Handbook of surface plasmon resonance:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Cambridge
RSC Publ.
2008
|
| Ausgabe: | Reprinted |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis Klappentext |
| Beschreibung: | XXI, 403 S. Ill., graph. Darst. |
| ISBN: | 9780854042678 0854042679 |
Internformat
MARC
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| 245 | 1 | 0 | |a Handbook of surface plasmon resonance |c ed. by R. B. M. Schasfoort ... |
| 250 | |a Reprinted | ||
| 264 | 1 | |a Cambridge |b RSC Publ. |c 2008 | |
| 300 | |a XXI, 403 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
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Datensatz im Suchindex
| _version_ | 1804139261851598848 |
|---|---|
| adam_text | Contents
Chapter
1
Introduction to Surface Plasmon Resonance
Anna J. Tudos and Richard B.M. Schasfoort
1.1
What is Surface Plasmon Resonance?
1
1.1.1
A Simple Experiment
1
1.1.2
From Dip to Real-time Measurement
2
1.2
How to Construct an SPR Assay?
3
1.2.1
The Steps of an Assay
4
1.2.2
Calibration Curve
6
1.2.3
Determination of Kinetic Parameters
7
1.2.4
Basics of Instrumentation
8
1.3
History of SPR Biosensors
9
1.3.1
Early History of SPR Biosensors
9
1.3.2
History of SPR Biosensors After
1990 11
1.4
How to Read This Book
12
1.5
Questions
13
References
13
Chapter
2
Physics of Surface Plasmon Resonance
Rob P.H. Kooyman
2.1
Introduction
15
2.2
The Evanescent Wave
16
2.3
Surface Plasmons
17
2.3.1
Surface Plasmon Dispersion Equations,
Resonance
17
2.3.2
Excitation of Surface Plasmons
19
2.3.3
Surface Plasmon Properties
21
2.3.4
Choice of Experimental Parameters
26
2.4
Analysis of Multi-layered Systems
27
2.5
SPR Spectroscopy
28
2.5.1
Enhancement of Fluorescence and Absorbance
28
2.5.2
SPR and Metal Nanoparticles
29
2.6
Concluding Remarks
31
xiv
Contents
2.7
Questions
32
2.8
Symbols
32
References
33
Chapter
3
SPR Instrumentation
Richard B.M. Schasfoort and Alan McWhirter
3.1
Introduction
35
3.1.1
From Surface Plasmon to SPR Signal
35
3.2
SPR Optics
38
3.2.1
Fan-shaped Beam
39
3.2.2
Fixed Angle
40
3.2.3
Angle Scanning
40
3.2.4
Grating Coupler
41
3.2.5
Other Optical Systems
42
3.2.6
SPR Imaging Instruments
43
3.2.7
General Optical Requirements
for SPR Instruments
44
3.3
SPR Liquid Handling Systems
45
3.3.1
Flow Cell Systems
45
3.3.2
Cuvette Systems
48
3.4
SPR Instruments: State of the Art
50
3.4.1
Examples of Fan-shaped Beam
SPR Instruments
50
3.4.2
Examples of Fixed-angle SPR Instruments
54
3.4.3
Examples of Angle Scanning SPR Instruments
59
3.4.4
Examples of Grating Coupler SPR Instruments
60
3.4.5
Examples of Other SPR Instruments
60
3.4.6
Examples of SPR Imaging Instruments
63
3.5
Protein Interaction Analysis Systems of Biacore
69
3.5.1
Introduction
69
3.5.2
Biacore T100
70
3.5.3
Biacore A100
73
3.5.4
FLEXChip
75
3.6
Conclusion
77
3.7
Questions
78
References
78
Chapter
4
Kinetic Models Describing Biomolecular Interactions
at Surfaces
Damien Hall
4.1
Introduction
81
4.1.1
Terminology of Adsorption
82
4.1.2
Optical Quantification of Adsorption
at an Interface
86
Contents
4.2
Defining Factors of the Adsorption Event
87
4.2.1
Mass Transfer
90
4.2.2
Adsorption Mechanisms
98
4.2.2.1
Idealized Partition Processes
99
4.2.2.2
Effect of Competing Reactions
101
4.2.2.3
Surface Functions for Different
Modes of Adsorption
102
4.3
Summary and Conclusions
115
4.4
Questions
116
4.5
Symbols
118
4.6
Acknowledgements
119
References
120
Chapter
5
Kinetic and Thermodynamic Analysis of Ligand-Receptor
Interactions: SPR Applications in Drug Development
Nico
J.
