Holdings: Basic solid state chemistry

Basic solid state chemistry:

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Bibliographic Details
Main Author:	West, Anthony R. (Author)
Format:	Book
Language:	English
Published:	Chichester [u.a.] Wiley 2008
Edition:	2. ed., reprinted
Subjects:	Festkörperchemie Lehrbuch
Online Access:	Inhaltsverzeichnis
Item Description:	Hier auch später erschienene, unvränderte Nachdrucke
Physical Description:	XVI, 480 S. Ill., graph. Darst.
ISBN:	0471987565 0471987557 kart. 9780471987567 geb. 9780471987550

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adam_text	Contents Preface ....................... xvi Chapter 1 Crystal Structures ................ 1 1.1 Unit cells and crystal systems ............. 1 1.2 Symmetry .................... 4 1.3 Symmetry and choice of unit cell ............ 7 1.4 Lattice, Bravais lattice ................ 9 1.5 Lattice planes and Miller indices ............ 10 1.6 Indices of directions ................. 12 1.7 ¿/-spacing formulae ................. 13 1.8 Crystal densities and unit cell contents .......... 13 1.9 Description of crystal structures ............ 14 1.10 Close packed structures — cubic and hexagonal close packing . . 15 1.11 Relationship between cubic close packed and face centred cubic 17 1.12 Hexagonal unit cell and close packing .......... 19 1.13 Density of close packed structures ........... 19 1.14 Unit cell projections and atomic coordinates ....... 20 1.15 Materials that can be described as close packed ...... 21 a) Metals .................... 21 b) Alloys .................... 21 c) Ionic structures ................. 21 i) Tetrahedral and octahedral sites ......... 22 ii) Relative sizes of tetrahedra and octahedra ..... 24 iii) Location of tetrahedra] and octahedral sites in a fee unit cell; bond length calculations; fractional atomic coordinates .............. 25 d) Covalent network structures ............ 27 e) Molecular structures ............... 27 f) Fullerenes and füllendes.............. 29 1.16 Structures built of space-filling polyhedra ........ 30 1.17 Some important structure types ............ 33 a) Rock salt (NaCl), zinc blende or sphalerite (ZnS), fluorite (CaF2), antifluorite (Na2O) .......... 33 i) Rock salt structure .............. 35 ii) Zinc blende (sphalerite) structure ......... 37 iii) Antifluorite/fluorite structure .......... 38 iv) Bond length calculations ............ 39 vii V i _____________________________________________________________ Contents b) Diamond .................. 41 c) Wurtzite (ZnS) and nickel arsenide (NiAs) ...... 41 d) Caesium chloride (CsCl) ............. 46 e) Other AX structures .............. 47 0 Rutile (ТІО2), cadmium iodide (Cdb), cadmium chloride (CdCli) and caesium oxide (Cs?O) ......... 48 g) Perovskite (SrTiO-O .............. 56 i) Tolerance factor .............. 57 ii) ВаТіОз ................. 58 iii) GdFeCb ................. 59 iv) Stoichiometry-property relations ........ 59 h) Rhenium trioxide (ReC^) and tungsten bronzes .... 59 i) Spinel ................... 60 j) Silicate structures — some tips to understanding them ... 63 Chapter 2 Bonding in Solids ............... 67 2.1 Ionic bonding .................. 67 2.2 Ions and ionic radii ................ 68 2.3 Ionic structures — general principles .......... 72 2.4 The radius ratio rule ................ 75 2.5 Borderline radius ratios and distorted structures ...... 78 2.6 Lattice energy of ionic crystals ............ 79 2.7 Kapustinskii s equation ............... 83 2.8 The Born-Haber cycle and thermochemical calculations ... 84 2.9 Stabilities of real and hypothetical ionic compounds .... 86 a) Inert gas compounds .............. 86 b) Lower and higher valence compounds ........ 87 2.10 Partial covalent bonding .............. 89 2.11 Coordinated polymeric structures — Sanderson s model ... 90 a) Effective nuclear charge ............. 90 b) Atomic radii ................. 91 c) Electronegativity and partially charged atoms ..... 91 2.12 Mooser-Pearson plots and ionicities .......... 96 2.13 Bond valence and bond length ............ 97 2.14 Non-bonding electron effects ............ 100 a) ¿-electron effects ............... 