Chemistry of nanocrystalline oxide materials: combustion synthesis, properties and applications
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Hackensack, NJ [u.a.]
World Scientific
2008
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis Klappentext |
| Beschreibung: | XVI, 345 S. Ill., graph. Darst. |
| ISBN: | 9789812793140 9812793143 |
Internformat
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| 245 | 1 | 0 | |a Chemistry of nanocrystalline oxide materials |b combustion synthesis, properties and applications |c K C Patil ... |
| 246 | 1 | 3 | |a Nanocrystalline oxide materials |
| 264 | 1 | |a Hackensack, NJ [u.a.] |b World Scientific |c 2008 | |
| 300 | |a XVI, 345 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 4 | |a Metallic oxides | |
| 650 | 4 | |a Nanocrystals | |
| 650 | 4 | |a Nanostructured materials | |
| 650 | 4 | |a Nanocristaux | |
| 650 | 4 | |a Nanomatériaux | |
| 650 | 4 | |a Nanomatériaux - Combustion | |
| 650 | 4 | |a Oxydes métalliques | |
| 650 | 4 | |a Metallic oxides | |
| 650 | 4 | |a Nanocrystals | |
| 650 | 4 | |a Nanostructured materials | |
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Datensatz im Suchindex
| _version_ | 1804138657614921728 |
|---|---|
| adam_text | Contents
Foreword
................................ xiii
Preface
................................. xv
1.
Introduction
1
1.1
General
............................. 1
1.2
Preparative Methods
...................... 3
1.3
Scope of the Book
........................ 5
2.
Combustible Solid Precursors to Nanocrystalline Oxide Materials
9
2.1
Introduction
.......................... 9
2.2
Combustible Metal Hydrazine and Metal Hydrazine
Carboxylate Complexes
..................... 11
Part I: Metal Hydrazine Carboxylates: Precursors
to Simple Metal Oxides
14
2.3
Preparation of Metal Formate, Acetate, Oxalate, and Hydrazine
Carboxylates
.......................... 14
2.3.1
Thermal Analysis and Combustion of Metal
Hydrazine Carboxylates
................ 16
Part II: Single Source Precursors to Mixed Metal Oxides
26
2.4
Mixed Metal Oxides
...................... 26
2.4.1
Mixed Metal Acetate and Oxalate Hydrazinates:
Precursors to Cobaltites
................ 27
VII
viii
Chemistry ofNanocrystalline
Oxide
Matériák
2.4.2
Mixed
Metal
Oxalate Hydrazinates: Precursors to
Spinel
Ferrites
..................... 27
2.4.3
Mixed
Metal Oxalate
Hydrates: Precursors
to Metal Titanates
................... 30
2.5
Mixed Metal Hydrazinium Hydrazine Carboxylates
....... 30
2.5.1
Mixed Metal Hydrazinium Hydrazine Carboxylates:
Precursors to Nano-Cobaltites and
Ferrites
...... 30
2.5.2
Mixed Metal Hydrazinium Hydrazine Carboxylates:
Precursors to Mixed
Ferrites
.............. 35
2.5.3
Mixed Metal Hydrazinium Hydrazine Carboxylates:
Precursors to Manganites
............... 37
2.6
Concluding Remarks
...................... 38
3.
Solution Combustion Synthesis of Oxide Materials
42
3.1
Introduction
.......................... 42
3.2
Solution Combustion Synthesis
(SCS)
............. 43
3.2.1
Synthesis of Alumina
................. 45
3.2.2
Mechanism of Aluminum Nitrate
—
Urea
Combustion Reaction
................. 46
3.2.3
Thermodynamic Calculation
............. 48
3.3
Role of Fuels
.......................... 49
3.4
A Recipe for the Synthesis of Various Classes of Oxides
..... 53
3.4.1
Recipe for Nanomaterials
............... 56
3.5
Salient Features of Solution Combustion Method
........ 58
4.
