Green chemistry: environmentally benign reactions
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Boca Raton [u.a.]
CRC Press
2008
New Delhi Ane Books |
| Ausgabe: | 1. publ. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIV, 210 S. Ill., graph. Darst. |
| ISBN: | 1420070703 9781420070705 |
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Datensatz im Suchindex
| _version_ | 1804138695014481920 |
|---|---|
| adam_text | Titel: Green chemistry
Autor: Ahluwalia, V. K
Jahr: 2008
Contents
Preface v
Foreword vii
1. GREEN CHEMISTRY 1
Introduction 1
1.1 The Need of Green Chemistry 1
1.2 Principlesof Green Chemistry 2
1.3 Planning a Green Synthesis in a Chemical Laboratory 10
2. GREENREACTIONS 17
Introduction 17
2.1 AcyloinCondensation 17
Mechanism 18
2.1.1 Acyloin Condensation using coenzyme, Thiamine 20
2.1.2 Applications 21
2.2 Aldol Condensation 22
Mechanism 22
The Aldol 23
2.2.1 Acid-Catalysed Aldol Condensation 23
2.2.2 Crossed Aldol Condensation 24
2.2.3 Aldol Type Condensations of Àldehydes with
NitroAlkanes and Nitriles 27
2.2.4 VtnytogousAMol Reaction 28
2.2.5 Aldol Condensation of SUyl Enol Ethers in
Aqueous Media 28
2.2.6 Aldol Condensation in SohdPhase 29
2.2.7 Applications 30
2.3 Arndt-Eistert Synthesis 33
Mechanism 34
2.3.1 Applications 35
2.4 Baeyer-VilìigerOxidation 38
x Contents
Mechanism 39
Migratory Aptitude 40
2.4.1 Baeyer-Villiger Oxidation in Aqueous Phase 41
2.4.2 Baeyer-Villiger Oxidation in Solid State 42
2.4.3 Enzymatic Baeyer-Villiger Oxidation 42
2.4.4 Applications 43
2.5 Barbier Reaction 47
2.5.1 Barbier Reaction under sonication 47
2.5.2 Applications 48
2.6 Barton Reaction 50
Mechanism 50
2.6.1 Applications 50
2.7 Benzoin Condensation 52
Mechanism 53
2.7.1 Benzoin condensation under catalytic conditions 53
2.7.2 Applications 54
2.8 Baker-VenkatAraman Rearrangement 56
2.8.1 PTC catalysed synthesis of Flavones 56
Mechanism 57
2.8.2 Application 57
2.9 Bouveault Reaction 57
2.9.1 Bouveault Reactions under sonication 58
2.10 Cannizzaro Reaction 58
Mechanism 59
2.10.1 Crossed Cannizzaro Reaction 60
2.10.2 Intramolecular Cannizzaro Reaction 60
2.10.3 Cannizzaro reactions under sonication 61
2.10.4 Applications 61
2.11 Claisen Rearrangement 63
Mechanism 63
2.11.1 Claisen Rearrangement in Water 66
2.11.2 Applications (Classical Claisen Condensation) 66
2.11.3 Applications (Aqueous Phase Claisen Rearrangement) 67
2.12 aaisen-Schmidt Reaction 69
Mechanism 70
2.12.1 Claisen schmidt reaction in aqueous phase 70
2.12.2 Applications 71
2.13 Clemmensen Reduction 73
Mechanism 73
Iimitations 73
2.13.1 Applications 74
2.14 Dakin Reaction 76
Mechanism 77
2.14.1 Applications 77
Contents xi
2.15 Darzen Reaction 79
2.15.1 Darzen reaction in presence of phase transfer catalyst 79
Mechanism 80
2.15.2 Applications 81
2.16 Dieckmann Condensation 82
Mechanism 83
2.16.1 Dieckmann Condensation in Solid State 83
2.16.2 Dieckmann Condensation Under Sonication 83
2.16.3 Dieckmann Condensation Using Polymer
Support Technique 84
2.16.4 Applications 84
2.17 Diels-Alder Reaction 86
Mechanism 89
2.17.1 Diels-Alder Reactions under microwave Irradiation 89
2.17.2 Diels-Alder reactions in aqueous phase 89
2.17.3 Diels-Alder reaction in Ionie Liquids 89
2.18 Grignard Reaction 90
Grignard Reagent 90
