complexes 158
William Levason, Thomas A. Logothetis, and Cill Reid
3.13 Cobalt Complexes of Dioxygen 167
David T. Richens and Christopher Clidewell
3.14 Ferrocene, (75-C5H5)2Fe, and its Derivatives 170
J. Derek Woollins
3.15 The Use of Organolithium Reagents
in the Preparation of Ferrocene Derivatives 173
Ian R. Butler
3.16 Complexes of ^-Bonding Arene Ligands 280
Andrew W. C. Piatt
3.17 Organotin Chemistry 183
Kieran C. Molloy and Timothy T. Paget
3.18 Transition Metal-Carbon Bonds in Chemistry and Biology 190
Christopher J. Jones
Contents XIII
3.19 Nickel-Catalysed Cross-Coupling of
Alkylmagnesium with Haloarene 201
C. Brent Young
3.20 Transition Metal Catalysis 205
Neil M. Boag
3.21 Nitration of Cobalt(lll) Acetylacetonate 209
David J. Otway
3.22 Phenyllithium and Tetraphenylsilane 211
Petr Kilian
3.23 Synthesis and Reactivity of Tertiary Phosphines 218
Neil M. Boag
3.24 Two-stage Synthesis of Ph2P(0)(CH2)4P(0)Ph2 222
Andrew C. Piatt
3.25 Inorganic Heterocycles: Cyclophosphazenes 226
Josef Novosad and Milan Albert!
3.26 Inorganic (Carbon-Free) Chelate Rings:
A Dithioimidodiphosphinato Ligand and Some of its
Metal Complexes 229
lonel Haiduc
3.27 Inorganic (Carbon-Free) Chelate Rings II:
Asymmetric Mixed-Donor P-N-P Ligand and its
Palladium Complex 234
David J. Birdsall and Josef Novosad
3.28 Amidosulftiric Acid, Trisilveramidosulfate Monohydrate
and S03 ¦ N (CH3)3 Complexes 239
Antonin Ruzicka and Zdirad 2dk
3.29 Anomalous Paramagnetism in Some Iron(lll) Chelates
Studied by the Evans N M R Method 243
David J. Otway
3.30 Cubic Molecular Aluminophosphonates 246
Jiri Pinkas
XIV Contents
3.31 Preparation and Optical Properties of Zinc Sulfide
Quantum Dots 249
Andrew L Hector
3.32 Four Methods for Analysing First Order Kinetics 255
Vironique Pimienta, Dominique Lavabre,
Jean-Claude Micheau, and Gaston Levy
3.33 Molecular Orbital Calculations of Inorganic Compounds 261
Carole A. Morrison, Neil Robertson, Andrew Turner,
Jano van Hemert, and Jos Koetsier
4 Advanced Experiments
4.1 2,2': 6,2' -Terpyridine Complexes and Metal Directed Reactivity 271
Edwin C. Constable
4.2 4-(4-Pyridyl)-2,2':6',2'-terpyridine: Coordination to Iron(ll)