100 i) Crystal field splitting of energy levels ....... 100 ii) Jahn-Teller distortions ............ 104 iii) Square planar coordination .......... 106 iv) Tetrahedral coordination ........... 106 v) Tetrahedral versus octahedral coordination .... 107 b) Inert pair effect ................ 109 2.15 Metallic bonding and band theory .......... 110 a) Band structure of metals ............. 114 b) Band structure of insulators ........... 115 c) Band structure of semiconductors: silicon ....... 115 Contents ¡x d) Band structure of inorganic solids ......... 117 i) III-V, II-VI and I- VII compounds ....... 117 ii) Transition metal compounds ......... 119 iii) Fullerenes and graphite ........... 121 2.16 Bands or bonds: a final comment .......... 123 Chapter 3 Crystallography and Diffraction Techniques ...... 125 3.1 General comments: molecular and non-molecular solids . . . 125 3.2 Characterization of solids .............. 126 3.3 X-ray diffraction ................. 127 a) Generation of X-rays .............. 127 b) An optical grating and diffraction of light ...... 130 c) Crystals and diffraction of X-rays ......... 132 i) The Laue equations ............. 133 ii) Bragg s law ............... 133 d) X-ray diffraction methods ............ 135 e) The powder method — principles and uses ...... 136 f) Powder diffractometers ............. 138 g) Focusing of X-rays: theorem of a circle ....... 139 h) Crystal monochromators ............ 140 i) Guinier focusing cameras ............ 141 j) A powder pattern of a crystalline phase is its fingerprint . 142 k) Intensities .................. 143 i) Scattering of X-rays by an atom: atomic scattering factors 143 ii) Scattering of X-rays by a crystal — systematic absences 146 iii) General formula for phase difference, б ..... 148 iv) Intensities and structure factors ........ 150 v) .R-factors and structure determination ...... 153 1) Electron density maps ............. 155 m) X-ray crystallography and structure determination — what s involved? .................. 156 i) The Patterson method ............ 159 ii) Fourier methods .............. 159 iii) Direct methods .............. 160 3.4 Electron diffraction ................ 160 3.5 Neutron diffraction ................ 161 a) Crystal structure determination .......... 162 b) Magnetic structure analysis ........... 162 c) Inelastic scattering, soft modes and phase transitions . . 165 Chapter 4 Other Techniques: Microscopy, Spectroscopy, Thermal Analysis ............... 167 4.1 Microscopic techniques .............. 167 a) Optical microscopy .............. 167 i) Polarizing microscope ............ 168 ii) Reflected light microscope .......... 169 x ___________________________ ______________^ ______Contents iii) Applications ............... 169 Crystal morphology and symmetry ..... 169 Phase identification, purity and homogeneity . . 170 Crystal defects — grain boundaries and dislocations 171 Refractive index determination, the Becke line and fibre optic communications ....... 171 b) Electron microscopy .............. 172 i) Particle size and shape, texture, surface detail .... 175 ii) Crystal defects ............... 175 iii) Precipitation and phase transitions ....... 176 iv) Chemical analysis ............. 176 v) Structure determination ........... 177 4.2 Spectroscopie techniques .............. 177 a) Yibrational spectroscopy: IR and Raman ....... 179 b) Visible and ultraviolet spectroscopy ......... 181 i) Structural studies on glass ........... 183 ii) Study of laser materials ........... 184 c) Nuclear magnetic resonance (NMR) spectroscopy . ... 184 d) Electron spin resonance (ESR) spectroscopy ...... 187 e) X-ray spectroscopies: XRF, AEFS, EXAFS ...... 189 i) Emission techniques ............. 191 ii) Absorption techniques ............ 192 XANES ............... 194 EXAFS ............... 194 f) Electron spectroscopies: ESCA, XPS, UPS, AES, EELS. . 196 g) Mössbauer spectroscopy ............. 200 4.3 Thermal analysis ................. 203 a) Thermogravimetry (TG) ............. 203 b) Differential thermal analysis (DTA) and differential scanning calorimetry (DSC) ........... 204 c) Applications ................. 