Micro-process engineering: a comprehensive handbook 2 Devices, reactions and applications
Gespeichert in:
| Format: | Buch |
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| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH
2009
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XXII, 515 S. Ill., graph. Darst. |
| ISBN: | 9783527315505 |
Internformat
MARC
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Datensatz im Suchindex
| _version_ | 1804138531794190336 |
|---|---|
| adam_text | Contents
Preface XV
About the Editors XVII
List of Contributors XIX
Part I Microreactor Design, Fabrication and Assembly 1
1 Silicon and Class Microreactors 3
Roald M. Tiggelaar and}. C. E. (Han) Cardeniers
1.1 Introduction 3
1.2 Design and Fabrication of Microreactors for Heterogeneous
Catalysis 4
1.2.1 Low-temperature Microreactors 5
1.2.2 High-temperature Microreactors 7
1.3 Design and Fabrication of Microreactors for High-pressure
Applications 14
1.4 Microreactors for liquid-phase Organic Chemistry and
Biochemistry 15
1.4.1 Integrated Microfluidic Networks for High-throughput
Experiments 15
1.4.2 Microreactors Employing Immobilized Molecular Catalysts 17
1.4.3 Enzymatic Microreactors 18
1.4.4 Synthesis of Bio-related Compounds: Peptides and Sugars 20
1.5 Conclusion 21
References 21
2 Metallic, Steel, Ceramic and Plastic Microreactors 25
JurgenJ. Brandner
2.1 Introduction 25
2.2 Manufacturing Techniques for Metals 26
2.2.1 Etching 26
2.2.2 Machining 28
Micro Process Engineering, Vol. 2: Devices, Reactions and Applications.
Edited by V. Hessel, A. Renken, J.C. Schouten, and J.-I. Yoshida
Copyright © 2009 WILEY-VCH Verlag GmbH Co. KGaA, Weinheim
ISBN: 978-3-527-31550-5
VI Contents
2.2.3 Generative Method: Selective Laser Melting 30
2.2.4 Metal Forming Techniques 31
2.2.5 Assembling and Bonding of Metal Microstructures 32
2.3 Ceramic and Glass Devices 33
2.3.1 Ceramic Devices 33
2.3.1.1 Joining and Sealing 35
2.3.2 Glass Devices 36
2.4 Polymer Microreactors 37
2.4.1 Bonding of Polymer Materials 39
2.5 Conclusion 39
References 40
Part II Bulk and Fine Chemistry 45
3 Liquid- and Liquid-Liquid-phase Reactions - Aliphatic Substitution
Reactions 47
Paul Watts and Charlotte Wiles
3.1 Nucleophilic Substitution at Saturated Carbon 47
3.2 Nucleophilic Substitution at Carbonyl Carbon 49
3.2.1 Amide Synthesis 49
3.2.2 Ester Synthesis 54
3.3 Conclusion 55
References 55
4 Liquid- and Liquid-Liquid-phase Reactions - Aromatic Substitution
Reactions 57
Stefan Lobbecke
4.1 Electrophilic Aromatic Substitution 57
4.1.1 Friedel-Crafts Reactions 57
4.1.2 Nitrations 60
4.1.3 Brominations and Iodinations 66
4.1.4 Other Electrophilic Aromatic Substitutions 69
4.2 Nucleophilic Aromatic Substitution 73
4.3 Conclusion 77
References 77
5 Liquid- and Liquid-Liquid-phase Reactions - Addition and
Elimination 8]
Jun-ichi Yoshida and Aiichiro Nagaki
5.1 Addition Reactions 81
5.2 Elimination Reactions 89
5.3 Addition-Elimination Reactions 90
5.4 Conclusion 95
References 96
Contents VII
6 Liquid- and Liquid-Liquid-phase Reactions - Coupling Reactions 99
llhyong Ryu and Takahide Fukuyama
6.1 Metal-catalyzed Coupling 99
6.2 Reactions Using Organometallic Reagents 102
6.3 Photochemical Coupling 104
6.4 Conclusion 106
References 106
7 Liquid- and Liquid-Liquid-phase Reactions - Oxidations and
Reduction 109
Jun-ichi Yoshida and Aiichiro Nagaki
7.1 Oxidation 109
7.1.1 Chemical Oxidation 109
7.1.2 Electrochemical Oxidation 112
7.1.3 Biochemical Oxidation 138
7.1.4 Miscellaneous Oxidations 122
