Determination of droplet surface temperature and drying kinetics of protein solutions using an ultrasonic levitator:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Aachen
Shaker
2009
|
| Schriftenreihe: | Monographs in pharmaceutics
10 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | VIII, 197 S. Ill., graph. Darst. 21 cm |
| ISBN: | 9783832282967 |
Internformat
MARC
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| 245 | 1 | 0 | |a Determination of droplet surface temperature and drying kinetics of protein solutions using an ultrasonic levitator |c Eva Cornelia Wulsten |
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Datensatz im Suchindex
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| adam_text | 3.4.1 INNER ACOUSTIC STREAMING 29 CONTENTS I TABLE OF CONTENTS 1
INTRODUCTION................................. 1 2 SINIZLC DRODLET
DRVINI? ................................ ..
.................................................... 4 2.1 A SHORT
HISTORY OF SINGLE DROPLET DRYING 4 2.2 HEAT TRANSFER 6 2.2.1 CONDUCTIVE
HEAT TRANSFER 6 2.2.2 CONVECTIVE HEAT TRANSFER 6 2.2.3 RADIATIVE HEAT
TRANSFER 7 2.3 DIFFUSION 11 2.3.1 FICK S FIRST LAW OF DIFFUSION 12 2.3.2
DIFFUSION COEFFICIENTS FOR GASES 12 2.3.3 CONVECTIVE MASS TRANSFER 13
2.4 MASS TRANSFER THEORIES 13 2.5 EVAPORATION OF PURE SOLVENT DROPLETS
14 2.5.1 EVAPORATION OF A SINGLE DROPLET 14 2.5.2 THEDMAW 15 2.5.3
DIFFUSION-CONTROLLED EVAPORATION OF SINGLE DROPLETS 16 2.5.4 EVAPORATION
OF DROPLETS CONTAINING SOLVENT MIXTURES 16 2.6 EVAPORATION OF SOLUTION
AND SUSPENSION DROPLETS 17 2.6.1 DRYING STAGES OF SOLUTION AND
SUSPENSION DROPLETS 17 2.6.2 PARTICLE FORMATION 20 2.6.3 MODELS FOR THE
DRYING OF SINGLE DROPLETS CONTAINING SOLIDS 22 3 ACOUSTIC ICVITAETION
*.....*......*........****.**.**.................»..****...*...»...*..*..*....».*....*
24 3.1 HISTORY AND APPLICATION OF ACOUSTIC LEVITATION 24 3.2 A SHORT
INTRODUCTION TO ACOUSTICS 25 3.3 LEVITATION FORCES 27 3.3.1 STANDING
ACOUSTIC WAVE 27 3.3.2 INTERACTION OF ULTRASONIC WAVE AND DROPLET 28 3.4
ACOUSTIC STREAMING 29 BIBLIOGRAFISCHE INFORMATIONEN
HTTP://D-NB.INFO/995049580 DIGITALISIERT DURCH 5.2.1 EVAPORATION OF PURE
WATER DROPLETS 67 II CONTENTS 3.4.2 OUTER ACOUSTIC STREAMING 30 3.5
VERTICAL POSITION OF THE LEVITATED DROPLET 31 3.6 TEMPERATURE OF THE
LEVITATION SYSTEM 32 3.7 SINGLE DROPLET DRYING USING AN ACOUSTIC
LEVITATOR 32 3.7.1 PURE SOLVENT DROPLETS 32 3.7.2 SOLUTION AND
SUSPENSION DROPLETS 35 4 MATERIALS AND METHODS 37 4.1 MATERIALS 37 4.1.1
PROTEINS 37 4.1.1.1 CARBONIC ANHYDRASE 37 4.1.1.2 L-LACTIC DEHYDROGENASE
39 4.1.1.3 TRYPSINOGEN AND TRYPSIN 40 4.1.2 ITRACONAZOLE 41 4.1.3
EXCIPIENTS AND REAGENTS 42 4.2 METHODS 44 4.2.1 ACOUSTIC LEVITATION 44
4.2.2 MICRODISPENSING SYSTEM 48 4.2.3 DROPLET SIZE MEASUREMENTS 51 4.2.4
DROPLET SURFACE TEMPERATURE MEASUREMENTS 51 4.2.5 SPRAY DRYING 52 4.2.6
SCANNING ELECTRON MICROSCOPY 53 4.2.7 ENZYME ACTIVITY ASSAY OF CARBONIC
ANHYDRASE 53 4.2.8 ENZYME ACTIVITY ASSAY OF L-LACTIC DEHYDROGENASE 54
4.2.9 ENZYME ACTIVITY ASSAY OF TRYPSINOGEN 55 5 RESULTS AND DISCUSSION
57 5. 1 PRELIMINARY EXPERIMENTS USING THE IR-CAMERA 57 5.1.1 HEATING-UP
OF THE LEVITATION SYSTEM 57 5.1.2 INFLUENCE OF DROPLET SIZE ON THE
SURFACE TEMPERATURE MEASUREMENT 58 5.1.3 DETERMINATION OF EMISSIVITIES
64 5.2 EVAPORATION OF PURE SOLVENT DROPLETS 67 8 REFERENCES 188 CONTENTS
IH 5.2.1.1 INFLUENCES OF THE INITIAL DROPLET SIZE ON THE EVAPORATION