206 Chapter 5 Crystal Defects, Non-Stoichiometry and Solid Solutions . . 211 5.1 Perfect and imperfect crystals ............ 211 5.2 Types of defect: point defects ............ 213 a) Schottky defect ................ 213 b) Frenkel defect ................ 214 i) The Kroger-Vink notation for crystal defects . ... 215 ii) Thermodynamics of Schottky and Frenkel defect formation ................ 215 Schottky defects ........... 216 Frenkel defects ............ 217 c) Colour centres ................ 219 d) Vacancies and interstitials in non-stoichiometric crystals: extrinsic and intrinsic defects ........... 221 e) Defect clusters or aggregates ........... 221 Contents xi f) Interchanged atoms: order-disorder phenomena .... 225 5.3 Solid solutions ................. 226 a) Substitutional solid solutions ........... 226 b) Interstitial solid solutions ............ 229 c) More complex solid solution mechanisms: aliovalent substitution ................. 230 i) Ionic compensation mechanisms ........ 230 1. Creating cation vacancies ......... 230 2. Creating interstitial anions ......... 232 3. Creating anion vacancies ......... 232 4. Creating interstitial cations ......... 232 5. Double substitution ........... 233 ii) Electronic compensation mechanisms: metals, semi- and superconductors .......... 233 d) Further comments on the requirements for solid solution formation .................. 236 e) Experimental methods for studying solid solutions . . . 237 i) X-ray powder diffraction ........... 237 ii) Density measurements ............ 238 iii) Changes in other properties — thermal activity and DTA 240 5.4 Extended defects ................. 240 a) Crystallographic shear structures ......... 240 b) Stacking faults ................ 243 c) Subgrain boundaries and antiphase domains (boundaries) . 244 5.5 Dislocations and mechanical properties of solids ..... 245 a) Edge dislocations ............... 246 b) Screw dislocations ............... 247 c) Dislocation loops ............... 248 d) Observation of dislocations ........... 251 e) Dislocations and crystal structure ......... 252 f) Mechanical properties of metals .......... 253 g) Dislocations, vacancies and stacking faults ...... 256 h) Dislocations and grain boundaries ......... 259 Chapter 6 Interpretation of Phase Diagrams ......... 261 6.1 The phase rule, phases, components, degrees of freedom and equilibrium ................... 261 6.2 One-component systems .............. 265 a) The system H2O ............... 266 b) The system SiO2 ............... 267 c) Condensed one-component systems ......... 268 6.3 Two-component condensed systems .......... 268 a) A simple eutectic system ............ 268 i) Liquidus and solidus ............ 270 ii) Eutectic ................. 270 iii) Lever rule ................ 270 xii______________________________________________________ Contents iv) Eutectic reaction .............. 272 v) The liquidus, saturation solubilities and freezing point depression .............. 272 b) Binary systems with compounds .......... 273 i) Congruent melting ............. 274 ii) Incongruent melting, peritectic point, peritectic reaction 274 iii) Non-equilibrium effects ........... 275 iv) Upper and lower limits of stability ....... 275 c) Binary systems with solid solutions ......... 275 i) Complete solid solution ............ 275 ii) Fractional crystallization ........... 276 iii) Thermal maxima and minima ......... 277 iv) Partial solid solution systems ......... 278 d) Binary systems with solid-solid phase transitions .... 280 e) Binary systems with phase transitions and solid solutions: eutectoids and peritectoids ............ 281 f) Binary systems with liquid immiscibility; MgO-SiC^ . . . 283 g) Some technologically important phase diagrams .... 284 i) The system Fe -С: iron and steel making ...... 284 ii) The system CaO-SiC^: cement manufacture .... 285 iii) The system Na-S: Na/S batteries ........ 286 iv) The system Na2O-SiCb: glass making ...... 286 v) The system LÍ2O-SÍO2: metastable phase separation and synthetic opals ............. 289 vi) Purification of semiconducting Si by zone refining . . 