de
Mol
and Marcel J.E. Fischer
5.1
Introduction
123
5.2
Affinity and Kinetics of a Transport-limited
Bimolecular Interaction at the Sensor Surface
125
5.2.1
Affinity Constants Derived from Equilibrium
SPR Signals
126
5.2.1.1
Correction for Depletion of Free
Analyte Concentration in the Cuvette
128
5.2.2
Affinity Constants and Rate Constants
Derived from Kinetic Analysis
129
5.2.2.1
kobs Kinetic Analysis
130
5.2.2.2
Global Kinetic Analysis with a
Simple Bimolecular Binding Model
131
5.3
Detecting Mass Transport Limitation: A Practical
Approach
135
5.3.1
Effect of Viscosity Change on the Association
Phase
135
5.3.2
Transport Limitation in the Dissociation
Phase
137
5.3.2.1
Rebinding Model for Transport-
limited Dissociation
137
5.3.2.2
Competing Ligand to Prevent
Rebinding During
Dissociation
139
5.3.2.3
Experimental Procedure to Assay
High Off-rates
141
5.3.3
Quantitative Considerations on Mass
Transport Limitation
142
5.3.3.1
Flow or Cuvette?
143
xvj
Contents
5.4
Global
Kinetic Analysis of Complex Binding
Models
143
5.4.1
Global Kinetic Analysis Including Mass
Transport and a Conformational Change
144
5.4.2
Unusual Kinetics: Intermolecular Bivalent
Binding to the Sensor Surface
147
5.4.3
Global Kinetic Analysis: Concluding Remarks
152
5.5
Affinity in Solution Versus Affinity at the Surface
154
5.6
Thermodynamic van t
Hoff
Analysis Using SPR Data
158
5.6.1
van t
Hoff
Thermodynamic Analysis
158
5.6.2
Comparison of SPR Thermodynamics
with Calorimetry
161
5.6.3
Transition State Analysis Using Eyring Plots
163
5.7
SPR Applications in Pharma Research: Concluding
Remarks and Future Perspectives
165
5.8
Questions
167
5.9
Symbols
168
5.10
Acknowledgements
169
References
169
Chapter
6
Surface Chemistry in SPR Technology
Erk T. Gedig
6.1
Introduction
173
6.1.1
General Aspects of Surfaces for Biomolecular
Interaction Analysis
174
6.1.2
Selection of the Optimal Surface
177
6.2
Adhesion Linking Layers for Gold, Glass and
Plastics
181
6.2.1
Adhesion Linking Layers for Metal Surfaces
182
6.2.2
Adhesion Linking Layers for Inorganic
Dielectrics
182
6.2.3
Adhesion Linking Layers for Plastics
183
6.3
Bioinert Matrices
183
6.3.1
Non-specific Adsorption of Biomolecules
183
6.3.2
Bioinert
Hydrogels
185
6.4
Choosing the Optimal Nanoarchitecture
187
6.4.1
Two-dimensional Surfaces
189
6.4.2
Three-dimensional
Hydrogels
191
6.5
Coupling Procedures for Ligand Immobilization
194
6.5.1
Adsorptive Immobilization
195
6.5.2
Preconcentration Methods Prior to Covalent
Immobilization
195
6.5.2.1
Electrostatic Preconcentration
195
6.5.2.2
Dry Immobilization
197
Contents xvii
6.5.3 Covalent
Activation Chemistries
199
6.5.3.1
Amine
Coupling via Reactive
Esters 199
6.5.3.2
Amine
Coupling Through Reductive
Amination 202
6.5.3.3
Thiol Coupling
203
6.5.3.4
Immobilization of Aldehydes
Through Hydrazide Groups
207
6.5.3.5
Coupling Through Epoxy Groups
208
6.5.4
Electrostatic Methods
210
6.5.5
Directed Immobilization
212
6.5.6
Immobilization of Membrane Proteins
213
6.6
Conclusions and Outlook
216
6.7
Questions
217
References
218
Chapter
7
Measurement of the Analysis Cycle: Scanning SPR
Microarray Imaging of Autoimmune Diseases
Richard
Β.Μ
.