Alumina and Related Oxide Materials
61
4.1
Introduction
.......................... 61
4.2
Alumina and Related Oxide Materials
.............. 62
4.3
a-Alumina
........................... 65
4.4
Metal Aluminates
(МАІ2О4)
.................. 68
4.5
Rare Earth Orthoaluminates (L11AIO3)
............. 73
4.6
Garnets
............................. 74
4.7
Aluminum
Borate
........................ 78
4.8
Tialite
(/З-АІ2ТІО5)
....................... 80
4.9
Aluminum Phosphate
...................... 83
Contents ix
4.10
Alumina
Composites
...................... 84
4.10.1
AI2O3
■
SiO2 System: Mullite
............. 85
4.10.2
AI2O3
■
SiO2 System: Cordierite
............ 87
4.10.3
AI2O3
·
S13
N4
System: SiAION
............ 91
4.11
Alumina Nanocomposites
.................... 93
4.11.1
Nanocatalysts, Dispersion
of
Nano-metals (Ag, Au, Pd,
andPt) inAl2O3
.................... 94
4.12
Nanopigments
......................... 99
4.12.1
Cobalt-Based Blue Alumina and Aluminates
...... 99
4.12.2
Chromium-Doped Pink Alumina (Cr3+/Al2O3): Ruby
104
4.12.3
Chromium-Doped Aluminates and Orthoaluminates
(Cr3+/MA12O4(M
=
Mg
&
Zn)) and LaAlO3)
.... 105
4.13
Nanophosphors
......................... 106
4.13.1
Phosphor Materials (Luminescence in Aluminum
Oxide Hosts)
..................... 108
4.14
Concluding Remarks
...................... 114
5.
Nano-Ceria and Metal-Ion-Substituted Ceria
117
5.1
Introduction
.......................... 117
5.2
Synthesis and Properties of Nano-Ceria
............. 119
5.3
Synthesis of Metal-Ion-Substituted Ceria
............ 121
5.4
Characterization of Metal-Ion-Substituted Ceria
........ 124
5.5
Oxygen Storage Materials
.................... 132
5.6
Metal-Ion-Substituted Ceria as Nanocatalysts
.......... 137
5.6.1
Ce!_xPdxO2-á
as a Three-Way Catalyst
........ 141
5.6.2
Cei_xPtxO2_a
..................... 146
5.6.3
Ce1_xRhxO2-(5
.................... 147
5.6.4
Bimetal Ionic Catalysts
(Сеі_хР^/2КЬх/2О2-а)
. . . 149
5.7
Concluding Remarks
...................... 151
6.
Nanocrystalline Fe2O3 and
Ferrites
154
6.1
Magnetic Materials
....................... 154
6.2
Y-Ve2O5
............................156
6.3
Spinel
Ferrites
(MFe2O4)
....................158
6.4
Mixed Metal
Ferrites
......................161
χ
Chemistry of Nanocrystalline Oxide Materials
6.4.1
Li-Zn
Ferrites
..................... 161
6.4.2
Mg-Zn
Ferrites
.................... 165
6.4.3
Ni-Zn
Ferrites
..................... 167
6.5
Rare Earth
Orthoferrites
.................... 170
6.6
Garnets (Ln3Fe5Oi2)
...................... 171
6.7
Barium and Strontium Hexaferrites
............... 174
6.8
Concluding Remarks
...................... 177
7.
Nano-Titania and Titanates
179
7.1
Introduction
.......................... 179
7.2
Nano-TiCh (Anatase)
...................... 182
7.2.1
Synthesis and Properties of Nano-TiC^ (Anatase)
... 183
7.3
Photocatalytic Properties of Nano-TiC^
............ 189
7
Λ
Metal-Ion-Substituted TiO2
.................. 197
7.4.1
Synthesis and Photocatalytic Properties of
Тч-хМхО2-ѕ
(M
=
Ag, Ce, Cu, Fe,
V,
W, and
Zr)
. . 197
7.4.2
Synthesis and Properties of
T¡i_xPdxO2-á
...... 199
7.4.3
Catalytic Properties of
Тії
_xPdxO2_5
......... 200
7.5
Titanates for Nuclear Waste Immobilization
.......... 203
7.5.1
Sintering and Microstructure Studies
......... 208
7.6
Concluding Remarks
...................... 209
8.
Zirconia and Related Oxide Materials
212
8.1
Introduction
.......................... 212
8.2
Zirconia
............................. 213
8.2.1
Preparation and Properties of ZrO2
.......... 215
8.3
Stabilized Zirconia.
