On the control of riboflavin (vitamin B 2) crystal structures:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Aachen
Shaker
2007
|
| Schriftenreihe: | Berichte aus der Verfahrenstechnik
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | 100 S. Ill., graph. Darst. |
| ISBN: | 9783832260644 3832260641 |
Internformat
MARC
| LEADER | 00000nam a2200000 c 4500 | ||
|---|---|---|---|
| 001 | BV026604467 | ||
| 003 | DE-604 | ||
| 005 | 20110228 | ||
| 007 | t | ||
| 008 | 110326s2007 ad|| m||| 00||| eng d | ||
| 015 | |a 07,N23,1340 |2 dnb | ||
| 015 | |a 07,A28,1463 |2 dnb | ||
| 016 | 7 | |a 984191925 |2 DE-101 | |
| 020 | |a 9783832260644 |9 978-3-8322-6064-4 | ||
| 020 | |a 3832260641 |9 3-8322-6064-1 | ||
| 035 | |a (OCoLC)918184402 | ||
| 035 | |a (DE-599)DNB984191925 | ||
| 040 | |a DE-604 |b ger |e rakwb | ||
| 041 | 0 | |a eng | |
| 049 | |a DE-188 | ||
| 082 | 0 | |a 660.284298 |2 22/ger | |
| 082 | 0 | |a 661.8 |2 22/ger | |
| 084 | |a 660 |2 sdnb | ||
| 100 | 1 | |a Mohnicke, Mandy |d 1976- |e Verfasser |0 (DE-588)133026361 |4 aut | |
| 245 | 1 | 0 | |a On the control of riboflavin (vitamin B 2) crystal structures |c Mandy Mohnicke |
| 264 | 1 | |a Aachen |b Shaker |c 2007 | |
| 300 | |a 100 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a Berichte aus der Verfahrenstechnik | |
| 502 | |a Zugl.: Halle-Wittenberg, Univ., Diss., 2006 | ||
| 650 | 0 | 7 | |a Prozessführung |g Technik |0 (DE-588)4197295-8 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Herstellung |0 (DE-588)4159653-5 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Vitamin B2 |0 (DE-588)4188444-9 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Kristallstrukturanalyse |0 (DE-588)4137204-9 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Kristallisation |0 (DE-588)4033215-9 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Trocknung |0 (DE-588)4124329-8 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Vitamin B2 |0 (DE-588)4188444-9 |D s |
| 689 | 0 | 1 | |a Kristallstrukturanalyse |0 (DE-588)4137204-9 |D s |
| 689 | 0 | |5 DE-604 | |
| 689 | 1 | 0 | |a Vitamin B2 |0 (DE-588)4188444-9 |D s |
| 689 | 1 | 1 | |a Herstellung |0 (DE-588)4159653-5 |D s |
| 689 | 1 | 2 | |a Kristallisation |0 (DE-588)4033215-9 |D s |
| 689 | 1 | 3 | |a Trocknung |0 (DE-588)4124329-8 |D s |
| 689 | 1 | 4 | |a Prozessführung |g Technik |0 (DE-588)4197295-8 |D s |
| 689 | 1 | |5 DE-604 | |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022159831&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 999 | |a oai:aleph.bib-bvb.de:BVB01-022159831 | ||
Datensatz im Suchindex
| _version_ | 1804145202252742656 |
|---|---|
| adam_text | BERICHTE AUS DER VERFAHRENSTECHNIK
MANDY MOHNICKE
ON THE CONTROL OF RIBOFLAVIN
(VITAMIN B
2
) CRYSTAL STRUCTURES
SHAKER VERLAG
AACHEN 2007
TABLE OF CONTENT
1. INTRODUCTION 5
2. STATE OF THE ART _ _._ 6
2.1 STRUCTURAL FUNDAMENTALS 6
2.1.1 CRYSTAL SYSTEMS AND LATTICES 6
2.1.2 CRYSTAL FORM, SHAPE AND CRYSTAL HABIT 8
2.2 POLYMORPHS, SOLVATES AND HYDRATES 10
2.3 PHASE LIABILITY AND PHASE
TRANSFORMATION................................. 12
2.4 IMPACT OF SOLID-STATE PROPERTIES ON APPLICATION AND PROCESSABLLITY
OF
POLYMORPHS AND SOLVATEI 16
2.5 CONTROLLING THE CRYSTAL STRUCTURE OF POLYMORPHS AND SOLVATES DARING
PROCESSING 17
2.5.1 EFFECTS OF PROCESSING, ALTER TREATMENT AND STORAGE ON THE CRYSTAL
STRUCTURE OF POLYMORPHS AND SOLVATES 19
2.6 ANALYTICAL TECHNIQUES FOR STUDYING AAD CHARACTERIZING POTYMORPNS AND
MLVATES 20
2.6.1 OPTICAL MICROSCOPY 20
2.6.2 THERMAL METHODS 22
2.6.3 X-RAY CRYSTALLOGRAPHY 23
2.6.4 SOLUBILITY ANALYSIS 24
2.7 RIBOFLAVIN 25
2.7.1 INDUSTRIAL PRODUCTION OF RIBOFLAVIN 26
2.7.2 CRYSTAL STRUCTURAL ASPECTS OF RIBOFLAVIN 26
2.8 AIM OF THE PRESENT WORK, 28
3. PHASE CHARACTERIZATION OF RIBOFLAVIN 29
