A nonlinear frequency response method for estimation of single solute and competitive adsorption isotherms:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Magdeburg
Docupoint-Verl.
2008
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| Ausgabe: | 1. Aufl. |
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | XII, 179 S. graph. Darst. 21 cm |
| ISBN: | 9783939665960 |
Internformat
MARC
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| 502 | |a Zugl.: Magdeburg, Univ., Diss., 2008 | ||
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Datensatz im Suchindex
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CONTENTS CONTENTS LIST OF SYMBOLS IX 1 INTRODUCTION 1 1.1 ADSORPTION
CQUILIBRIUM 1 1.2 NONLINEAR SYSTEM ANALYSIS 2 1.3 APPLICATION OF THE
FREQUENCY RESPONSE METHODS IN CHEMICAL ENGINEERING 3 1.4
OBJECTIVESANDLAYOUTOFTHE WORK 5 2 ADSORPTION ISOTHERMS AND
CHROMATOGRAPHY 7 2.1 ADSORPTION ISOTHERMS 7 2.1.1 MODELS OF SINGLE
SOLUTE ISOTHERMS IN LIQUID-SOLID EQUILIBRIUM 9 2.1.2 COMPETITIVE
ADSORPTION ISOTHERM MODEIS 10 2.1.2.1 IDEAL ADSORBED SOLUTION THEORY 10
2.1.2.2 REAL ADSORBED SOLUTION THEORY 12 2.2 MODELINGOF CHROMATOGRAPHIE
PROCESSES 13 2.2.1 EQUILIBRIUM THEORY 13 2.2.2 EQUILIBRIUM-DISPERSIVE
MODEL 14 2.2.3 INITIAL AND BOUNDARY CONDITIONS 15 2.3 DETERMINATION OF
ADSORPTION ISOTHERMS 15 2.3.1 STATIC METHODS 17 2.3.2 DYNAMIC METHODS 18
2.4 SUMMARY 25 3 HIGHER ORDER FREQUENCY RESPONSE FUNETIONS OF A
CHROMATOGRAPHIE COLUMN 26 3.1 CONCEPT OF HIGHER ORDER FREQUENCY RESPONSE
FUNETIONS 26 3.1.1 SINGLE-INPUT VOLTERRA SERIES 27 3.1.2 FREQUENCY
RESPONSE OF A NONLINEAR SYSTEM 30 3.1.3 MULTI-INPUT VOLTERRA SERIES 32
3.1.4 HARMONIE PROBING METHOD 34 3.2 DERIVATION OF THE FRFS FOR THE
ADSORPTION OF A BINARY MIXTURE 35 BIBLIOGRAFISCHE INFORMATIONEN
HTTP://D-NB.INFO/991687744 DIGITALISIERT DURCH CONTENTS 3.2.1 DEFINITION
AND PROCEDURE DESCRIPTION 36 3.2.2 FIRST ORDER FRFS 39 3.2.3 SECOND
ORDER FRFS 41 3.2.4 THIRD ORDER FRFS 44 3.3 COMPARISON OF THE FRFS FOR
DIFFERENT INLET CONCENTRATION CHANGES 49 3.4 SUMMARY 53 NONLINEAR
FREQUENCY RESPONSE METHOD FOR ESTIMATION OF ADSORPTION ISOTHERMS 54 4.1
ESTIMATION OF SINGLE SOLUTE ADSORPTION ISOTHERM INFORMATION 54 4.2
ESTIMATION OF COMPETITIVE ADSORPTION ISOTHERM INFORMATION 55 4.2.1
CONCENTRATION CHANGE OF THE COMPONENT 1 AT THE INLET 56 4.2.2
CONCENTRATION CHANGE OF THE COMPONENT 2 AT THE INLET 58 4.2.3
CONCENTRATION CHANGE OF BOTH COMPONENTS AT THE INLET 60 4.3 ANALYSIS OF
THE THEORETICAL FRFS FOR THE ADSORPTION OF A SINGLE SOLUTE 63 4.3.1
DEFINITION OF DIMENSIONLESS GROUPS USED FOR UNIFIED REPRESENTATION OF
THE FRFS 65 4.3.2 NORMALIZED FRF FIRST ORDER DERIVATIVES AND NORMALIZED
RATIO OF THE FRFS AND THE CORRESPONDING FREQUENCIES 66 4.3.3 INFLUENCE
OF THE NUMBER OF THEORETICAL PLATES 67 4.3.4 INFLUENCE OF THE
STEADY-STATE CONCENTRATIONS 69 4.3.5 ERROR ANALYSIS OF THE ESTIMATED
DIMENSIONLESS ISOTHERM COEFFICIENTS 70 4.4 ANALYSIS OF THE THEORETICAL
FRFS FOR THE ADSORPTION OF A BINARY MIXTURE 72 4.4.1 FRFS CALCULATED FOR