Schasfoort,
Angélique
M.C. Lokáte, J.
Bianca
Beusink,
Ger
J.M. Pruijn and
Gerard
H.M. Engbers
7.1
Introduction
221
7.2
The Analysis Cycle
222
7.3
Buffer Solutions
for Measuring the Analysis
Cycle
224
7.3.1
Baseline Buffer
224
7.3.2
Regeneration Solution
225
7.4
SPR-based Immunoassays
225
7.4.1
Direct Assay
226
7.4.2
Competition Assay
226
7.4.3
Inhibition Assay
227
7.4.4
Sandwich Assay
228
7.5
Detection of Multiplex Analysis Cycles Using
Scanning SPR Imaging
228
7.5.1
Dynamic Range of Scanning SPR Imaging
230
7.5.2
Liquid Handling Procedures
232
7.5.3
Determination of the Limit of Detection Using
Multiplex Analysis Cycles
232
7.6
Monitoring of Autoantibodies in Serum
of Rheumatoid Arthritis Patients
235
7.6.1
Experimental Conditions for Serum
Measurements
235
7.6.1.1
Serum Samples
235
7.6.1.2
SPR Microarray Interaction Studies
236
7.6.2
Results and Discussion of Monitoring Analysis
Cycles for Autoantibody Screening
236
xviii Contents
7.7 Features
and Benefits of
Monitoring
Analysis Cycles
with SPR Imaging
241
7.8
Conclusion
242
7.9
Questions
243
7.10
Acknowledgement
243
References
243
Chapter
8
Advanced Methods for SPR Imaging Biosensing
Alastair W. Wark, Hye Jin Lee and Robert M. Corn
8.1
Introduction
246
8.2
Advances in SPRI Instrumentation and Surface
Chemistry
247
8.3
Surface Enzymatic Transformations for Enhanced
SPRI Biosensing
254
8.3.1
Measuring Surface Enzyme Kinetics
254
8.3.2
RNase H-Amplified Detection of
DNA 257
8.3.3
Fabrication of
RNA Microarrays
with
RNA-DNA Surface Ligation Chemistry
259
8.4
Nanoparticle-amplified SPRI Biosensing
260
8.4.1
Single Nucleotide Polymorphism Genotyping
262
8.4.2
MicroRNA Detection
264
8.5
Summary and Outlook
269
8.6
Questions
270
8.7
Acknowledgements
271
References
271
Chapter
9
Surface Plasmon Fluorescence Techniques
for Bioaffinitv Studies
Wolfgang Knoll,
Amai Kasry,
Jing Liu, Thomas Neumann,
Lifang Niu, Hyeyoung Park,
Harald Paulsen,
Rudolf
Robe lek, Danfeng
Yao and Fang Yu
9.1
Introduction
275
9.2
Surface Plasmon Fluorescence Spectroscopy (SPFS)
278
9.3
Interface Kinetics Based on the Langmuir Adsorption
Model
282
9.3.1
Mass Transport-controlled Kinetics
284
9.3.2
Interaction-controlled Kinetics
284
9.3.3
Equilibrium Analysis
286
9.4
Applications of the Kinetic Model
286
9.4.1
Surface Hybridization Reactions
of Oligonucleotides
286
9.4.2
Protein Binding Studies
298
9.5
Novel Approaches to SPFS
300
Contents
xix
9.5.1
Grating Coupling for SPFS
301
9.5.2
Long-range Surface Plasmons for SPFS
303
9.5.3
Fluorescence Imaging and Color Multiplexing
306
9.6
Conclusions
309
9.7
Questions
309
9.8
Acknowledgements
310
References
310
Chapter
10
S
PR Imaging for Clinical Diagnostics
Elain
Fu,
Timothy Chinowsky,
Kjell
Nelson and Paul Yager
10.1
Introduction
313
10.2
Achieving Miniaturization and Low Cost
314
10.2.1
Tuning in SPR Imager Design
315
10.2.2
Compact Design of Additional SPR Imager
Optical Elements
315
10.3
Optimizing Imager Performance
317
10.3.1
Refractive Index Resolution
317
10.3.2
Lateral Resolution Over the Field of View
320
10.4
Robust Operation
321
10.4.1
Effects of Temperature Fluctuations
321
10.4.2
Strategies to Alleviate the Effects
of Temperature Fluctuations
322
10.4.3
Bulk RI Compensation
323
10.5
SPR Imaging Assays
324
10.5.1
Microfluidic Immunoassay Design for Small
Molecule Analytes
324
10.5.2
Assay Compatibility with Complex
Samples
327
10.5.3
Assay Implementation
329
10.6
Conclusion
329
10.7
Questions
330
References
330
Chapter
11
The Benefits and Scope of Surface Plasmon Resonance-based
Biosensors in Food Analysis
Alan McWhirter and
Lennart Wahlström
11.1
Introduction
333
11.1.1
Why Analyze Food?