3.1 POWDER XRD ANALYTIC! OR RIBOFLAVIN CRYSTAL STRUCTURES 29
3.2 NOMENCLATURE AND STRUCTURAL RELATIONSHIP* OF RIBOFLAVIN CRYSTAL
STRUCTURES 32
3J THERMO ANALYTICS OF RIBAFLAVIN CRYSTAL STRUCTURE* _ 33
3.4 SOLUBILITY ANALYTICS OF RIBOFLAVIN CRYSTAL STRUCTURES 35
3.5 DISSOLUTION KINETICS OF RIBOFLAVIN CRYSTAL STRUCTURES 36
3.6 OPTICAL CHARACTERIZATION OF CRYSTALLINE AND AMORPHOUS RIBOFLAVIN 38
3.6.1 RIBOFLAVIN ANHYDRATE I - TYPE A RIBOFLAVIN 38
3.6.2 RIBOFLAVIN MONOHYDRATE II - TYPE B/C RIBOFLAVIN 39
3.6.3 RIBOFLAVIN DIHYDRATE II - TYPE F RIBOFLAVIN 40
3.6.4 RIBOFLAVIN TETRAHYDRATE IN * TYPE E RIBOFLAVIN 41
3.6.5 RIBOFLAVIN X? HYDRATE III - TYPE E, RIBOFLAVIN 41
3.6.6 RIBOFLAVIN ANHYDRATE II - TYPE B/CO AND RIBOFLAVIN ANHYDRATE LIT -
TYPE E0... 42
3.7 AMORPHOUS RIBOFLAVIN 41
4. IMPACT OF PROCESS PARAMETERS ON CRYSTAL STRUCTURE AND
SOLID-STATE PROPERTIES OF RIBOFLAVIN 45
4.1 INFLUENCE OF PROCESS PANTMETEN ON PHASE STABILITY NND PHASE
TRANSITION
BEHAVIOUR ORRIBOFTAVT* 45
4.1.1 INFLUENCE OF TEMPERATURE 45
4.1.2 INFLUENCE OF PH 47
4.1.3 INFLUENCE OF SOLVENT 48
4.2 INFLUENCE OF PHASE TRANSITION PROCESSES ON COLOUR AND TEITNRE SF
RIBOFLAVIN. 49
43 INFLUENCE OF DRYING PROCESSES ON CRYSTAL STRUCTURE AAD SOND-STAFI-
DWRACTERLSIKIOFRIBAFLNVLN - 51
4.3.1 INFLUENCE OF SURROUNDING SOLVENT AND SOLVENT CONCENTRATION ON THE
CRYSTAL STRUCTURE
OF DRIED RIBOFLAVIN 54
5. CONTROL OF RIBOFLAVIN CRYSTAL STRUCTURES DURING
CRYSTALLIZATION 56
5.1 METASTAME ZONE WIDTH 56
5.2 VARIATION OF PRODUCTION METHODS IN THE CRYSTALLIZATION OF RIBOFLAVIN
57
5.2.1 BATCH CRYSTALLIZATION OF RIBOFLAVIN 58
5.2.2 SEEDED BATCH CRYSTALLIZATION OF RIBAFLAVIN 60
5J SPRAY DRYING TECHNIQUES IN THE CRYSTALLIZATION OF RIBOFLAVIN 61
5.3.1 INFLUENCE OF PROCESS PARAMETERS ON CRYSTAL STRUCTURE AND
SOLID-STATE
PROPERTIES OF SPRAY DRIED RIBOFLAVIN 61
5.3.2 INFLUENCE OF PH AND TEMPERATURE ON THE CRYSTAL STRUCTURE OF SPRAY
DRIED
RIBOFLAVIN 64
5.4 ART OF KNOWLEDGE IN THE CONTROL OF RIBOFLAVIN CRYSTAL STRUCTURES 66
5.5 SUMMARY OF THE EXPERIMENTAL RESULTS 67
6. DISCUSSION OF ERRORS 68
6.1 SOURCES OF ERRORS IN THE SAMPLING OF RIBOFLAVIN 68
6.2 SOURCE OR ERRORS IN THE PHASE ANALYSIS OF RIBOFLAVIN ~ 69
6.2.1 THERMAL ANALYSIS 69
6.2.2 POWDER XRD ANALYSIS 70
6.2.3 SOLUBILITY ANALYTICS - INTERACTIONS OF PHASE TRANSFORMATION AND
DISSOLUTION
PROCESSES. , 70
7. DISCUSSION * 73
7.1 RIBOFLAVUI CRYSTAL STRUCTURES 73
7.1.2 CONCLUSION 75
7.2 PNASE TRANSITION AND PHASE STABILITY OF RIBOFLAVIN CRYSTAL
STRUCTURES 75
7.2.L CONCLUSION 81
73 CRYSTALLIZATION OF DIFFERENT RIBOFLAVIN CRYSTAL STRUCTURES 81
7.3.1 INFLUENCE OF PROCESS PARAMETERS ON THE CRYSTAL STRUCTURE
RIBOFLAVIN 81
7.3.2 CONTROLLING THE SOLID-STATE-PROPERTIES OF RIBOFLAVIN BY ACTIVE
PROCESS
PARAMETER CONTROL 84
7.3.3 CONCLUSION 84
7A OUTLOOK 84
8. SUMMARY 85
9. ZUSAMMENFASSUNG 87
10. NOMENCLATURE 90
11. REFERENCES _ 91
|
| any_adam_object | 1 |
| author | Mohnicke, Mandy 1976- |
| author_GND | (DE-588)133026361 |
| author_facet | Mohnicke, Mandy 1976- |
| author_role | aut |
| author_sort | Mohnicke, Mandy 1976- |
| author_variant | m m mm |
| building | Verbundindex |
| bvnumber | BV026604467 |
| ctrlnum | (OCoLC)918184402 (DE-599)DNB984191925 |
| dewey-full | 660.284298 661.8 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering 661 - Technology of industrial chemicals |
| dewey-raw | 660.284298 661.8 |
| dewey-search | 660.284298 661.8 |
| dewey-sort | 3660.284298 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie |
| format | Thesis Book |
