Multiscale operational organic chemistry: a problem-solving approach to the laboratory course
Gespeichert in:
1. Verfasser: | |
---|---|
Format: | Buch |
Sprache: | English |
Veröffentlicht: |
Upper Saddle River, N.J.
Pearson Prentice Hall
c2009
|
Ausgabe: | 2nd ed. |
Schlagworte: | |
Online-Zugang: | Inhaltsverzeichnis |
Beschreibung: | XIII, 970 S. |
ISBN: | 9780132413756 0132413752 |
Internformat
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100 | 1 | |a Lehman, John W. |e Verfasser |4 aut | |
245 | 1 | 0 | |a Multiscale operational organic chemistry |b a problem-solving approach to the laboratory course |c John W. Lehman |
250 | |a 2nd ed. | ||
264 | 1 | |a Upper Saddle River, N.J. |b Pearson Prentice Hall |c c2009 | |
300 | |a XIII, 970 S. | ||
336 | |b txt |2 rdacontent | ||
337 | |b n |2 rdamedia | ||
338 | |b nc |2 rdacarrier | ||
650 | 4 | |a Chemistry, Organic |v Laboratory manuals | |
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Datensatz im Suchindex
_version_ | 1804138064232054784 |
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adam_text | Contents
Preface
xi
To the Instructor
xi
Acknowledgments
xiii
Introduction
1
Problem Solving in the Organic Chemistry Laboratory
Scientific Methodology
2
Organization of This Book
6
A Guide to Success in the Organic Chemistry Lab
9
Laboratory Safety
13
Safety Standards
14
Protecting Yourself
14
Preventing Laboratory Accidents
14
Reacting to Accidents: First Aid
16
Reacting to Accidents: Fire
19
Chemical Hazards
19
Finding and Using Chemical Safety Information
23
Chemistry and tbe Environment
31
Disposal of Hazardous Wastes
32
Green Chemistry
32
Part I Mastering the Operations
39
1
Learning Basic Operations. The Effect of
pH
on a Food
Preservative
40
2
Extraction and Evaporation. Separating
the Components of Panacetin
48
3
Recrystallization and Melting-Point
Measurement. Identifying a Constituent
of Panacetin
56
4
Heating Under Reflux. Synthesis of Salicylic Acid from
Wintergreen
Oil
61
5
Simple Distillation, Gas Chromatography. Preparation
of Synthetic Banana Oil
70
6
Fractional Distillation. Separation of Petroleum
Hydrocarbons
79
7
Addition, Sublimation. A Green Synthesis
of Camphor
86
8
Boiling Point, Refractive Index. Identification
of a Petroleum Hydrocarbon
93
9
Column Chromatography, UV-VIS Spectrometry.
Isolation and Isomerization of Lycopene from Tomato
Paste
100
10
Steam Distillation, Infrared Spectrometry. Isolation and
Identification of the Major Constituent of Clove Oil
109
11
Thin-Layer Chromatography, NMR Spectrometry.