334
11.1.2
Food Analysis Steps and SPR Assay
Formats
334
11.2
Biacore
Q
and Qflex Kits
-
the Workhorse of Food
Analysis
338
11.2.1
Qflex Kits for Screening Veterinary Drug
Residues
339
xx
Contents
11.2.2
Qflex Kits for Quantifying Vitamin Content
343
11.2.3
AOAC Certification of Qflex Kits
344
11.3
Examples of Applications for SPR-based Biosensors
in Food Analysis
345
11.3.1
Quantifying Antibiotics in Honey
345
11.3.2
Screening for Veterinary Drug Residues
346
11.3.3
Milk Testing
347
11.3.4
Detecting Antibodies to Salmonella in Meat
350
11.3.5
Genetically Modified Organisms
350
11.4
Conclusions
351
11.5
Questions
352
References
352
Chapter
12
Future Trends in SPR Technology
Richard B.M. Schasfoort and Peter Schuck
12.1
Introduction
354
12.2
Trends in SPR Instrumentation
355
12.2.1
SPR Imaging
356
12.2.2
Hyphenation SPR Technology
356
12.2.2.1
SPR-MS
357
12.2.2.2
Other Hyphenated SPR
Techniques
359
12.2.3
Nanoparticle SPR
360
12.3
Trends in Fluidics
361
12.3.1
Microarray Spotting on Gold
362
12.3.1.1 DNA
Coding Technology
364
12.3.2
Prospects for SPR-based Point of Care
Devices
366
12.3.3
Implementation of Lab-on-a-Chip Devices
for SPR Systems
367
12.3.3.1
Pumping Liquids Using
Electroosmotic Flow in Micro-
fluidic Devices with Gold Layers
367
12.3.4
Lab-on-a-Chip Implementation Using Free
Flow Electrophoresis and SPR Imaging
for Proteomics-on-a-Chip
369
12.3.5
Digital Microfluidics
373
12.3.5.1
Cell Diagnosis and Monoclonal
Antibody Screening Using SPR
Imaging and Digital Microfluidics
375
12.4
Trends in Sensor Surfaces
376
12.4.1
Smart Polymer Brushes
376
12.4.2
Photoactivation of Surfaces
for Immobilization
378
12.4.3
Gradient Chemistries
380
Contents xxi
12.5 Trends in
Measuring Reliable Kinetic
Parameters 381
12.5.1
Introduction
381
12.5.2
The Model for Distribution Analysis of Rate
and Equilibrium Constants
383
12.5.3
Examples of the Distribution Analysis
Method
385
12.5.4
Conclusions and Perspectives of the
Distribution Analysis Model
388
12.6
Final Comments
391
12.7
Questions
391
References
392
Subject Index
395
Surface plasmon
resonance (SPR) plays
a dominant
role in
real-time
interaction
sensing of biomolecular binding events.
Although the last decades have seen the birth of various books
on sensors and biosensors with some mention of surface
plasmon resonance, such a comprehensive work on SPR covering
the issues relevant for the interested student or the practicing
researcher has long been awaited.
The Handbook of Surface Plasmon Resonance covers all
relevant aspects of present technology spanning a bridge
between theory, instrumentation and applications. The book
provides a thorough theoretical introduction, including kinetic
models of biomolecular interactions as well
asa
practical guide
for assay development.