2.18.1 Grignard reaction under Sonication 90
Structure of grignard Reagent 91
Grignard Reaction 91
Reaction Mechanism 92
Limitations 92
2.18.2 Grignard Reaction in Solid State 93
2.18.3 Applications 94
2.19 Heck Reaction 103
Mechanism 103
2.19.1 Heck reaction in aqueous phase 103
2.19.2 Heck reaction under PTC conditions 104
2.19.3 Heck reaction in Ionie Liquids 105
2.19.4 Applications 105
2.20 Knoevenagel Condensation 106
Mechanism 107
2.20.1 Knoevenagel Reaction in Water 108
2.20.2 Knoevenagel Reaction in Solid State 109
2.20.3 Knoevenagel Reaction m look Liquids 109
2.20.4 Applications 109
2.21 Michael Addiuon HI
Mechanism HI
2.21.1 Michael Addition Under PTC Conditions 113
2.21.2 Micliael Addition in Aqueous Medium 113
2.21.3 Michael Addition in Solid State 116
2.21.4 MichaelAdditionmlomcliquids 118
2.2lÌ A|vficfltÌDiv H9
xii Contents
2.22 Mukaiyama Reaction 123
2.22.1 Mukaiyama reaction in Aqueous Phase 124
2.23 Reformatsky Reaction 125
Mechanism 125
2.23.1 Reformatsky Reaction Using Sonication 126
2.23.2 Reformatsky Reaction in Solid State 127
2.23.3 Applications 127
2.24 Simmons-Smith Reaction 130
Mechanism 130
2.24.1 Simmons-Smith Reaction Under Sonication 131
2.24.2 Applications 132
2.25 Strecker Synthesis 133
Mechanism 134
2.25.1 Strecker Synthesis Under Sonication 134
2.25.2 Applications 135
2.26 Ullmann Reaction 136
Mechanism 136
2.26.1 Ullmann coupling under sonication 137
2.26.2 Applications 138
2.27 Weiss?Cook Reaction 140
2.28 Williamsons Ether Synthesis 140
Mechanism 141
2.28.1 Phase Transfer Catalysed Williamson Ether Synthesis 141
2.28.2 Applications 142
2.29 Wittig Reaction 143
The Phosphorus Ylides 144
Mechanism 144
2.29.1 The Wittig Reaction with Aqueous Sodium Hydroxide 145
Modifications of Wittig Reagent 146
2.29.2 Wittig Reaction in Solid Phase 148
2.29.3 Wittig Reaction in Ionie Liquids 149
2.29.4 Applications 149
2.30 Wurtz Reaction 152
Mechanism 153
2.30.1 Wurtz Reaction under Sonication 154
2.30.2 Wurtz Reaction in Water 154
2.30.3 Apphcations 154
3 GREENPREPARATION 155
3.1 Aquous Phase Reactions 155
3.1.1 HydrolysisofMethylSalicylatewithAlkali 155
3.1.2 Chalcone 156
3.1.3 6-EthoxycarboByl-3^-diphenyl-2-cyclohexenone 157
3.1.4 A,,9-Octalone 159
Contents xiii
3.1.5 p-Ethoxyacetanilide (Phenacetin) 160
3.1.6 p-Acetamidophenol (Tyienol) 161
3.1.7 VanilUdeneactone 162
3.1.8 2,4-dihydroxybenzoic aicd (B-resorcylic acid) 163
3.1.9 Iodoform 164
3.1.10 Endo-cis-1,4-endoxo-A5-cyclohexene-2,
3-dicarboxylic acid 164
3.1.11 Trans stilbene 165
3.1.12 2-Methyl-2-(3-oxobutyl)-l, 3-cyclopentanedione. 166
3.1.13 HeteroDields-AlderAdduct 167
3.2 Solid state (solventless) reactions 168
3.2.1 3-Pyridyl-4(3H)quinazolone 168
3.2.2 Diphenylcarbinol 168
3.2.3 Phenylbenzoate 169
3.3 Photochemical Reactions 169
3.3.1 Benzopionacol 169
3.3.2 Conversion of trans azobenzene to cis azobenzene 170
3.3.3 Conversionn of trans stilbene into cis stilbene 172
3.4 PTC catalysed reactions 172
3.4.1 Phenylisocyanide (C6H5N = C) 172
3.4.2 l-CyanoOctaneCC^CCH^CHjCN) 173
3.4.3 l-Oxaspiro-t2,5]-octane-2-carbonitrile 174
3.4.4 3,4-Diphenyl-7-hydroxycoumarin 174
3.4.5 Flavone 176
3.4.6 Dichloronorcarane [2,2-Dichlorobicyclo (4.1.0) heptane] 177
3.4.7 Oxidation of toluene to benzoic acid 178
3.4.8 Benzonitrile from benzamide 179