Identification of Unknown Ketones
117
12
Vacuum Distillation, Optical Rotation. The Optical
Activity of a-Pinene: A Chemical Mystery
124
Part II Correlated Laboratory Experiments
131
13
Investigation of a Chemical Bond by Infrared
Spectrometry
132
14
Properties of Common Functional Groups
139
15
Thin-Layer
Chromatographie
Analysis of Drug
Components
147
16
Separation of an Alkane Clathrate
152
17
Isomers and Isomerization Reactions
160
18
Structures and Properties of Stereoisomers
166
19
Bridgehead Reactivity in an SN1 Solvolysis
Reaction
174
20
Reaction of Iodoethane with Sodium Saccharin,
an Ambident Nucleophile
182
21
Dehydration of Methylcyclohexanols and the Evelyn
Effect
188
22
Testing Markovnikov s Rule
199
23
Stereochemistry of Bromine Addition to
íraní-Cinnamic
Acid
208
24
A Green Synthesis of Adipic Acid
216
25
Preparation of Bromotriphenylmethane and the Trityl
Free Radical
223
vii
viii
Contents
26
Chain-Growth Polymerization of
Styrene
and Methyl
Methacrylate
232
27
Synthesis of
Ethanol
by Fermentation
241
28
Reaction of Butanols with Hydrobromic Acid
250
29
Borohydride Reduction of Vanillin to Vanillyl
Alcohol
260
30
Synthesis of Triphenylmethanol and the Trityl
Carbocation
269
31
An Unexpected Reaction of
2,3-Dimethyl-2,3-
butanediol
281
32
Identification of a Conjugated
Diene
from
Eucalyptus Oil
287
33
Spectral Identification of Monoterpenes
295
34
Synthesis and Spectral Analysis of Aspirin
302
35
Directive Effects in the
Bromina tion
of Vanillin
311
36
Mechanism of the Nitration of
Arenes
by Nitronium
Fluoborate
316
37
Friedel-Crafts Acylation of
Anisóle
323
38
Determination of the Structure of a Natural Product in
Anise Oil
333
39
Identification of an Oxygen-Containing Organic
Compound
340
40
Oxidation of the Insect Repellent
6-12 347
41
Isomerization of a Cyclic
Ketone
354
42
A
Wittig
Reaction of irans-Cinnamaldehyde
361
43
Effect of Reaction Conditions on the Condensation
of Furfural with Cyclopentanone
370
44
Electronic Effect of
a para-lodo
Substituent
380
45
Synthesis and Identification of an Unknown Carboxylic
Acid
389
46
Preparation of the Insect Repellent
ЛТ
iV-Diethyl-meŕe-
toluamide
395
47
Synthesis of Dimedone and Measurement of Its
Tautomerie
Equilibrium Constant
406
48
Preparation of Para Red and Related
Azo
Dyes
415
49
Reaction of Phthalimide with Sodium
Hypochlorite
424
50
Identification of an Unknown
Amine
434
51
Preparation and Mass Spectrum of 2-Phenylindole
442
52
Nucleophilic Strength and Reactivity in SNAr
Reactions
452
53
Structure of an Unknown D-Hexose
459
54
Fatty Acid Content of Commercial Cooking Oils
468
55
Structure of an Unknown Dipeptide
477
56
Multistep Synthesis of Benzilic Acid from
Benzaldehyde 487
57
Using the Chemical Literature in an Organic
Synthesis
497
58
A Research Project in Organic Chemistry
504
Partili
Minilabs 515
1
Making Useful Laboratory Items
516
2
Extraction of Iodine by Dichloromethane
517
3
Purification of an Unknown Compound
by Recrystallization
518
4
Developing and Testing a Hypothesis
518
5
Preparation of Acetate Esters
520
6 Gas Chromatographie
Analysis of Commercial
Xylene
521
7
Isolation of an Expectorant from Cough Capsules
522
8
A Missing-Label Puzzle
523
9
Paper Chromatography of Dyes in Commercial Drink
Mixes
523
10 Gas Chromatographie
Analysis of an Essential Oil from
Orange Peel
525
11
Identification of an Unknown Felt-Tip Pen Ink
by
TLC
526
12
Optical Rotation of Turpentine
527
13
The Structures of Organic Molecules
527
14
Who Else Has My Compound?