The book describes the instrumentation of SPR in terms of
optics, fluidics, surface chemistries and kinetics with an easy-
to-follow guide of how to use the technique providing relevant
applications. The history of SPR, new trends, and a vision of
future developments and needs of the SPR market are given.
The potential of SPR is revealed by showing highly exciting and
unique opportunities for unraveling the functional relationships
of complex biological processes.
The book is a comprehensive source of information with easy
to use, stand-alone chapters, and will be essential for scientists
in industry and
academia
working with or affiliated to the
technology. Intended for a wide audience,The Handbook
of Surface Plasmon Resonance is also aspiring students to
use the technology, and the wide public interested in SPR as a
phenomenon and in its applications.
ISBN
978-0-85404-207-8
9
78085A
042678
RSC Publishing
www.rsc.org/books
|
| any_adam_object | 1 |
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| discipline | Chemie / Pharmazie Physik Biologie Chemie |
| edition | Reprinted |
| format | Book |
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| genre | (DE-588)4143413-4 Aufsatzsammlung gnd-content |
| genre_facet | Aufsatzsammlung |
| id | DE-604.BV035596872 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T21:41:17Z |
| institution | BVB |
| isbn | 9780854042678 0854042679 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-017651992 |
| oclc_num | 254726062 |
| open_access_boolean | |
| owner | DE-20 DE-355 DE-BY-UBR DE-M49 DE-BY-TUM DE-526 DE-B768 |
| owner_facet | DE-20 DE-355 DE-BY-UBR DE-M49 DE-BY-TUM DE-526 DE-B768 |
| physical | XXI, 403 S. Ill., graph. Darst. |
| publishDate | 2008 |
| publishDateSearch | 2008 |
| publishDateSort | 2008 |
| publisher | RSC Publ. |
| record_format | marc |
| spelling | Handbook of surface plasmon resonance ed. by R. B. M. Schasfoort ... Reprinted Cambridge RSC Publ. 2008 XXI, 403 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Surface plasmon resonance Oberflächenplasmonresonanz (DE-588)4737046-4 gnd rswk-swf Biomolekül (DE-588)4135124-1 gnd rswk-swf Biosensor (DE-588)4193016-2 gnd rswk-swf Chemische Bindung (DE-588)4009843-6 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Oberflächenplasmonresonanz (DE-588)4737046-4 s Biomolekül (DE-588)4135124-1 s Chemische Bindung (DE-588)4009843-6 s DE-604 Biosensor (DE-588)4193016-2 s 1\p DE-604 Schasfoort, Richard B. M. 1959- Sonstige (DE-588)134269713 oth Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017651992&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017651992&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA Klappentext 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Handbook of surface plasmon resonance Surface plasmon resonance Oberflächenplasmonresonanz (DE-588)4737046-4 gnd Biomolekül (DE-588)4135124-1 gnd Biosensor (DE-588)4193016-2 gnd Chemische Bindung (DE-588)4009843-6 gnd |
| subject_GND | (DE-588)4737046-4 (DE-588)4135124-1 (DE-588)4193016-2 (DE-588)4009843-6 (DE-588)4143413-4 |
| title | Handbook of surface plasmon resonance |
| title_auth | Handbook of surface plasmon resonance |
| title_exact_search | Handbook of surface plasmon resonance |
| title_full | Handbook of surface plasmon resonance ed. by R. B. M. Schasfoort ... |
| title_fullStr | Handbook of surface plasmon resonance ed. by R. B. M. Schasfoort ... |
| title_full_unstemmed | Handbook of surface plasmon resonance ed. by R. B. M. Schasfoort ... |
| title_short | Handbook of surface plasmon resonance |
| title_sort | handbook of surface plasmon resonance |
| topic | Surface plasmon resonance Oberflächenplasmonresonanz (DE-588)4737046-4 gnd Biomolekül (DE-588)4135124-1 gnd Biosensor (DE-588)4193016-2 gnd Chemische Bindung (DE-588)4009843-6 gnd |
| topic_facet | Surface plasmon resonance Oberflächenplasmonresonanz Biomolekül Biosensor Chemische Bindung Aufsatzsammlung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017651992&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017651992&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA |
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