PROCESS 67 5.2.1.2 INFLUENCE OF THE DRYING AIR STREAM ON THE EVAPORATION
PROCESS 84 5.2.2 EVAPORATION OF PURE ORGANIC SOLVENT DROPLETS 96 5.2.3
EVAPORATION OF DROPLETS CONTAINING SOLVENT MIXTURES 103 5.3 EVAPORATION
OF EXCIPIENT SOLUTION DROPLETS 110 5.3.1 TREHALOSE SOLUTION DROPLETS 110
5.3.2 MANNITOL SOLUTION DROPLETS 121 5.3.3 SUCROSE SOLUTION DROPLETS 133
5.3.4 COPOLYVIDONE AND HPMC SOLUTION DROPLETS 136 5.4 ITRACONAZOLE
FORMULATION EXPERIMENTS 141 5.5 DRYING OF PROTEIN SOLUTIONS 148 5.5.1
BOVINE CARBONIC ANHYDRASE (BCA) DROPLETS 148 5.5.1.1 BCA-TREHALOSE 10
%(W/V) TOTAL SOLIDS FORMULATIONS 151 5.5.1.2 BCA 10 %(W/V) PLUS
TREHALOSE FORMULATIONS 157 5.5.2 L-LACTIC DEHYDROGENASE (LDH) DROPLETS
161 5.5.2.1 LDH-TREHALOSE 10 % (W/V) TOTAL SOLIDS FORMULATIONS 163
5.5.2.2 LDH 10 % (W/V) PLUS TREHALOSE FORMULATIONS 170 5.5.3 TRYPSINOGEN
DROPLETS 174 6 SUMMARY AND CONCLUSIONS 177 7 ZUSAMMENFASSUNG 182
|
| any_adam_object | 1 |
| author | Wulsten, Eva Cornelia 1979- |
| author_GND | (DE-588)138700265 |
| author_facet | Wulsten, Eva Cornelia 1979- |
| author_role | aut |
| author_sort | Wulsten, Eva Cornelia 1979- |
| author_variant | e c w ec ecw |
| building | Verbundindex |
| bvnumber | BV035651030 |
| ctrlnum | (OCoLC)458692957 (DE-599)DNB995049580 |
| dewey-full | 615.19 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 615 - Pharmacology and therapeutics |
| dewey-raw | 615.19 |
| dewey-search | 615.19 |
| dewey-sort | 3615.19 |
| dewey-tens | 610 - Medicine and health |
| discipline | Medizin |
| format | Thesis Book |
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| genre_facet | Hochschulschrift |
| id | DE-604.BV035651030 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T21:42:28Z |
| institution | BVB |
| isbn | 9783832282967 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-017705627 |
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| owner | DE-29 DE-29T |
| owner_facet | DE-29 DE-29T |
| physical | VIII, 197 S. Ill., graph. Darst. 21 cm |
| publishDate | 2009 |
| publishDateSearch | 2009 |
| publishDateSort | 2009 |
| publisher | Shaker |
| record_format | marc |
| series | Monographs in pharmaceutics |
| series2 | Monographs in pharmaceutics |
| spelling | Wulsten, Eva Cornelia 1979- Verfasser (DE-588)138700265 aut Determination of droplet surface temperature and drying kinetics of protein solutions using an ultrasonic levitator Eva Cornelia Wulsten Aachen Shaker 2009 VIII, 197 S. Ill., graph. Darst. 21 cm txt rdacontent n rdamedia nc rdacarrier Monographs in pharmaceutics 10 Zugl.: Erlangen-Nürnberg, Univ., Diss., 2009 Lösungsmittel - Tropfen - Verdampfungstrocknung - Schweben - Ultraschall Lösungsmittel - Wirkstoff - Tropfen - Verdampfungstrocknung - Schweben - Ultraschall Pharmazeutischer Hilfsstoff - Lösung - Tropfen - Verdampfungstrocknung - Schweben - Ultraschall Schweben (DE-588)4264210-3 gnd rswk-swf Lösungsmittel (DE-588)4036160-3 gnd rswk-swf Lösung Chemie (DE-588)4036159-7 gnd rswk-swf Ultraschall (DE-588)4061555-8 gnd rswk-swf Pharmazeutischer Hilfsstoff (DE-588)4137744-8 gnd rswk-swf Verdampfungstrocknung (DE-588)4395982-9 gnd rswk-swf Wirkstoff (DE-588)4066383-8 gnd rswk-swf Tropfen (DE-588)4130676-4 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Lösungsmittel (DE-588)4036160-3 s Tropfen (DE-588)4130676-4 s Verdampfungstrocknung (DE-588)4395982-9 s Schweben (DE-588)4264210-3 s Ultraschall (DE-588)4061555-8 s DE-604 Pharmazeutischer Hilfsstoff (DE-588)4137744-8 s Lösung Chemie (DE-588)4036159-7 