528
15
Isomers and Molecular Structure
529
16
Reactivities of
Alkyl
Halides
in Nucleophilic
Substitution Reactions
531
17
An SN1 Reaction of Bromotriphenylmethane
533
18
Preparation and Properties of a Gaseous Alkene
534
19
Addition of Iodine to a-Pinene
536
20
Unsaturation in Commercial Products
537
21
Free-Radical Stability
538
22
The Nylon Rope Trick
539
23
Nucleophilic Substitution Rates of Alcohols
541
24
Photoreduction of Benzophenone
542
25
Oxidation of Alcohols by Potassium Permanganate
543
26
Preparation of a Fluorescent Dye
544
27
Diels-Alder Reaction of Maleic Anhydride
and
Furan
546
28
Identification of an Unknown
Arene
by NMR
Spectrometry
547
29
Interpretation of a Mass Spectrum
548
30
Nitration of Naphthalene
549
31
Preparation of Carbocations by the Friedel-Crafts
Reaction
551
32
Air Oxidation of Fluorene to 9-Fluorenone
552
33
A Nucleophilic Addition-Elimination Reaction of
Benzii
553
34
Preparation of Aldol Condensation Products
554
35
A Spontaneous Reaction of
Benzaldehyde 556
36
Acid-Base Strengths of Organic Compounds
556
37
Hydrolysis Rates of Esters
558
38
Preparation of Benzamide
559
39
Synthesis of Dimedone Derivatives
of
Benzaldehyde 560
Contents
ix
40
A Diazonium Salt Reaction of 2-Aminobenzoic
Acid
561
41 Beckmann
Rearrangement of Benzophenone
Oxime
562
42
Dyeing with Indigo
563
43
Reactions of Monosaccharides with Phenols
44
Isolation of Trimyristin from Nutmeg
567
45
Preparation of a Soap Using a Phase-Transfer
Catalyst
568
46
Isolation of a Protein from Milk
568
565
Part IV Qualitative Organic Analysis
571
An Overview of
Qual
Organic
572
Preliminary Work
573
Purification
573
Measurement of Physical Constants
573
Physical Examination
574
Ignition Test
574
Classification
575
Solubility Tests
575
Classification Tests
579
Spectral Analysis
595
Infrared Spectra
595
NMR Spectra
596
Identification
596
List of Possibilities
596
Additional Tests and Data
597
Preparation of Derivatives
598
Report
616
Exercises
616
Part V Laboratory Operations
619
A. Basic Operations
620
1
Cleaning and Drying Glassware
620
2
Using Specialized Glassware
622
3
Using Glass Rod and Tubing
626
4
Weighing
629
5
Measuring Volume
631
6
Making Transfers
636
B. Operations for Conducting Chemical Reactions
640
7
Heating
640
a. Heat Sources
640
b. Smooth Boiling Devices
649
с
Heating Under Reflux
650
8
Cooling
655
9
Temperature Monitoring
657
10
Mixing
658
11
Addition of Reactants
661
12
Excluding Water from Reaction Mixtures
664
a. Using Drying Tubes
664
b. Water Separation
665
13
Excluding Air from Reaction Mixtures
666
14
Trapping Gases
668
C. Separation Operations
671
15
Gravity Filtration
671
16
Vacuum Filtration
676
17
Centrifugation
680
18
Extraction
682
a. Liquid-Liquid Extraction
682
b. Salting Out
693
с
Liquid-Solid Extraction
693
19
Evaporation
694
20
Steam Distillation
700
a. External Steam Distillation
702
b. Internal Steam Distillation
705
21
Column Chromatography
707
a. Liquid-Solid Column Chromatography
708
b. Flash Chromatography
718
с
Reversed-Phase Column Chromatography
22
Thin-Layer Chromatography
720
23
Paper Chromatography
728
D. Washing and Drying Operations
733
24
Washing Liquids
733
25
Drying Liquids
735
26
Washing and Drying Solids
741
a. Washing Solids
742
b. Drying Solids
743
27
Cleaning and Drying Gases
746
E. Purification Operations
748
28
Recrystallization
748
a. Recrystallization from a Single Solvent
749
b. Recrystallization from Mixed Solvents
763
c. Choosing a Recrystallization Solvent
764
29
Sublimation
766
30
Simple Distillation
769
a. Distillation of Liquids
769
b. Distillation of Solids
782
31
Vacuum Distillation
783
32
Fractional Distillation
795
720
Contents
F.
Measuring Physical
Constants
808
33
Melting
Point
808
34
Boiling
Point
816
a. Distillation
Boiling
Point
817
b.
Capillary-Tube Boiling
Point
818
35
Refractive
Index
821
36
Optical
Rotation
825
G. Instrumental
Analysis
831
37 Gas
Chromatography
831
38 High-Performance Liquid
Chromatography
842
39
Infrared
Spectrometry
846
40
Nuclear Magnetic Resonance
Spectrometry
Interpretation of Infrared Spectra
861
a.