DIFFERENT STEADY-STATE CONCENTRATIONS AND THE SAME RELATIVE MIXTURE
COMPOSITION OF 1:1 73 4.4.2 FRFS CALCULATED FOR DIFFERENT MIXTURE
COMPOSITIONS 1 :X 76 4.4.3 FRFS CALCULATED FOR DIFFERENT MIXTURE
COMPOSITIONS X:L 78 4.4. CONTENTS 5 SIMULATIONS OF THE FREQUENCY
RESPONSE OF A CHROMATOGRAPHIE COLUMN 89 5.1 NUMERICAL METHOD USED FOR
SIMULATIONS 89 5.2 ESTIMATION OF THE FRFS FROM INLET AND OUTLET
CONCENTRATION CHANGES 90 5.2.1 HARMONIE ANALYSIS OF COMPLEX PERIODIC
SIGNALS 91 5.2.2 ESTIMATION OF THE FRFS FROM ONE AND MORE EXCITATION
AMPLITUDES 91 5.3 FR OF A CHROMATOGRAPHIE COLUMN FOR THE ADSORPTION OF A
SINGLE SOLUTE 93 5.3.1 ANALYSIS OF DATA SIMULATED FOR DIFFERENT
EXCITATION AMPLITUDES 94 5.3.2 ESTIMATION OF THE COEFFICIENTS FROM
DIFFERENT EXCITATION AMPLITUDES 95 5.4 SENSITIVITY OF THE METHOD
ILLUSTRATED FOR SINGLE SOLUTE ADSORPTION 99 5.4.1 NUMBER OF ANALYZED
POINTS 99 5.4.2 SHAPE OF THE INPUT FUNETION 100 5.4.3 VELOCITY
FLUETUATIONS 102 5.4.4 NOISE 102 5.5 FR OF A CHROMATOGRAPHIE COLUMN FOR
THE ADSORPTION OF A BINARY MIXTURE 104 5.5.1 DIFFERENT INLET
CONCENTRATION CHANGES 104 5.5.2 DIFFERENT STEADY-STATE CONCENTRATIONS
107 5.5.3 DIFFERENT RELATIVE MIXTURE COMPOSITIONS 109 5.6 SUMMARY 111 6
EXPERIMENTALPART 112 6.1 DESCRIPTION OF THE EXPERIMENTAL SETUP AND
INVESTIGATED SYSTEMS 112 6.1.1 CHEMICALS 112 6.1.2 COLUMNS 114 6.1.3
EXPERIMENTAL SETUP 116 6.2 PROCEDURES FOR DIFFERENT TYPES OF EXPERIMENTS
118 6.2.1 EXPERIMENTS FOR ESTIMATION OF THE INITIAL SLOPE OF AN
ADSORPTION ISOTHERM . 118 6.2.2 EXPERIMENTS FOR ESTIMATION OF THE
CRITICAL FREQUENCY 118 6.2.3 EXPERIMENTS FOR ESTIMATION OF ADSORPTION
ISOTHERMS BY CLASSICAL METHODS. 120 6.2.3. YNI CONTENTS 6.2.4.3
PERIODICA! EXPERIMENTS FOR A BINARY MIXTURE 126 6.3 ESTIMATION OF SINGLE
SOLUTE ADSORPTION ISOTHERMS 128 6.3.1 FRONTAL ANALYSIS 128 6.3.2
NONLINEAR FR METHOD 131 6.3.3 COMPARISON OF SINGLE SOLUTE ISOTHERMS
ESTIMATED BY DIFFERENT METHODS 139 6.4 ESTIMATION OF COMPETITIVE
ADSORPTION ISOTHERMS 142 6.4.1 PERTURBATION METHOD 142 6.4.2 NONLINEAR
FR METHOD 143 6.4.3 COMPARISON OF COMPETITIVE ISOTHERMS OBTAINED USING
DIFFERENT METHODS 149 6.5 SUMMARY 150 7 CONCLUSIONS AND OUTLOOK 151
APPENDIX 154 A FRFS FOR THE ADSORPTION OFA SINGLE SOLUTE 154 B
INTEGRATION CONSTANTS OF THE FRFS FOR THE ADSORPTION OF A BINARY MIXTURE
156 C EXPERIMENTALLY ESTIMATED FRFS FOR THE ADSORPTION OF A BINARY
MIXTURE 167 BIBLIOGRAPHY 172 |
| any_adam_object | 1 |
| author | Ilić, Milica 1979- |
| author_GND | (DE-588)137184107 |
| author_facet | Ilić, Milica 1979- |
| author_role | aut |
| author_sort | Ilić, Milica 1979- |
| author_variant | m i mi |
| building | Verbundindex |
| bvnumber | BV035640451 |
| ctrlnum | (OCoLC)362799622 (DE-599)DNB991687744 |
| dewey-full | 660.284201519544 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering |
| dewey-raw | 660.284201519544 |
| dewey-search | 660.284201519544 |
| dewey-sort | 3660.284201519544 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie |
| edition | 1. Aufl. |