3.4.9 n-Butylbenzyl ether 180
3.4.10 Salicylaldehyde 181
3.5 Rearrangement Reactions 182
3.5.1 Benzopinacolone 182
3.5.2 2-AUylphenol 183
3.6 Microwave induced reactions 184
3.6.1 9,10-Dmyd^oanthiacene^naoKX,B^succinic anhydride
(Anthracene-maleic anhydride adduct) 184
3.6.2 3-methyl-l-phenyl-5-pyrazolone 185
3.6.3 Preparation of derivatives of some organic compounds 186
3.7 Enzymatic Transformations 187
3.7.1 Emanol 187
Analysis of the distillate 188
3.7.2 (SM+)-Ethyl 3-hydroxybutanoate 189
Cakulation of optical purity or Enaatiomeric excess 190
3.7.3 Benzoin 191
xiv Contents
3.7.4 l-Phenyl-(lS) ethan-1-ol from acetophenone 193
3.7.5 Deoximation of oximes by ultrasonically
stimulated Bakers yeast 194
3.8 Sonication reactions 195
3.8.1 Butyraldehyde 195
3.8.2 2-Chloro-N-arylanthranilicacid 196
3.9 Esterification 196
3.9.1 Benzocaine (Ethyl p-aminobenzoate) 196
3.9.2 Isopentyl acetate (Banana oil) 198
3.9.3 Methyl salicylate (oil of wintergreen) 198
3.10 Enamine reaction 200
3.10.1 2-Acetyl cyclohexanone 200
3.11 Reactions in ionie liquids 201
3.11.1 1-Acetylnaphthalene 201
3.11.2 Ethyl 4-methy 1-3-cyclohexene carboxylate 202
Index 205
|
| any_adam_object | 1 |
| author | Ahluwalia, V. K. |
| author_facet | Ahluwalia, V. K. |
| author_role | aut |
| author_sort | Ahluwalia, V. K. |
| author_variant | v k a vk vka |
| building | Verbundindex |
| bvnumber | BV035368021 |
| classification_rvk | VN 9200 |
| ctrlnum | (OCoLC)255273980 (DE-599)BSZ278203833 |
| discipline | Chemie / Pharmazie |
| edition | 1. publ. |
| format | Book |
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| id | DE-604.BV035368021 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T21:32:16Z |
| institution | BVB |
| isbn | 1420070703 9781420070705 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-017171960 |
| oclc_num | 255273980 |
| open_access_boolean | |
| owner | DE-29T DE-19 DE-BY-UBM DE-188 |
| owner_facet | DE-29T DE-19 DE-BY-UBM DE-188 |
| physical | XIV, 210 S. Ill., graph. Darst. |
| publishDate | 2008 |
| publishDateSearch | 2008 |
| publishDateSort | 2008 |
| publisher | CRC Press Ane Books |
| record_format | marc |
| spelling | Ahluwalia, V. K. Verfasser aut Green chemistry environmentally benign reactions [V. K. Ahluwalia] 1. publ. Boca Raton [u.a.] CRC Press 2008 New Delhi Ane Books XIV, 210 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Erneuerbare Ressourcen (DE-588)4152831-1 gnd rswk-swf Chemisches Produkt (DE-588)4009875-8 gnd rswk-swf Minimierung (DE-588)4251074-0 gnd rswk-swf Schutzgruppe (DE-588)4180268-8 gnd rswk-swf Lösungsmittel (DE-588)4036160-3 gnd rswk-swf Ausgangsmaterial (DE-588)4143518-7 gnd rswk-swf Wässriges Lösungsmittel (DE-588)4390651-5 gnd rswk-swf Chemische Reaktion (DE-588)4009853-9 gnd rswk-swf Nebenprodukt (DE-588)4253822-1 gnd rswk-swf Nachhaltigkeit (DE-588)4326464-5 gnd rswk-swf Chemische Industrie (DE-588)4009848-5 gnd rswk-swf Toxizität (DE-588)4078372-8 gnd rswk-swf Katalyse (DE-588)4029921-1 gnd rswk-swf Ionische Flüssigkeit (DE-588)7548899-1 gnd rswk-swf Energieeinsparung (DE-588)4014700-9 gnd rswk-swf Grüne Chemie (DE-588)7563215-9 gnd rswk-swf Grüne Chemie (DE-588)7563215-9 s DE-604 Chemische Industrie (DE-588)4009848-5 s Nachhaltigkeit (DE-588)4326464-5 s