....................... 220
8.3.1
Magnesia-Stabilized Zirconia
............. 221
8.3.2
Calcia-Stabilized Zirconia
............... 223
8.3.3
Yttria-Stabilized Zirconia (YSZ)
............ 225
8.3.4
Nickel in Yttria-Stabilized Zirconia (Ni-YSZ)
..... 227
8.4
Nano-Zirconia Pigments
.................... 232
8.5
Ζ1Ό2-ΑΙ2Ο3
System: ZTA
................... 235
8.6
ZrO2-CeO2 System
...................... 238
8.7
гЮ2-ТіО2
System (ZrTiO4 and Zr5Ti7O24)
......... 242
Contents xi
8.8
гЮг-ЬпгОз
System:
Pyrochlores
............... 245
8.9 NASICONs........................... 247
8.9.1 MZr2P3Oi2(M = Na, K, 1/2 Ca, and 1/4 Zr)
andNbZrP3Oi2.................... 247
8.9.2 NASICON (Na Superionic
Conductor)
Materials
(Nai+ÄPa-ÄCb)................ 251
8.10
Concluding Remarks
...................... 254
9. Perovskite Oxide Materials 256
9.1
Introduction
.......................... 256
9.2
Dielectric
Materials....................... 256
9.2.1 MTiO3> MZrO3
(M
=
Ca, Sr, and Ba)
........ 258
9.2.2
Lead-Based Dielectric Materials (PbTiO3, PbZrO3,
PZT, andPLZT)
................... 259
9.3
Relaxor Materials (PFN, PMN, PNN, and PZN)
........ 265
9.4
Microwave Resonator Materials
................. 270
9.5
Preparation and Properties of LnMO3 (M
=
Cr, Mn, Fe,
Co, and
Ni)
........................... 276
9.6
Preparation and Properties of Lai-^Sr^MC^ (M
=
Mn and Fe)
281
9.7
Concluding Remarks
...................... 289
10.
Nanocrystalline Oxide Materials for Special Applications
292
10.1
Synthesis and Properties of Simple Oxides
........... 292
10.2
Metal Silicates
.......................... 295
10.3
Ceramic Pigments
........................ 298
10.3.1
Borate
Pigments
.................... 299
10.3.2
Metal
Chromíte
Pigments
............... 302
10.3.3
Silicate Pigments
.................... 305
10.3.4
Ceria-Based Pigment —
Cei_xPrxO2-¿
........ 308
10.4
Eu3+-Ion-Doped
Red Phosphors
................ 313
10.5
Metal Vanadates
......................... 318
10.6
Rare Earth Metal Oxides (La2MO4)
.............. 320
10.7
Concluding Remarks
...................... 327
xii
Chemistry of Nanocrystalline Oxide MateriaL·
Appendix A
330
A.
1
Oxidizers (Metal Nitrates)
.................... 330
АЛЛ
Preparation ofTitanyl Nitrate (TiO(NO3)2)
...... 330
A.2 Fuels
.............................. 331
А.2Л
Carbohydrazide (CH), CH6N4O
........... 331
A.2.2 Oxalyl Dihydrazide (ODH), C2H6N4O2
....... 332
A.2.3
Tetraformal
Trisazine (TFTA),
C4HK5NĆO2
...... 332
A.2.4 N, N -Diformyl Hydrazine (DFH), C2H4N2O2
... 332
A.2.5 Maleic Hydrazide (MH), C4H4N2O2
......... 333
A.2.6 MalonicAcid Dihydrazide (MDH), C3H8N4O2
... 333
A.2.7 3-Methyl Pyrazole 5-One (3MP5O), C4H6N2O
... 333
A.3 Useful Suggestions
....................... 334
Index
.................................. 337
Nanocrystalline
Oxide
Materials
Combustion
Synthesis, Properties and
Applications
Nanoscience
and Nanotechnology have captured the
imagination
of people worldwide
and nanochemistry has stirred tremendous interest. The term, Nanotechnology
was coined by a Japanese engineer, Nario Taniguchi in
1974.
Eric Drexler in his book
Engines of Creations published in
1986
envisaged the building of molecular machines
by bringing atom by atom in a precise manner to make many simple desired systems.
However, Drexler s dream continues to be implausible since the laws of chemistry
do not easily allow this kind of assembly at the molecular level. The challenge facing
nanotechnologists today is in designing fine grained structures, unlike biomolecular
structures. A bigger confrontation is to merge the science intensive process with its
engineering aspect. In this context the present book on Chemistry of Nanocrystalline
Oxide Materials is a step closer to this challenge.
Nanocrystalline oxides exhibit interesting magnetic, dielectric, optical and catalytic
properties and find applications as sensors, pigments, phosphors and catalysts for air
and water purification. Prof.