s Wirkstoff (DE-588)4066383-8 s Monographs in pharmaceutics 10 (DE-604)BV020836677 10 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017705627&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Wulsten, Eva Cornelia 1979- Determination of droplet surface temperature and drying kinetics of protein solutions using an ultrasonic levitator Monographs in pharmaceutics Lösungsmittel - Tropfen - Verdampfungstrocknung - Schweben - Ultraschall Lösungsmittel - Wirkstoff - Tropfen - Verdampfungstrocknung - Schweben - Ultraschall Pharmazeutischer Hilfsstoff - Lösung - Tropfen - Verdampfungstrocknung - Schweben - Ultraschall Schweben (DE-588)4264210-3 gnd Lösungsmittel (DE-588)4036160-3 gnd Lösung Chemie (DE-588)4036159-7 gnd Ultraschall (DE-588)4061555-8 gnd Pharmazeutischer Hilfsstoff (DE-588)4137744-8 gnd Verdampfungstrocknung (DE-588)4395982-9 gnd Wirkstoff (DE-588)4066383-8 gnd Tropfen (DE-588)4130676-4 gnd |
| subject_GND | (DE-588)4264210-3 (DE-588)4036160-3 (DE-588)4036159-7 (DE-588)4061555-8 (DE-588)4137744-8 (DE-588)4395982-9 (DE-588)4066383-8 (DE-588)4130676-4 (DE-588)4113937-9 |
| title | Determination of droplet surface temperature and drying kinetics of protein solutions using an ultrasonic levitator |
| title_auth | Determination of droplet surface temperature and drying kinetics of protein solutions using an ultrasonic levitator |
| title_exact_search | Determination of droplet surface temperature and drying kinetics of protein solutions using an ultrasonic levitator |
| title_full | Determination of droplet surface temperature and drying kinetics of protein solutions using an ultrasonic levitator Eva Cornelia Wulsten |
| title_fullStr | Determination of droplet surface temperature and drying kinetics of protein solutions using an ultrasonic levitator Eva Cornelia Wulsten |
| title_full_unstemmed | Determination of droplet surface temperature and drying kinetics of protein solutions using an ultrasonic levitator Eva Cornelia Wulsten |
| title_short | Determination of droplet surface temperature and drying kinetics of protein solutions using an ultrasonic levitator |
| title_sort | determination of droplet surface temperature and drying kinetics of protein solutions using an ultrasonic levitator |
| topic | Lösungsmittel - Tropfen - Verdampfungstrocknung - Schweben - Ultraschall Lösungsmittel - Wirkstoff - Tropfen - Verdampfungstrocknung - Schweben - Ultraschall Pharmazeutischer Hilfsstoff - Lösung - Tropfen - Verdampfungstrocknung - Schweben - Ultraschall Schweben (DE-588)4264210-3 gnd Lösungsmittel (DE-588)4036160-3 gnd Lösung Chemie (DE-588)4036159-7 gnd Ultraschall (DE-588)4061555-8 gnd Pharmazeutischer Hilfsstoff (DE-588)4137744-8 gnd Verdampfungstrocknung (DE-588)4395982-9 gnd Wirkstoff (DE-588)4066383-8 gnd Tropfen (DE-588)4130676-4 gnd |
| topic_facet | Lösungsmittel - Tropfen - Verdampfungstrocknung - Schweben - Ultraschall Lösungsmittel - Wirkstoff - Tropfen - Verdampfungstrocknung - Schweben - Ultraschall Pharmazeutischer Hilfsstoff - Lösung - Tropfen - Verdampfungstrocknung - Schweben - Ultraschall Schweben Lösungsmittel Lösung Chemie Ultraschall Pharmazeutischer Hilfsstoff Verdampfungstrocknung Wirkstoff Tropfen Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017705627&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV020836677 |
| work_keys_str_mv | AT wulstenevacornelia determinationofdropletsurfacetemperatureanddryingkineticsofproteinsolutionsusinganultrasoniclevitator |