Chemische Reaktion (DE-588)4009853-9 s Katalyse (DE-588)4029921-1 s Ausgangsmaterial (DE-588)4143518-7 s Minimierung (DE-588)4251074-0 s Nebenprodukt (DE-588)4253822-1 s Toxizität (DE-588)4078372-8 s Lösungsmittel (DE-588)4036160-3 s Wässriges Lösungsmittel (DE-588)4390651-5 s Ionische Flüssigkeit (DE-588)7548899-1 s Energieeinsparung (DE-588)4014700-9 s Schutzgruppe (DE-588)4180268-8 s Erneuerbare Ressourcen (DE-588)4152831-1 s Chemisches Produkt (DE-588)4009875-8 s HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017171960&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Ahluwalia, V. K. Green chemistry environmentally benign reactions Erneuerbare Ressourcen (DE-588)4152831-1 gnd Chemisches Produkt (DE-588)4009875-8 gnd Minimierung (DE-588)4251074-0 gnd Schutzgruppe (DE-588)4180268-8 gnd Lösungsmittel (DE-588)4036160-3 gnd Ausgangsmaterial (DE-588)4143518-7 gnd Wässriges Lösungsmittel (DE-588)4390651-5 gnd Chemische Reaktion (DE-588)4009853-9 gnd Nebenprodukt (DE-588)4253822-1 gnd Nachhaltigkeit (DE-588)4326464-5 gnd Chemische Industrie (DE-588)4009848-5 gnd Toxizität (DE-588)4078372-8 gnd Katalyse (DE-588)4029921-1 gnd Ionische Flüssigkeit (DE-588)7548899-1 gnd Energieeinsparung (DE-588)4014700-9 gnd Grüne Chemie (DE-588)7563215-9 gnd |
| subject_GND | (DE-588)4152831-1 (DE-588)4009875-8 (DE-588)4251074-0 (DE-588)4180268-8 (DE-588)4036160-3 (DE-588)4143518-7 (DE-588)4390651-5 (DE-588)4009853-9 (DE-588)4253822-1 (DE-588)4326464-5 (DE-588)4009848-5 (DE-588)4078372-8 (DE-588)4029921-1 (DE-588)7548899-1 (DE-588)4014700-9 (DE-588)7563215-9 |
| title | Green chemistry environmentally benign reactions |
| title_auth | Green chemistry environmentally benign reactions |
| title_exact_search | Green chemistry environmentally benign reactions |
| title_full | Green chemistry environmentally benign reactions [V. K. Ahluwalia] |
| title_fullStr | Green chemistry environmentally benign reactions [V. K. Ahluwalia] |
| title_full_unstemmed | Green chemistry environmentally benign reactions [V. K. Ahluwalia] |
| title_short | Green chemistry |
| title_sort | green chemistry environmentally benign reactions |
| title_sub | environmentally benign reactions |
| topic | Erneuerbare Ressourcen (DE-588)4152831-1 gnd Chemisches Produkt (DE-588)4009875-8 gnd Minimierung (DE-588)4251074-0 gnd Schutzgruppe (DE-588)4180268-8 gnd Lösungsmittel (DE-588)4036160-3 gnd Ausgangsmaterial (DE-588)4143518-7 gnd Wässriges Lösungsmittel (DE-588)4390651-5 gnd Chemische Reaktion (DE-588)4009853-9 gnd Nebenprodukt (DE-588)4253822-1 gnd Nachhaltigkeit (DE-588)4326464-5 gnd Chemische Industrie (DE-588)4009848-5 gnd Toxizität (DE-588)4078372-8 gnd Katalyse (DE-588)4029921-1 gnd Ionische Flüssigkeit (DE-588)7548899-1 gnd Energieeinsparung (DE-588)4014700-9 gnd Grüne Chemie (DE-588)7563215-9 gnd |
| topic_facet | Erneuerbare Ressourcen Chemisches Produkt Minimierung Schutzgruppe Lösungsmittel Ausgangsmaterial Wässriges Lösungsmittel Chemische Reaktion Nebenprodukt Nachhaltigkeit Chemische Industrie Toxizität Katalyse Ionische Flüssigkeit Energieeinsparung Grüne Chemie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017171960&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT ahluwaliavk greenchemistryenvironmentallybenignreactions |