290 vii) The system ZrO2-Y2C»3: yttria-stabilized zirconia solid electrolyte .............. 290 Chapter 7 Electrical Properties .............. 293 7.1 Survey of electrical properties and electrical materials .... 293 7.2 Metallic conductivity: organic metals .......... 295 a) Conjugated systems .............. 295 i) Doped polyacetylene ............. 295 ii) Polyparaphenylene and polypyrrole ....... 298 b) Organic charge transfer complexes ......... 298 7.3 Superconductivity ................. 300 a) The property of zero resistance .......... 300 b) Perfect diamagnetism; the Meissner effect ....... 301 c) Critical temperature Tc, critical field Hc and critical current Ус 303 d) Type I, type II superconductors, the vortex (mixed) state . 304 e) Survey of superconducting materials ........ 305 t) Crystal chemistry of cuprate perovskites ....... 307 g) YBa2Cu307 ................. 308 i) Crystal structure .............. 308 ii) Atom valencies and the superconducting mechanism . 310 iii) Oxygen content, ¿, of УВагСизОй ....... 311 Contents_________________________________________________________xiii iv) Determination of oxygen content, б ....... 311 h) Füllendes.................. 314 і) Applications of superconductors .......... 315 7.4 Semiconductivity ................. 315 a) Doped silicon ................ 316 b) Other semiconductors ............. 318 c) Applications ................. 320 7.5 Ionic conductivity ................ 321 a) Alkali halides: vacancy conduction ......... 322 i) Activation energy for ion hopping: geometrical considerations ............... 324 ii) Ionic conductivity of NaCl crystals ....... 326 iii) Extrinsic conductivity in NaCl — control by aliovalent doping ................. 328 b) Silver chloride: interstitial conduction ........ 329 c) Alkaline earth fluorides ............. 332 d) Solid electrolytes (or fast ion conductors, superionic conductors) ................. 332 i) General considerations ............ 332 ii) /3-aliimina and Nasicon ........... 336 Crystal structures of /?,0 - aluminas ..... 336 Conduction plane structure and conduction mechanism in /9-alumina ......... 338 Nasicon ............... 341 iii) Agi and Ag^ ion solid electrolytes ....... 341 iv) Anion conductors ............. 344 PbF2 and other halides ......... 344 Yttria-stabilized zirconia and related oxides . . 345 v) Li+ ion conductors ............. 346 vi) Proton conductors ............. 351 vii) Mixed ionic/electronic conductors ....... 351 viii) Applications of solid electrolytes and mixed conductors 353 Thermodynamic measurements ...... 353 The sodium-sulphur and Zebra batteries . . . 354 Miniature cells, heart pacemakers ...... 355 Lithium batteries ........... 356 Electrochromic devices, smart windows. . . . 359 Gas sensors ............. 360 Transport number measurements ...... 361 Solid oxide fuel cells, SOFC; steam electrolysers; oxygen pumps ............ 361 7.6 Dielectric materials ................ 361 7.7 Ferroelectricity ................. 362 7.8 Pyroelectricity .................. 369 7.9 Piezoelectricity ................. 369 7.10 Applications of ferro-, pyro-and piezoelectrics ...... 370 xiv_________________________________________________________Contents Chapter 8 Magnetic and Optical Properties .......... 373 8.1 Magnetic properties ................ 373 a) Behaviour of substances in a magnetic field ...... 374 b) Effects of temperature: Curie and Curie-Weiss laws . . . 375 c) Magnetic moments ............... 377 d) Mechanisms of ferro- and antiferromagnetic ordering: superexchange ................ 380 e) Some more definitions ............. 381 f) Selected examples of magnetic materials, their structures and properties ................ 382 i) Metals and alloys .............. 382 Pauli paramagnetism and ferromagnetism . . 384 Lanthanide elements .......... 386 ii) Transition metal monoxides .......... 387 iii) Transition metal dioxides .......... 387 iv) Spinels ................. 388 v) Garnets ................. 391 vi) Ilmenites and perovskites ........... 393 vii) Magnetoplumbites ............. 394 g) Applications: structure-property relations ...... 394 i) Transformer cores ............. 395 ii) Information storage ............. 