7.2 Reduction 123
7.3 Conclusion 124
References 125
8 Cas-Liquid-phase Reactions: Substitution 131
Jun-ichi Yoshida and Aiichiro Nagaki
8.1 Fluorination 131
8.2 Chlorination 138
8.3 Nitration 139
8.4 Conclusion 139
References 140
9 Cas-Liquid-phase Reactions: Addition 143
Claude de Bellefon
9.1 Types of Reactors 143
9.2 Additions of H2( O2 O3 and CO/H2 Across C=C 149
9.3 Other H2 Additions Across C=O, C=N, C=C, Aromatic, Nitro and 0=0
Bonds 154
9.4 Miscellaneous Additions 161
9.5 Conclusion 162
References 162
10 Cas-Liquid-phase Reactions: Reduction 167
Harshal Surangalikar, Shaun McCovern, and Ronald S. Besser
10.1 Microreactor Configurations for Hydrogenation and Dehydrogenation
Reactions 168
10.1.1 Glass/Quartz Microreactors 168
10.1.2 Metal/Alloy Microreactors 168
10.1.3 Silicon-based Microreactors 169
VIII Contents
10.1.4 Ceramic Microreactors 170
10.2 Catalysts 170
10.3 Gas-phase Hydrogenation Reactions 170
10.4 Multiphase Hydrogenation Reactions 176
10.5 Conclusion 182
References 182
11 Gas-Liquid-phase Reactions: Miscellaneous Reactions 187
llhyong Ryu and Md Taifur Rahman
11.1 Dehydration 187
11.2 Phosgene Synthesis 188
11.3 Fischer-Tropsch Synthesis 190
11.4 Carbonylation 191
11.5 Conclusion 195
References 3 96
Part III Polymerization 197
12 Free Radical Polymerization 199
Christophe Sena
12.1 Introduction 199
12.1.1 Mechanism 199
12.1.2 Main Features of FRP 201
12.1.3 Goodness of Mixing 202
12.2 Use of Microsystems in FRP 202
12.2.1 Advantages 202
12.2.2 Experimental Investigations of the Use of Microsystems in FRP 203
12.2.2.1 Micromixer-assisted Polymerization of Acrylate Resins 203
12.2.2.2 FRP in Microreactors 204
12.2.2.3 Numerical Simulations of Styrene FRP in Microsystems 209
12.3 Conclusion 211
References 212
13 Living Radical Polymerization 213
Thomas E. Enright
13.1 Living Polymerization 213
13.1.1 Free Radical Polymerization Mechanism 215
13.2 Living Radical Polymerization General Mechanisms 217
13.2.1 Dissociation-Combination 217
13.2.2 Atom Transfer 217
13.2.3 Degenerative Chain Transfer 218
13.3 Nitroxide-mediated Polymerization 218
13.4 Atom Transfer Radical Polymerization 219
13.5 Reversible Addition-Fragmentation Chain Transfer 220
Contents IX
13.6 NMP, ATRP and RAFT Summary 220
13.7 Living Radical Polymerization in Tubular Reactors 221
13.8 Living Radical Polymerization in Microreactors 221
13.9 Conclusion 223
References 223
14 Cationic Polymerization 229
Jun-ichi Yoshida and Aiichiro Nagaki
14.1 Introduction 229
14.1.1 Basic Principles of Cationic Polymerization 229
14.1.2 Controlled/Living Cationic Polymerization Based on Cation
Stabilization 230
14.2 Cationic Polymerization Involving Carbocationic Intermediates Using
Microflow Systems 231
14.2.1 Controlled/Living Cationic Polymerization Based on Cation Stabilization
Using Microflow Systems 231
14.2.2 Controlled/Living Cationic Polymerization Without Stabilization of
Carbocationic Intermediates Using Microflow Systems 232
14.2.2.1 Concept of Microflow System-controlled Polymerization Technology
(MCPT) 232
14.2.2.2 Cation Pool -initiated Polymerization Using a Microflow System 233
14.2.2.3 Proton Acid-initiated Polymerization Using Microflow Systems 236
14.3 Ziegler-Natta Polymerization 241
14.4 Conclusion 241
References 242
15 Polycondensation 245
Takeshi Honda and Hideaki Maeda
15.1 Introduction 245
15.2 Synthesis of Fine Solid Material in a Microreactor 246
15.2.1 Synthesis of Polymer Membranes 246
15.2.2 Syntheses of Various Solid Materials by Polycondensation 248