| fullrecord | <?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>02228nam a2200565 c 4500</leader><controlfield tag="001">BV026604467</controlfield><controlfield tag="003">DE-604</controlfield><controlfield tag="005">20110228 </controlfield><controlfield tag="007">t</controlfield><controlfield tag="008">110326s2007 ad|| m||| 00||| eng d</controlfield><datafield tag="015" ind1=" " ind2=" "><subfield code="a">07,N23,1340</subfield><subfield code="2">dnb</subfield></datafield><datafield tag="015" ind1=" " ind2=" "><subfield code="a">07,A28,1463</subfield><subfield code="2">dnb</subfield></datafield><datafield tag="016" ind1="7" ind2=" "><subfield code="a">984191925</subfield><subfield code="2">DE-101</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">9783832260644</subfield><subfield code="9">978-3-8322-6064-4</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">3832260641</subfield><subfield code="9">3-8322-6064-1</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)918184402</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)DNB984191925</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-604</subfield><subfield code="b">ger</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1="0" ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-188</subfield></datafield><datafield tag="082" ind1="0" ind2=" "><subfield code="a">660.284298</subfield><subfield code="2">22/ger</subfield></datafield><datafield tag="082" ind1="0" ind2=" "><subfield code="a">661.8</subfield><subfield code="2">22/ger</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">660</subfield><subfield code="2">sdnb</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Mohnicke, Mandy</subfield><subfield code="d">1976-</subfield><subfield code="e">Verfasser</subfield><subfield code="0">(DE-588)133026361</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">On the control of riboflavin (vitamin B 2) crystal structures</subfield><subfield code="c">Mandy Mohnicke</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">Aachen</subfield><subfield code="b">Shaker</subfield><subfield code="c">2007</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">100 S.</subfield><subfield code="b">Ill., graph. Darst.</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="490" ind1="0" ind2=" "><subfield code="a">Berichte aus der Verfahrenstechnik</subfield></datafield><datafield tag="502" ind1=" " ind2=" "><subfield code="a">Zugl.: Halle-Wittenberg, Univ., Diss., 2006</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Prozessführung</subfield><subfield code="g">Technik</subfield><subfield code="0">(DE-588)4197295-8</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Herstellung</subfield><subfield code="0">(DE-588)4159653-5</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Vitamin B2</subfield><subfield code="0">(DE-588)4188444-9</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Kristallstrukturanalyse</subfield><subfield code="0">(DE-588)4137204-9</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Kristallisation</subfield><subfield code="0">(DE-588)4033215-9</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Trocknung</subfield><subfield code="0">(DE-588)4124329-8</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="655" ind1=" " ind2="7"><subfield code="0">(DE-588)4113937-9</subfield><subfield code="a">Hochschulschrift</subfield><subfield code="2">gnd-content</subfield></datafield><datafield tag="689" ind1="0" ind2="0"><subfield code="a">Vitamin B2</subfield><subfield code="0">(DE-588)4188444-9</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="1"><subfield code="a">Kristallstrukturanalyse</subfield><subfield code="0">(DE-588)4137204-9</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="689" ind1="1" ind2="0"><subfield code="a">Vitamin B2</subfield><subfield code="0">(DE-588)4188444-9</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2="1"><subfield code="a">Herstellung</subfield><subfield code="0">(DE-588)4159653-5</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2="2"><subfield code="a">Kristallisation</subfield><subfield