and Protonation Studies 274
Catherine E. Housecroft, Edwin C. Constable, and Emma L Dunphy
4.3 Heteronuclear d-fComplexes Containing Binucleating Ligands 283
Francisco J. Arndiz, Jean-Pierre Costes, and Javier Garcia-Tojal
4.4 Electronic Characterisation of a Transition Metal Complex
Using Electrochemical UV/Vis and EPR Techniques 287
Lesley J. Yellowlees
4.5 Chlorotris(tert-butylimido)manganese(VII) 290
Andreas A. Danopoulos and Geoffrey Wilkinson
4.6 Tetrakisphosphorane Imirtato Complexes of Transition Metals 293
Kurt Dehnicke
4.7 Magnetochemistry Experiments:
Exchange Coupling in Copper(ll)-Nickel(ll) Bimetallic Complexes
and Spin Transition in Iron Complexes 297
Eugenia Coronado and J. J. Borrds-Almenar
Contents XV
4.8 Metal-Containing Liquid Crystals.
The Synthesis of trons-bis(4-Alkyl-4'-cyano-
l,l'-biphenyl)dichloroplatinum(ll) and Related Species -
The Use of Melt Syntheses 301
Duncan W. Bruce
4.9 Structural, Electrical and Magnetic Properties
of Perovskite Ceramics 309
Colin Greaves
4.10 Polyoxomolybdate Clusters: Nanoscopic Wheels and Balls 315
Leroy Cronin, Ekkehard Diemann, and Achim Muller
4.11 Reaction of Alkali Metal Polyselenides and Polytellurides
with Group 6 Metal Carbonyls 322
Joseph W. Kolis
4.12 Chlorothionitrene and Cyclothiazeno Complexes of Tungsten 327
Kurt Dehnicke
4.13 Sulfur-Rich Homocycles and Heterocycles:
Titanocene Pentasulfide, cyc/o-Heptasulfiir and
1,2,3,4,5,6,7-Heptathionane 330
Jorg Albertsen and RalfSteudel
4.14 N-Ferrocenyl Amine and Some Reactive Derivatives 334
Max Herberhold, Heidi E. Maisel, and Bernd Wrackmeyer
4.15 1,1 '-Bis(trimethylsilylamino)ferrocene -
A Useful Precursor to 1 ,n-Diaza-[n)ferrocenophanes 341
Max Herberhold, Elena V. Klimkina, and Bernd Wrackmeyer
4.16 Organometallic Molybdenum Compounds 353
Manfred Bochmann and Petr Klian
4.17 Migratory Insertion Reactions
in Organo Transition-Metal Chemistry 364
MarkJ. Winter
4.18 A Transition-Metal Alkylidyne Complex 369
Stephen Anderson, Darren Cook, and Anthony F. Hill
XVI Contents
4.19 The Synthesis of i/6-Arenetricarbonyl Chromium(O) Complexes 372
David A. Widdowson
4.20 Preparation of the Iron Tricarbonyl Complex
of Methyl-ZrAcetamidoacrylate 3 75
M. Elena Lasterra-Sanchez and Susan E. Gibson
4.21 Halfsandwich Carbonyl Vanadium Complexes 377
Max Herberhold and Matthias Schrepfermann
4.22 Covalent and Ionic Metallocene Hexafluoroarsenate Complexes 383
Inis C. Tornieporth-Oetting and Thomas M. Klapotke
4.23 The Preparation of rac-Ethylene-1,2-bis(l-indenyl)zirconium
Dichloride and Dibenzyl Complexes 386
Manfred Bochmann and Simon J. Lancaster
4.24 One-Pot Preparation of Ru3(CO)12 from RuCI3 ? 3 H20 391
Guy Lavigne, Catherine Saccavini, and Remi Chauvin
4.25 Synthesis of Well-defined Organometallic Hydroxides:
[LCaOH]2, LAI(Me)OH and LGeOH 396
Herbert W. Roesky
4.26 Alumazene- Inorganic Benzene Analogue 402
Jiri Pinkas
4.27 Preparation of [Bu4N][B3Hg] and the Formation of
RuH[B3Hg](CO){PPh3)2 405
Anthony F. Hill and J. Derek Woollins
4.28 Vacuum Line Techniques: Preparation of SiF4 and SiF4(C5H5N)2 409
J. Derek Woollins
4.29 Amino- and Nitrotetrazoles: Nitrogen-rich Heterocycles 413
Davin G. Piercey and Thomas M. Klapotke
4.30 Ammonium 5-Nitro-lH-Tetrazolate-Hemihydrate 417
Franz Xaver Steemann and Thomas M. Klapotke
4.31 Arsenium Cations: Carbene Analogues 420
Neil Burford and Trenton M. Parks
Contents XVII
4.32 Preparation and Structure of the Acetyl Chloride-Antimony
Pentachloride Complex 425
Peter N. Gates
4.33 Preparation and Some Reactions of the Folded P2N4S2 Ring 428
Tristram Chivers, Daniel D. Doxsee, and Robert W. Hilts
4.34 Sulfur-Nitrogen Heterocycles and [SNBr0.4]* Polymer 432
J. Derek Woollins
4.35 Selenium-Nitrogen and Tellurium-Nitrogen Compounds 436
Herbert W. Roesky and Judith Gindl
4.36 Nitride Chlorides of Selenium(lll) and Selenium(IV):
SezNCU and Se2NCI5 440
Kurt Dehnicke
4.37 The Synthesis and Ring-Opening Polymerisation Behaviour
of a [l]Silaferrocenophane 444
Ian Manners
Index 447 |
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| discipline | Chemie / Pharmazie Chemie |
| edition | 3., rev. ed. |
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| id | DE-604.BV035660377 |
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| indexdate | 2024-07-20T10:16:18Z |
| institution | BVB |
| isbn | 9783527324729 |
| language | English |
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| spelling | Inorganic experiments ed. by J. Derek Woollins 3., rev. ed. Weinheim Wiley-VCH 2010 XXVI, 456 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chemistry, Inorganic Experiments Anorganische Chemie (DE-588)4002145-2 gnd rswk-swf (DE-588)4127380-1 Praktikum gnd-content Anorganische Chemie (DE-588)4002145-2 s DE-604 Woollins, J. Derek Sonstige oth text/html http://deposit.dnb.de/cgi-bin/dokserv?id=3294492&prov=M&dok_var=1&dok_ext=htm Inhaltstext HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017714809&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
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| subject_GND | (DE-588)4002145-2 (DE-588)4127380-1 |
| title | Inorganic experiments |
| title_auth | Inorganic experiments |
| title_exact_search | Inorganic experiments |
| title_full | Inorganic experiments ed. by J. Derek Woollins |
| title_fullStr | Inorganic experiments ed. by J. Derek Woollins |
| title_full_unstemmed | Inorganic experiments ed. by J. Derek Woollins |
| title_short | Inorganic experiments |
| title_sort | inorganic experiments |
| topic | Chemistry, Inorganic Experiments Anorganische Chemie (DE-588)4002145-2 gnd |
| topic_facet | Chemistry, Inorganic Experiments Anorganische Chemie Praktikum |
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