15.3 Solution-phase Polymerization Controlled in a Microreactor 249
15.3.1 Amino Acid Polymer Synthesis 249
15.3.2 Combinatorial and High-throughput Technologies in Microfluidic
Polymerization 253
15.4 Conclusion 254
References 255
Part IV Functional Materials 257
16 Organic Particles and Pigments 259
Hieng Kim
16.1 Introduction 259
X Contents
16.1.1 Definition of Microfluidics 259
16.1.1.1 Further Definitions 260
16.1.2 Historical Development of Pigments/
Colorants 260
16.1.3 Conventional Production Methods/Conventional Continuous
Processes 261
16.2 Suitability of Microfiuidic Devices for the Preparation of Organic
Particles and Pigments 264
16.2.1 Mixing and Nucleation 264
16.3 Laboratory-Scale Preparation 265
16.3.1 Pigments, Colorants 265
16.3.2 Monomeric Dyes 266
16.3.3 Polymer-analogue Dyes 267
16.4 Technical-scale Production of Organic Particles and
Pigments 268
16.4.1 Pigments, Colorants 268
16.5 Conclusion and Outlook 269
References 270
17 Inorganic Particles 273
Michael Kohler
17.1 Introduction 273
17.2 Dielectric Nanoparticles 274
17.3 Semiconductor Nanoparticles 275
17.4 Metal Nanoparticles 276
17.5 Transport Conditions in Nanoparticle Formation 284
17.6 Applications of Nanoparticles in Microreactors 285
17.7 Conclusion 286
References 286
18 Polymer Particles 289
Christophe Sena
18.1 Introduction 289
18.2 Most Common Microsystems 290
18.2.1 Emulsification Technique 290
18.2.2 Projection Photolithography Technique 291
18.3 Examples of Various Polymer Particles Produced with
Microsystems 292
18.3.1 Terrace-like MicroChannel Devices 292
18.3.2 T-junction MicroChannel Devices 294
18.3.3 Flow Focusing Devices 298
18.3.4 Projection Photolithography Devices 307
18.4 Conclusion 310
References 311
Contents
19 Microencapsulates, Proteins and Lipids/Vesides 313
John van der Schaaf
19.1 Introduction 313
19.2 Production Methods 314
19.3 Conclusion 321
References 321
20 Oil-in-Water and Water-in-Oil Emulsions 325
Heike P. Schuchmann, Karsten Kohler, Freddy Aguilar, and Andreas Hensel
20.1 Emulsion Basics 325
20.1.1 Definitions, Major and Minor Ingredients 325
20.1.2 Emulsion Properties and Their Design 326
20.1.3 Principle of Emulsification 327
20.2 Emulsification Process Functions 327
20.2.1 Droplet Disruption Theory 327
20.2.2 Droplet Disruption in Turbulent and Laminar Flow 328
20.2.3 Droplet Formation and Detachment at Membrane Surfaces 330
20.3 Emulsification Processes 331
20.3.1 Conventional and Innovative Techniques 331
20.3.2 Microengineered Devices 332
20.3.2.1 High-pressure Homogenization Nozzles 332
20.3.2.2 Membranes, Microporous and MicroChannel Systems 332
20.3.2.3 Microengineered Mixers (Micromixers) 335
20.3.2.4 Simultaneous Mixing and Homogenization (Microengineered
SMH-Valve) 337
20.3.3 Emulsification in Microengineered Devices 339
20.4 Conclusion and Outlook 340
References 341
21 Double, Triple and Complex Multilayered Emulsions 345
Takasi Nisisako
21.1 Introduction 345
21.2 Membrane Emulsification 347
21.3 MicroChannel (MC) Emulsification 348
21.4 Two-dimensional Microfluidic Systems 350
21.5 Three-dimensional (3D) Coaxial Microcapillary Systems 352
21.6 Applications to Novel Materials 355
21.7 Conclusion 355
References 355
22 Microreactor Applications in the Consumer Goods Industry 363
Patrick Lob, Volker Hessel, and Alberto Simoncelli
22.1 Introduction 363
22.2 General Aspects of Microreactor Applications for Emulsification
Processes 364
XII Contents
22.3 Comparison of Micromixers with Regard to Performance in Liquid-
liquid Dispersions 366