λΗ
NMR Spectrometry
876
b. 13C NMR Spectrometry
889
41
Ultraviolet-Visible Spectrometry
891
a. UV-VIS Spectra
892
b. Colorimetry
895
42
Mass Spectrometry
897
Interpretation of Mass Spectra
902
875
Appendixes and Bibliography
907
I Laboratory Equipment
908
II Keeping a Laboratory Notebook
912
III Writing a Laboratory Report
913
IV Calculations for Organic Synthesis
918
V Planning an Experiment
922
VI Properties of Organic Compounds
923
VII
The Chemical Literature
933
Bibliography
948
Index
955
|
adam_txt |
Contents
Preface
xi
To the Instructor
xi
Acknowledgments
xiii
Introduction
1
Problem Solving in the Organic Chemistry Laboratory
Scientific Methodology
2
Organization of This Book
6
A Guide to Success in the Organic Chemistry Lab
9
Laboratory Safety
13
Safety Standards
14
Protecting Yourself
14
Preventing Laboratory Accidents
14
Reacting to Accidents: First Aid
16
Reacting to Accidents: Fire
19
Chemical Hazards
19
Finding and Using Chemical Safety Information
23
Chemistry and tbe Environment
31
Disposal of Hazardous Wastes
32
Green Chemistry
32
Part I Mastering the Operations
39
1
Learning Basic Operations. The Effect of
pH
on a Food
Preservative
40
2
Extraction and Evaporation. Separating
the Components of "Panacetin"
48
3
Recrystallization and Melting-Point
Measurement. Identifying a Constituent
of "Panacetin"
56
4
Heating Under Reflux. Synthesis of Salicylic Acid from
Wintergreen
Oil
61
5
Simple Distillation, Gas Chromatography. Preparation
of Synthetic Banana Oil
70
6
Fractional Distillation. Separation of Petroleum
Hydrocarbons
79
7
Addition, Sublimation. A Green Synthesis
of Camphor
86
8
Boiling Point, Refractive Index. Identification
of a Petroleum Hydrocarbon
93
9
Column Chromatography, UV-VIS Spectrometry.
Isolation and Isomerization of Lycopene from Tomato
Paste
100
10
Steam Distillation, Infrared Spectrometry. Isolation and
Identification of the Major Constituent of Clove Oil
109
11
Thin-Layer Chromatography, NMR Spectrometry.
Identification of Unknown Ketones
117
12
Vacuum Distillation, Optical Rotation. The Optical
Activity of a-Pinene: A Chemical Mystery
124
Part II Correlated Laboratory Experiments
131
13
Investigation of a Chemical Bond by Infrared
Spectrometry
132
14
Properties of Common Functional Groups
139
15
Thin-Layer
Chromatographie
Analysis of Drug
Components
147
16
Separation of an Alkane Clathrate
152
17
Isomers and Isomerization Reactions
160
18
Structures and Properties of Stereoisomers
166
19
Bridgehead Reactivity in an SN1 Solvolysis
Reaction
174
20
Reaction of Iodoethane with Sodium Saccharin,
an Ambident Nucleophile
182
21
Dehydration of Methylcyclohexanols and the Evelyn
Effect
188
22
Testing Markovnikov's Rule
199
23
Stereochemistry of Bromine Addition to
íraní-Cinnamic
Acid
208
24
A Green Synthesis of Adipic Acid
216
25
Preparation of Bromotriphenylmethane and the Trityl
Free Radical
223
vii
viii
Contents
26
Chain-Growth Polymerization of
Styrene
and Methyl
Methacrylate
232
27
Synthesis of
Ethanol
by Fermentation
241
28
Reaction of Butanols with Hydrobromic Acid
250
29
Borohydride Reduction of Vanillin to Vanillyl
Alcohol
260
30
Synthesis of Triphenylmethanol and the Trityl
Carbocation