Patii
and his colleagues at HSc, Bangalore, have developed
an original low temperature initiated self propagating synthetic route by solution
combustion and combustible precursors processes. A characteristic feature of this
process is in preparing homogenous multicomponent oxide powders of desired
composition, structure and properties. Also, doping of impurity metal atoms/ions in
an oxide matrix producing
nano
composite materials is achieved instantaneously in a
single step.
Combustion synthesis has generated great interest among chemists, physicists and
materials scientists because of its ease and rapidity as compared to the traditional
cumbersome powder synthesis methods. This book on Chemistry of Nanocrystalline
Oxides serves as a reference manual/monograph for the preparation of all types of
oxides and is expected to be useful to students and researchers of nanomaterials alike.
It also provides industrial units a unique opportunity to upscale this process into
technology and exploit its myriad potential applications.
This process heralds an exciting era in Nanochemistry.
|
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| id | DE-604.BV035341223 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T21:31:40Z |
| institution | BVB |
| isbn | 9789812793140 9812793143 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-017145518 |
| oclc_num | 185082224 |
| open_access_boolean | |
| owner | DE-703 |
| owner_facet | DE-703 |
| physical | XVI, 345 S. Ill., graph. Darst. |
| publishDate | 2008 |
| publishDateSearch | 2008 |
| publishDateSort | 2008 |
| publisher | World Scientific |
| record_format | marc |
| spelling | Chemistry of nanocrystalline oxide materials combustion synthesis, properties and applications K C Patil ... Nanocrystalline oxide materials Hackensack, NJ [u.a.] World Scientific 2008 XVI, 345 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Metallic oxides Nanocrystals Nanostructured materials Nanocristaux Nanomatériaux Nanomatériaux - Combustion Oxydes métalliques Legierung (DE-588)4035035-6 gnd rswk-swf Metalloxide (DE-588)4169619-0 gnd rswk-swf Nanotechnologie (DE-588)4327470-5 gnd rswk-swf Nanokristall (DE-588)7574326-7 gnd rswk-swf Metalloxide (DE-588)4169619-0 s Nanokristall (DE-588)7574326-7 s Nanotechnologie (DE-588)4327470-5 s Legierung (DE-588)4035035-6 s DE-604 Patil, K. C. Sonstige (DE-588)138148236 oth Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017145518&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017145518&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA Klappentext |
| spellingShingle | Chemistry of nanocrystalline oxide materials combustion synthesis, properties and applications Metallic oxides Nanocrystals Nanostructured materials Nanocristaux Nanomatériaux Nanomatériaux - Combustion Oxydes métalliques Legierung (DE-588)4035035-6 gnd Metalloxide (DE-588)4169619-0 gnd Nanotechnologie (DE-588)4327470-5 gnd Nanokristall (DE-588)7574326-7 gnd |
| subject_GND | (DE-588)4035035-6 (DE-588)4169619-0 (DE-588)4327470-5 (DE-588)7574326-7 |
| title | Chemistry of nanocrystalline oxide materials combustion synthesis, properties and applications |
| title_alt | Nanocrystalline oxide materials |
| title_auth | Chemistry of nanocrystalline oxide materials combustion synthesis, properties and applications |
| title_exact_search | Chemistry of nanocrystalline oxide materials combustion synthesis, properties and applications |
| title_full | Chemistry of nanocrystalline oxide materials combustion synthesis, properties and applications K C Patil ... |
| title_fullStr | Chemistry of nanocrystalline oxide materials combustion synthesis, properties and applications K C Patil ... |
| title_full_unstemmed | Chemistry of nanocrystalline oxide materials combustion synthesis, properties and applications K C Patil ... |
| title_short | Chemistry of nanocrystalline oxide materials |
| title_sort | chemistry of nanocrystalline oxide materials combustion synthesis properties and applications |
| title_sub | combustion synthesis, properties and applications |
| topic | Metallic oxides Nanocrystals Nanostructured materials Nanocristaux Nanomatériaux Nanomatériaux - Combustion Oxydes métalliques Legierung (DE-588)4035035-6 gnd Metalloxide (DE-588)4169619-0 gnd Nanotechnologie (DE-588)4327470-5 gnd Nanokristall (DE-588)7574326-7 gnd |
| topic_facet | Metallic oxides Nanocrystals Nanostructured materials Nanocristaux Nanomatériaux Nanomatériaux - Combustion Oxydes métalliques Legierung Metalloxide Nanotechnologie Nanokristall |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017145518&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017145518&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT patilkc chemistryofnanocrystallineoxidematerialscombustionsynthesispropertiesandapplications AT patilkc nanocrystallineoxidematerials |