22.4 Dispersion and Mixing of High-viscosity Liquids 368
22.5 Cream Formation in Micromixers Targeting a Reduction in Emulsifiers
and Preservatives 371
22.6 Customer-based Production of Emulsions and More 372
22.7 Vesicle Formation in Microfluidic Structures 376
22.8 Liquid Detergent Production by Surfactant Dispersion 377
22.9 Screening of Cream Formulations 380
22.10 Microencapsulation Processes 381
22.11 Alginate Gelation in Microfluidic Channels 383
22.12 Production of Base Chemicals Exemplified by SO3 and Detergent
Production 384
22.12.1 Introduction 385
22.12.2 Sulfonation of Toluene with Gaseous Sulfur Trioxide in a Microreactor
Setup 385
22.12.3 One-pass Synthesis of Pure Sulfur Trioxide in Microreactors 387
22.13 Homogenization of Dairy Products 389
22.14 Outline of Additional and Potential Aspects of Microreactor Applications
in the Consumer Goods Industry 390
22.14.1 Microfluidic Devices in Chemical Sensing of Flavors and
Fragrances 391
22.14.2 Accessibility of New Materials Exemplified by the Controlled Synthesis of
Polymer Particles 393
22.14.3 Controlled Formation of Monodisperse Double Emulsions in a
Microfluidic System 394
22.15 Summary and Outlook 395
References 399
Part V Fuel Processing 403
23 Application and Operation of Microreactors for Fuel Conversion 405
Peter Pfeifer, Katja Haas-Santo, and Oliver Corke
23.1 Applications of Fuel Conversion 405
23.1.1 Power Range 405
23.1.2 Demands from Applications 406
23.1.3 Fuels 407
23.2 Operation of Microreactors for Fuel Conversion 407
23.2.1 Routes for Fuel Conversion 407
23.2.2 Gas Clean-up 409
23.2.3 Heat Generation 410
23.2.4 Development Stages 411
23.2.5 Integrated Plant Concepts 411
23.2.6 Examples of Different Approaches and Integration Levels 412
Contents XIII
23.2.7 Influences on Efficiency 417
23.3 Conclusion and Outlook 418
References 419
24 Steam Reforming 421
Cunther Kolb
24.1 Introduction 421
24.2 Reaction System 421
24.3 Catalyst Coatings for Steam Reforming in Microchannels 422
24.3.1 Catalyst Development and Characterization for Alcohol Steam
Reforming in Microchannels 422
24.3.2 Development of Catalyst Coatings for Hydrocarbon Steam Reforming
in Microchannels 425
24.4 System Design and Integrated Microstrucrured Reactors 426
24 A.I Design Concepts of Microstrucrured Fuel Processors for Fuel Cells 426
24.4.2 Reactors for Alcohol Steam Reforming 427
24.4.2.1 Reactors for Methanol Steam Reforming in the Low and Sub-watt
Power Range 428
24.4.2.2 Alcohol Steam Reforming in Microstrucrured Plate Heat Exchangers 431
24.4.2.3 Hydrocarbon Steam Reforming in Microstrucrured Plate Heat
Exchangers 435
24.5 Conclusion 439
References 439
25 Partial Oxidation 445
Peter Pfeifer
25.1 Distinction Between Catalytic and Industrial Processes 446
25.2 Catalysts 446
25.2.1 Catalytically Active Species 447
25.2.2 Catalytic Supports and Promoters 448
25.3 Reactor Design and Results 450
25.3.1 Packed Beds and Foams in Microstructures 451
25.3.2 Catalytic Wall Reactors 453
25.3.2.1 Microstructured Catalytically Active Materials 453
25.3.2.2 Deposition of Catalytically Active Species on Microstructure Walls 455
25.3.2.3 Deposition of Catalytically Active Species on Additional Catalyst
Supports 457
25.4 Reactor Comparison 460
25.5 Conclusion 462
References 463
26 CO Clean-up: Water Cas Shift and Methanation Reactions 465
Andre C. van Veen, Yves Schuurman, and Claude Mirodatos
26.1 Background of the Two Reactions 465
26.2 Commercial and R D Catalysts 468
XIV Contents
26.2.1 Temperature Range of Operation 468