269
31
An Unexpected Reaction of
2,3-Dimethyl-2,3-
butanediol
281
32
Identification of a Conjugated
Diene
from
Eucalyptus Oil
287
33
Spectral Identification of Monoterpenes
295
34
Synthesis and Spectral Analysis of Aspirin
302
35
Directive Effects in the
Bromina tion
of Vanillin
311
36
Mechanism of the Nitration of
Arenes
by Nitronium
Fluoborate
316
37
Friedel-Crafts Acylation of
Anisóle
323
38
Determination of the Structure of a Natural Product in
Anise Oil
333
39
Identification of an Oxygen-Containing Organic
Compound
340
40
Oxidation of the Insect Repellent
"6-12" 347
41
Isomerization of a Cyclic
Ketone
354
42
A
Wittig
Reaction of irans-Cinnamaldehyde
361
43
Effect of Reaction Conditions on the Condensation
of Furfural with Cyclopentanone
370
44
Electronic Effect of
a para-lodo
Substituent
380
45
Synthesis and Identification of an Unknown Carboxylic
Acid
389
46
Preparation of the Insect Repellent
ЛТ
iV-Diethyl-meŕe-
toluamide
395
47
Synthesis of Dimedone and Measurement of Its
Tautomerie
Equilibrium Constant
406
48
Preparation of Para Red and Related
Azo
Dyes
415
49
Reaction of Phthalimide with Sodium
Hypochlorite
424
50
Identification of an Unknown
Amine
434
51
Preparation and Mass Spectrum of 2-Phenylindole
442
52
Nucleophilic Strength and Reactivity in SNAr
Reactions
452
53
Structure of an Unknown D-Hexose
459
54
Fatty Acid Content of Commercial Cooking Oils
468
55
Structure of an Unknown Dipeptide
477
56
Multistep Synthesis of Benzilic Acid from
Benzaldehyde 487
57
Using the Chemical Literature in an Organic
Synthesis
497
58
A Research Project in Organic Chemistry
504
Partili
Minilabs 515
1
Making Useful Laboratory Items
516
2
Extraction of Iodine by Dichloromethane
517
3
Purification of an Unknown Compound
by Recrystallization
518
4
Developing and Testing a Hypothesis
518
5
Preparation of Acetate Esters
520
6 Gas Chromatographie
Analysis of Commercial
Xylene
521
7
Isolation of an Expectorant from Cough Capsules
522
8
A Missing-Label Puzzle
523
9
Paper Chromatography of Dyes in Commercial Drink
Mixes
523
10 Gas Chromatographie
Analysis of an Essential Oil from
Orange Peel
525
11
Identification of an Unknown Felt-Tip Pen Ink
by
TLC
526
12
Optical Rotation of Turpentine
527
13
The Structures of Organic Molecules
527
14
Who Else Has My Compound?
528
15
Isomers and Molecular Structure
529
16
Reactivities of
Alkyl
Halides
in Nucleophilic
Substitution Reactions
531
17
An SN1 Reaction of Bromotriphenylmethane
533
18
Preparation and Properties of a Gaseous Alkene
534
19
Addition of Iodine to a-Pinene
536
20
Unsaturation in Commercial Products
537
21
Free-Radical Stability
538
22
The Nylon Rope Trick
539
23
Nucleophilic Substitution Rates of Alcohols
541
24
Photoreduction of Benzophenone
542
25
Oxidation of Alcohols by Potassium Permanganate
543
26
Preparation of a Fluorescent Dye
544
27
Diels-Alder Reaction of Maleic Anhydride
and
Furan
546
28
Identification of an Unknown
Arene
by NMR
Spectrometry
547
29
Interpretation of a Mass Spectrum
548
30
Nitration of Naphthalene
549
31
Preparation of Carbocations by the Friedel-Crafts
Reaction
551
32
Air Oxidation of Fluorene to 9-Fluorenone
552
33
A Nucleophilic Addition-Elimination Reaction of
