Analysis for drugs and metabolites, including anti-infective agents: [based on proceedings of the eighth International Bioanalytical Forum entitled "Analysis for drugs and metabolites, including anti-infective agents", held September 5 - 8, 1989 in Guildford, UK]
Gespeichert in:
| Weitere Verfasser: | |
|---|---|
| Format: | Tagungsbericht Buch |
| Sprache: | English |
| Veröffentlicht: |
London
Royal Soc. of Chemistry
1990
|
| Schriftenreihe: | Methodological surveys in biochemistry and analysis
20 |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIV, 386 S. graph. Darst. |
| ISBN: | 0851869564 |
Internformat
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| adam_text | IMAGE 1
METHODOLOGICAL SURVEYS IN BIOCHEMISTRY AND ANALYSIS,
VOLUME 20
ANALYSIS FOR DRUGS AND
METABOLITES, INCLUDING ANTI-INFECTIVE AGENTS
EDITED BY ERIC REID GUILDFORD ACADEMIC ASSOCIATES, GUILDFORD, UNITED
KINGDOM
IAN D. WILSON ICI PHARMACEUTICAL DIVISION, MACCLESFIELD, UNITED KINGDOM
ROYAL (SOCIETY OF CHEMISTRY
IMAGE 2
CONTENTS
THE NOTES & COMMENTS ( NC ITEMS) AT THE END OF EACH SECTION INCLUDE
COMMENTS MADE AT THE FORUM ON WHICH THE BOOK IS BASED, ALONG WITH SOME
SUPPLEMENTARY MATERIAL.
SENIOR EDITOR S PREFACE, WITH AN ABBREVIATIONS LIST V
LIST OF AUTHORS XII
#A PRODUCING VALID AND ACCEPTABLE ANALYTICAL RESULTS 1
#A-1 PROBLEMS AND PITFALLS IN ANALYTICAL REQUIREMENTS FOR
PHARMACOKINETIC STUDIES BY THE MEDICINES COMMISSION - R. CALVERT & A.
MEHTA 3
#A-2 VIEWS ON METHOD VALIDATION - D. DELL 9
WITH QUESTIONNAIRE RESULTS, P. 21
#A-3 QUANTITATIVE CHARACTERIZATION OF ANALYTICAL METHODS - L.J.
PHILLIPS, J. ALEXANDER & H.M. HILL .... 23
#A-4 DATA HANDLING AND QUALITY CONTROL IN THE BIOANALYTICAL ENVIRONMENT
- F. VAN ROMPAEY, R. WOESTENBORGHS & J. HEYKANTS 37
#A-5 VALIDATION REQUIREMENTS OF BIOANALYTICAL METHODS IN RELATION TO
POSSIBLE INTERFERING AGENTS - G.S. LAND & R.D. MCDOWALL 49
#A-6 THE VALIDATION OF BIOANALYTICAL ASSAYS - R.J.N. TANNER 57
#NCA NOTES AND COMMENTS RELATING TO THE FOREGOING TOPICS 65 (FDA
VIEWPOINTS, & OTHER ITEMS, LISTED ON P. 65) INCLUDING NOTES ON:
#NCA-L EXPERIENCES AT THE INTERFACE BETWEEN THE BIOANALYST AND THE
REGULATORS - P. HAJDUKIEWICZ 67
#NCA-2 QUALITY CONTROL OF ROUTINE ASSAYS AT CONTRACT FACILITIES - R.J.
SIMMONDS & S.A. WOOD : 69
#NCA-3 QUALITY AND PRODUCTIVITY IN THE BIOANALYTICAL LABORATORY
( OUTLIERS : P. 78) - G.S. CLARKE ..75
#NCA-4 OBSERVATIONS ON THE USEFULNESS OF INTERNAL STANDARDS IN THE
ANALYSIS OF DRUGS IN BIOLOGICAL FLUIDS - I.D. WILSON 79
IMAGE 3
VIII CONTENTS
#B ANTI-INFECTIVE DRUGS AND THEIR METABOLITES 91
#B-1 A COMPARISON OF HPLC AND BIOASSAY FOR P-LACTAM ANTIBIOTICS - R.