26.2.2 Operational Limits 469
26.2.3 Non-pyrophoric Catalysts 469
26.2.4 Methanation Catalysts 470
26.3 Motivation for Microstructured Reactors 470
26.3.1 WGS Reaction 470
26.3.2 Methanation Reaction 470
26 A Examples of Microstructured Reactor Developments 471
26.4.1 WGS Reaction 471
26.4.2 Methanation Reaction 475
26.5 Conclusion 476
References 476
27 CO Clean-up: Preferential Oxidation 479
Xun Ouyang and Ronald S. Besser
27.1 Introduction 479
27.2 PrOx Kinetics 480
27.3 PrOx in Microreactors 482
27.3.1 Microreactors as Tools for Catalyst and Kinetic Studies 482
27.3.1.1 Catalyzed Microstructured Reactors for PrOx Catalyst Screening 482
27.3.1.2 Silicon Microfabricated PrOx Reactor with Washcoated Microposts 484
27.3.1.3 Improved PrOx Performance Versus Monolith 484
27.3.1.4 PrOx Study with Grooved Stainless-steel Foils and Au-based
Catalysts 485
27.3.2 PrOx in Integrated Fuel Processors 486
27.3.2.1 A 2.4 We Micro Fuel Processor Based on Microchannels 486
27.3.2.2 MicroChannel Reactors for a 100 We Portable Fuel Processor 488
27.3.2.3 A 100 We Gasoline Fuel Processor Based on Foam Structure with
Micropores 489
27.3.2.4 A 2 kWe Multistage PrOx MicroChannel Reactor 490
27 A A Detailed Example: A Thin-film Catalytic Microreactor as a Kinetic
Tool 491
27.4.1 Experimental 492
27.4.2 Microkinetic Reaction Simulation 493
27A3 Quasi-3D Non-isothermal Reactor Model 495
27.5 Conclusion 499
References 499
Index 503
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| indexdate | 2024-07-09T21:29:40Z |
| institution | BVB |
| isbn | 9783527315505 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-017057950 |
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| spelling | Micro-process engineering a comprehensive handbook 2 Devices, reactions and applications ed. by Volker Hessel ... Weinheim Wiley-VCH 2009 XXII, 515 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Mikroverfahrenstechnik (DE-588)7660041-5 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Mikroverfahrenstechnik (DE-588)7660041-5 s DE-604 Hessel, Volker 1964- Sonstige (DE-588)128736267 oth (DE-604)BV035252316 2 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017057950&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Micro-process engineering a comprehensive handbook Mikroverfahrenstechnik (DE-588)7660041-5 gnd |
| subject_GND | (DE-588)7660041-5 (DE-588)4143413-4 |
| title | Micro-process engineering a comprehensive handbook |
| title_auth | Micro-process engineering a comprehensive handbook |
| title_exact_search | Micro-process engineering a comprehensive handbook |
| title_full | Micro-process engineering a comprehensive handbook 2 Devices, reactions and applications ed. by Volker Hessel ... |
| title_fullStr | Micro-process engineering a comprehensive handbook 2 Devices, reactions and applications ed. by Volker Hessel ... |
| title_full_unstemmed | Micro-process engineering a comprehensive handbook 2 Devices, reactions and applications ed. by Volker Hessel ... |
| title_short | Micro-process engineering |
| title_sort | micro process engineering a comprehensive handbook devices reactions and applications |
| title_sub | a comprehensive handbook |
| topic | Mikroverfahrenstechnik (DE-588)7660041-5 gnd |
| topic_facet | Mikroverfahrenstechnik Aufsatzsammlung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017057950&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV035252316 |
| work_keys_str_mv | AT hesselvolker microprocessengineeringacomprehensivehandbook2 |