| format | Thesis Book |
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| spelling | Ilić, Milica 1979- Verfasser (DE-588)137184107 aut A nonlinear frequency response method for estimation of single solute and competitive adsorption isotherms von Milica Ilić 1. Aufl. Magdeburg Docupoint-Verl. 2008 XII, 179 S. graph. Darst. 21 cm txt rdacontent n rdamedia nc rdacarrier Zugl.: Magdeburg, Univ., Diss., 2008 Adsorptionsisotherme (DE-588)4327003-7 gnd rswk-swf Chromatographiesäule (DE-588)4290388-9 gnd rswk-swf Nichtlineares Phänomen (DE-588)4136065-5 gnd rswk-swf Frequenzgang (DE-588)4155400-0 gnd rswk-swf Parameterschätzung (DE-588)4044614-1 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Chromatographiesäule (DE-588)4290388-9 s Adsorptionsisotherme (DE-588)4327003-7 s Parameterschätzung (DE-588)4044614-1 s Frequenzgang (DE-588)4155400-0 s Nichtlineares Phänomen (DE-588)4136065-5 s DE-604 text/html http://deposit.dnb.de/cgi-bin/dokserv?id=3192977&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017695250&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Ilić, Milica 1979- A nonlinear frequency response method for estimation of single solute and competitive adsorption isotherms Adsorptionsisotherme (DE-588)4327003-7 gnd Chromatographiesäule (DE-588)4290388-9 gnd Nichtlineares Phänomen (DE-588)4136065-5 gnd Frequenzgang (DE-588)4155400-0 gnd Parameterschätzung (DE-588)4044614-1 gnd |
| subject_GND | (DE-588)4327003-7 (DE-588)4290388-9 (DE-588)4136065-5 (DE-588)4155400-0 (DE-588)4044614-1 (DE-588)4113937-9 |
| title | A nonlinear frequency response method for estimation of single solute and competitive adsorption isotherms |
| title_auth | A nonlinear frequency response method for estimation of single solute and competitive adsorption isotherms |
| title_exact_search | A nonlinear frequency response method for estimation of single solute and competitive adsorption isotherms |
| title_full | A nonlinear frequency response method for estimation of single solute and competitive adsorption isotherms von Milica Ilić |
| title_fullStr | A nonlinear frequency response method for estimation of single solute and competitive adsorption isotherms von Milica Ilić |
| title_full_unstemmed | A nonlinear frequency response method for estimation of single solute and competitive adsorption isotherms von Milica Ilić |
| title_short | A nonlinear frequency response method for estimation of single solute and competitive adsorption isotherms |
| title_sort | a nonlinear frequency response method for estimation of single solute and competitive adsorption isotherms |
| topic | Adsorptionsisotherme (DE-588)4327003-7 gnd Chromatographiesäule (DE-588)4290388-9 gnd Nichtlineares Phänomen (DE-588)4136065-5 gnd Frequenzgang (DE-588)4155400-0 gnd Parameterschätzung (DE-588)4044614-1 gnd |
| topic_facet | Adsorptionsisotherme Chromatographiesäule Nichtlineares Phänomen Frequenzgang Parameterschätzung Hochschulschrift |
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