Benzii
553
34
Preparation of Aldol Condensation Products
554
35
A Spontaneous Reaction of
Benzaldehyde 556
36
Acid-Base Strengths of Organic Compounds
556
37
Hydrolysis Rates of Esters
558
38
Preparation of Benzamide
559
39
Synthesis of Dimedone Derivatives
of
Benzaldehyde 560
Contents
ix
40
A Diazonium Salt Reaction of 2-Aminobenzoic
Acid
561
41 Beckmann
Rearrangement of Benzophenone
Oxime
562
42
Dyeing with Indigo
563
43
Reactions of Monosaccharides with Phenols
44
Isolation of Trimyristin from Nutmeg
567
45
Preparation of a Soap Using a Phase-Transfer
Catalyst
568
46
Isolation of a Protein from Milk
568
565
Part IV Qualitative Organic Analysis
571
An Overview of
Qual
Organic
572
Preliminary Work
573
Purification
573
Measurement of Physical Constants
573
Physical Examination
574
Ignition Test
574
Classification
575
Solubility Tests
575
Classification Tests
579
Spectral Analysis
595
Infrared Spectra
595
NMR Spectra
596
Identification
596
List of Possibilities
596
Additional Tests and Data
597
Preparation of Derivatives
598
Report
616
Exercises
616
Part V Laboratory Operations
619
A. Basic Operations
620
1
Cleaning and Drying Glassware
620
2
Using Specialized Glassware
622
3
Using Glass Rod and Tubing
626
4
Weighing
629
5
Measuring Volume
631
6
Making Transfers
636
B. Operations for Conducting Chemical Reactions
640
7
Heating
640
a. Heat Sources
640
b. Smooth Boiling Devices
649
с
Heating Under Reflux
650
8
Cooling
655
9
Temperature Monitoring
657
10
Mixing
658
11
Addition of Reactants
661
12
Excluding Water from Reaction Mixtures
664
a. Using Drying Tubes
664
b. Water Separation
665
13
Excluding Air from Reaction Mixtures
666
14
Trapping Gases
668
C. Separation Operations
671
15
Gravity Filtration
671
16
Vacuum Filtration
676
17
Centrifugation
680
18
Extraction
682
a. Liquid-Liquid Extraction
682
b. Salting Out
693
с
Liquid-Solid Extraction
693
19
Evaporation
694
20
Steam Distillation
700
a. External Steam Distillation
702
b. Internal Steam Distillation
705
21
Column Chromatography
707
a. Liquid-Solid Column Chromatography
708
b. Flash Chromatography
718
с
Reversed-Phase Column Chromatography
22
Thin-Layer Chromatography
720
23
Paper Chromatography
728
D. Washing and Drying Operations
733
24
Washing Liquids
733
25
Drying Liquids
735
26
Washing and Drying Solids
741
a. Washing Solids
742
b. Drying Solids
743
27
Cleaning and Drying Gases
746
E. Purification Operations
748
28
Recrystallization
748
a. Recrystallization from a Single Solvent
749
b. Recrystallization from Mixed Solvents
763
c. Choosing a Recrystallization Solvent
764
29
Sublimation
766
30
Simple Distillation
769
a. Distillation of Liquids
769
b. Distillation of Solids
782
31
Vacuum Distillation
783
32
Fractional Distillation
795
720
Contents
F.
Measuring Physical
Constants
808
33
Melting
Point
808
34
Boiling
Point
816
a. Distillation
Boiling
Point
817
b.
Capillary-Tube Boiling
Point
818
35
Refractive
Index
821
36
Optical
Rotation
825
G. Instrumental
Analysis
831
37 Gas
Chromatography
831
38 High-Performance Liquid
Chromatography
842
39
Infrared
Spectrometry
846
40
Nuclear Magnetic Resonance
Spectrometry
Interpretation of Infrared Spectra
861
a.