396 iii) Magnetic bubble memory devices ........ 396 iv) Permanent magnets ............. 396 8.2 Optical properties: luminescence, lasers ......... 397 a) Luminescence and phosphors ........... 397 b) Configurational coordinate model ......... 399 c) Some phosphor materials ............ 401 d) Anti-Stokes phosphors ............. 402 e) Lasers ................... 403 i) The ruby laser ............... 404 ii) Neodymium lasers ............. 405 Chapter 9 Synthesis Methods ............... 407 9.1 General observations ............... 407 9.2 Solid state reaction or shake n bake methods ....... 407 a) Nucleation and growth, epitaxy and topotaxy ..... 408 b) Examples of solid state reactions .......... 411 i) LÍ4SÍO4 ................. 412 ii) YBa2Cu3O7 ................ 412 iii) Na β/β alumina ............. 412 c) Problem: how to homogenize reaction mixtures? . . . . 413 9.3 Sol-gel methods ................. 413 a) Synthesis of MgAl2O4 ............. 414 b) Synthesis of silica glass ............. 414 c) Spinning of alumina fibres ............ 415 Contents xv d) Preparation of indium tin oxide (ITO) and other coatings. 415 e) Fabrication of YSZ ceramics ........... 416 f) Synthesis of zeolites .............. 416 g) Preparation of alumina-based abrasives ....... 416 h) Preparation of YBCO superconductor ....... 417 9.4 Use of homogeneous, single source precursors ...... 417 9.5 Hydrothermal synthesis .............. 418 9.6 Intercalation and deinterca&tion ........... 419 9.7 Vapour phase transport .............. 421 9.8 Preparation of thin films; electrochemical methods, chemical vapour deposition, sputtering and laser ablation ...... 425 a) Electrochemical methods ............ 425 i) Cathodic deposition ............. 425 ii) Electroless deposition ............ 425 iii) Anodic oxidation ............. 425 b) Thermal oxidation .............. 426 c) Chemical vapour deposition fCVD) ........ 426 i) Amorphous silicon ............. 427 ii) Diamond films .............. 430 d) Sputtering and evaporation ........... 432 9.9 Combustion synthesis ............... 434 9.10 Crystal growth ................. 435 a) Czochralski method .............. 435 b) Bridgman and Stockbarger methods ........ 435 c) Zone melting ................. 437 d) Precipitation from solution or melt: flux method .... 438 e) Verneuil flame fusion method ........... 438 9.11 High pressure methods .............. 438 Further Reading .................... 441 Appendices ...................... 447 1. Interplanar spacings and unit cell volumes ........ 447 2. Model building .................. 448 3. Geometrical considerations in crystal chemistry ...... 451 4. The elements and some of their properties ........ 455 Questions ...................... 459 Index ........................ 467
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spelling	West, Anthony R. Verfasser aut Basic solid state chemistry Anthony R. West 2. ed., reprinted Chichester [u.a.] Wiley 2008 XVI, 480 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Hier auch später erschienene, unvränderte Nachdrucke Festkörperchemie (DE-588)4129288-1 gnd rswk-swf 1\p (DE-588)4123623-3 Lehrbuch gnd-content Festkörperchemie (DE-588)4129288-1 s DE-604 Digitalisierung UB Augsburg application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017006854&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk
spellingShingle	West, Anthony R. Basic solid state chemistry Festkörperchemie (DE-588)4129288-1 gnd
subject_GND	(DE-588)4129288-1 (DE-588)4123623-3
title	Basic solid state chemistry
title_auth	Basic solid state chemistry
title_exact_search	Basic solid state chemistry
title_full	Basic solid state chemistry Anthony R. West
title_fullStr	Basic solid state chemistry Anthony R. West
title_full_unstemmed	Basic solid state chemistry Anthony R. West
title_short	Basic solid state chemistry
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topic	Festkörperchemie (DE-588)4129288-1 gnd
topic_facet	Festkörperchemie Lehrbuch
url	http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017006854&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
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