code="0">(DE-588)4033215-9</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2="3"><subfield code="a">Trocknung</subfield><subfield code="0">(DE-588)4124329-8</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2="4"><subfield code="a">Prozessführung</subfield><subfield code="g">Technik</subfield><subfield code="0">(DE-588)4197295-8</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">DNB Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022159831&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="999" ind1=" " ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-022159831</subfield></datafield></record></collection> |
| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV026604467 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T23:15:42Z |
| institution | BVB |
| isbn | 9783832260644 3832260641 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-022159831 |
| oclc_num | 918184402 |
| open_access_boolean | |
| owner | DE-188 |
| owner_facet | DE-188 |
| physical | 100 S. Ill., graph. Darst. |
| publishDate | 2007 |
| publishDateSearch | 2007 |
| publishDateSort | 2007 |
| publisher | Shaker |
| record_format | marc |
| series2 | Berichte aus der Verfahrenstechnik |
| spelling | Mohnicke, Mandy 1976- Verfasser (DE-588)133026361 aut On the control of riboflavin (vitamin B 2) crystal structures Mandy Mohnicke Aachen Shaker 2007 100 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Berichte aus der Verfahrenstechnik Zugl.: Halle-Wittenberg, Univ., Diss., 2006 Prozessführung Technik (DE-588)4197295-8 gnd rswk-swf Herstellung (DE-588)4159653-5 gnd rswk-swf Vitamin B2 (DE-588)4188444-9 gnd rswk-swf Kristallstrukturanalyse (DE-588)4137204-9 gnd rswk-swf Kristallisation (DE-588)4033215-9 gnd rswk-swf Trocknung (DE-588)4124329-8 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Vitamin B2 (DE-588)4188444-9 s Kristallstrukturanalyse (DE-588)4137204-9 s DE-604 Herstellung (DE-588)4159653-5 s Kristallisation (DE-588)4033215-9 s Trocknung (DE-588)4124329-8 s Prozessführung Technik (DE-588)4197295-8 s DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022159831&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Mohnicke, Mandy 1976- On the control of riboflavin (vitamin B 2) crystal structures Prozessführung Technik (DE-588)4197295-8 gnd Herstellung (DE-588)4159653-5 gnd Vitamin B2 (DE-588)4188444-9 gnd Kristallstrukturanalyse (DE-588)4137204-9 gnd Kristallisation (DE-588)4033215-9 gnd Trocknung (DE-588)4124329-8 gnd |
| subject_GND | (DE-588)4197295-8 (DE-588)4159653-5 (DE-588)4188444-9 (DE-588)4137204-9 (DE-588)4033215-9 (DE-588)4124329-8 (DE-588)4113937-9 |
| title | On the control of riboflavin (vitamin B 2) crystal structures |
| title_auth | On the control of riboflavin (vitamin B 2) crystal structures |
| title_exact_search | On the control of riboflavin (vitamin B 2) crystal structures |
| title_full | On the control of riboflavin (vitamin B 2) crystal structures Mandy Mohnicke |
| title_fullStr | On the control of riboflavin (vitamin B 2) crystal structures Mandy Mohnicke |
| title_full_unstemmed | On the control of riboflavin (vitamin B 2) crystal structures Mandy Mohnicke |
| title_short | On the control of riboflavin (vitamin B 2) crystal structures |
| title_sort | on the control of riboflavin vitamin b 2 crystal structures |
| topic | Prozessführung Technik (DE-588)4197295-8 gnd Herstellung (DE-588)4159653-5 gnd Vitamin B2 (DE-588)4188444-9 gnd Kristallstrukturanalyse (DE-588)4137204-9 gnd Kristallisation (DE-588)4033215-9 gnd Trocknung (DE-588)4124329-8 gnd |
| topic_facet | Prozessführung Technik Herstellung Vitamin B2 Kristallstrukturanalyse Kristallisation Trocknung Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022159831&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT mohnickemandy onthecontrolofriboflavinvitaminb2crystalstructures |