λΗ
NMR Spectrometry
876
b. 13C NMR Spectrometry
889
41
Ultraviolet-Visible Spectrometry
891
a. UV-VIS Spectra
892
b. Colorimetry
895
42
Mass Spectrometry
897
Interpretation of Mass Spectra
902
875
Appendixes and Bibliography
907
I Laboratory Equipment
908
II Keeping a Laboratory Notebook
912
III Writing a Laboratory Report
913
IV Calculations for Organic Synthesis
918
V Planning an Experiment
922
VI Properties of Organic Compounds
923
VII
The Chemical Literature
933
Bibliography
948
Index
955 |
any_adam_object | 1 |
any_adam_object_boolean | 1 |
author | Lehman, John W. |
author_facet | Lehman, John W. |
author_role | aut |
author_sort | Lehman, John W. |
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building | Verbundindex |
bvnumber | BV035101761 |
callnumber-first | Q - Science |
callnumber-label | QD261 |
callnumber-raw | QD261 |
callnumber-search | QD261 |
callnumber-sort | QD 3261 |
callnumber-subject | QD - Chemistry |
classification_rvk | VK 5100 VK 7100 |
ctrlnum | (OCoLC)191865810 (DE-599)BVBBV035101761 |
dewey-full | 547.0078 |
dewey-hundreds | 500 - Natural sciences and mathematics |
dewey-ones | 547 - Organic chemistry |
dewey-raw | 547.0078 |
dewey-search | 547.0078 |
dewey-sort | 3547.0078 |
dewey-tens | 540 - Chemistry and allied sciences |
discipline | Chemie / Pharmazie |
discipline_str_mv | Chemie / Pharmazie |
edition | 2nd ed. |
format | Book |
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id | DE-604.BV035101761 |
illustrated | Not Illustrated |
index_date | 2024-07-02T22:14:26Z |
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institution | BVB |
isbn | 9780132413756 0132413752 |
language | English |
lccn | 2008005082 |
oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-016769730 |
oclc_num | 191865810 |
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physical | XIII, 970 S. |
publishDate | 2009 |
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publisher | Pearson Prentice Hall |
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spelling | Lehman, John W. Verfasser aut Multiscale operational organic chemistry a problem-solving approach to the laboratory course John W. Lehman 2nd ed. Upper Saddle River, N.J. Pearson Prentice Hall c2009 XIII, 970 S. txt rdacontent n rdamedia nc rdacarrier Chemistry, Organic Laboratory manuals Praktikum (DE-588)4127380-1 gnd rswk-swf Experiment (DE-588)4015999-1 gnd rswk-swf Labortechnik (DE-588)4123602-6 gnd rswk-swf Organische Chemie (DE-588)4043793-0 gnd rswk-swf Organische Chemie (DE-588)4043793-0 s Praktikum (DE-588)4127380-1 s DE-604 Experiment (DE-588)4015999-1 s Labortechnik (DE-588)4123602-6 s 1\p DE-604 Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016769730&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
spellingShingle | Lehman, John W. Multiscale operational organic chemistry a problem-solving approach to the laboratory course Chemistry, Organic Laboratory manuals Praktikum (DE-588)4127380-1 gnd Experiment (DE-588)4015999-1 gnd Labortechnik (DE-588)4123602-6 gnd Organische Chemie (DE-588)4043793-0 gnd |
subject_GND | (DE-588)4127380-1 (DE-588)4015999-1 (DE-588)4123602-6 (DE-588)4043793-0 |
title | Multiscale operational organic chemistry a problem-solving approach to the laboratory course |
title_auth | Multiscale operational organic chemistry a problem-solving approach to the laboratory course |
title_exact_search | Multiscale operational organic chemistry a problem-solving approach to the laboratory course |
title_exact_search_txtP | Multiscale operational organic chemistry a problem-solving approach to the laboratory course |
title_full | Multiscale operational organic chemistry a problem-solving approach to the laboratory course John W. Lehman |
title_fullStr | Multiscale operational organic chemistry a problem-solving approach to the laboratory course John W. Lehman |
title_full_unstemmed | Multiscale operational organic chemistry a problem-solving approach to the laboratory course John W. Lehman |
title_short | Multiscale operational organic chemistry |
title_sort | multiscale operational organic chemistry a problem solving approach to the laboratory course |
title_sub | a problem-solving approach to the laboratory course |
topic | Chemistry, Organic Laboratory manuals Praktikum (DE-588)4127380-1 gnd Experiment (DE-588)4015999-1 gnd Labortechnik (DE-588)4123602-6 gnd Organische Chemie (DE-588)4043793-0 gnd |
topic_facet | Chemistry, Organic Laboratory manuals Praktikum Experiment Labortechnik Organische Chemie |
url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016769730&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
work_keys_str_mv | AT lehmanjohnw multiscaleoperationalorganicchemistryaproblemsolvingapproachtothelaboratorycourse |