HORTON 93
#B-2 DEVELOPMENT OF A SENSITIVE AND ROBUST ASSAY FOR THE AMINOCYCLITOL
ANTIBIOTIC, TROSPECTOMYCIN - S.A. WOOD & R.J. SIMMONDS 103
#B-3 CEFTETRAME: HPLC ASSAY PROBLEMS AND ASSEMBLY OF RESULTS - C. TOWN,
N. OLDFIELD, D. CHANG & W.A. GARLAND 109
#B-4 DEVELOPMENT OF AN EFFICIENT HPLC ANALYSIS FOR LINCOMYCIN FOR USE IN
CONTRACT LABORATORIES - C.A. JAMES, R.J. SIMMONDS & S.A. WOOD 117
#B-5 SIMULTANEOUS HPLC DETERMINATION OF TRIMETHOPRIM, SULPHAMETHOXAZOLE
AND ITS #^-ACETYL METABOLITE IN BIOLOGICAL FLUIDS - 0. VAROQUAUX, P.
CORDONNIER, C. ADVENIER & M. PAYS 123
#B-6 HPLC OF RECENT QUINOLONE ANTIMICROBIALS - KLAUS BORNER, ELLEN
BORNER, HILDEGARD HARTWIG & HARTMUT LODE 131
#B-7 QUANTITATIVE ANALYSIS OF THE ANTIFUNGAL AGENT, FLUCONAZOLE BY
CAPILLARY GAS CHROMATOGRAPHY WITH ION-TRAP DETECTION - P.V. MACRAE 145
#B-8 ASSAY METHODS FOR IMIDAZOLE- AND TRIAZOLE-LIKE ANTIFUNGALS AND FOR
SOME ANTIHELMINTHICS - R. WOESTENBORGHS & J. HEYKANTS 153
#B-9 EXPERIENCES WITH ASSAYING HYDROXYNAPHTHOQUINONES - A PROBLEM OF
SOLUBILITY? - M.V. DOIG & A.E. JONES.... 157
#B-10 ASSAY OF FAMCICLOVIR AND ITS METABOLITES, INCLUDING THE
ANTI-HERPES AGENT PENCICLOVIR, IN PLASMA AND URINE OF RAT, DOG AND MAN -
C.F. WINTON, S.E. FOWLES, R.A. VERE HODGE & D.M. PIERCE 163
#B-11 THE ANALYSIS OF ZIDOVUDINE AND ITS GLUCURONIDE METABOLITE BY HPLC
- S.S. GOOD, D.J. REYNOLDS & P. DE MIRANDA 173
#B-12 IMMUNOASSAY PROCEDURES, INCLUDING RIA, FOR THE DETECTION OF
ANTIVIRAL COMPOUNDS: ZOVIRAX AND RETROVIR AS EXAMPLES - RICHARD P.
QUINN, SARVAMANGALATADEPALU, BARBARAS. ORBAN & LEROY GERALD 185
IMAGE 4
CONTENTS IX
#NCB NOTES AND COMMENTS RELATING TO THE FOREGOING TOPICS 195 (ADDITIONAL
ASSAY CITATIONS: P. 231; ITEMIZATION, P. 195) INCLUDING NOTES ON:
#NCB-L HPLC DETERMINATION OF CEFMETAZOLE AND ITS DEGRADATION PRODUCT,
L-METHYL-LH-TETRAZOLE-5-THIOL, IN BIOLOGICAL SAMPLES - P.A. BOMBARDT,
W.M. BOTHWELL, K.S. CATHCART, M. COURTNEY, H. KO & G.W. PENG 197
#NCB-2 ANALYTICAL PROBLEMS WITH CICLOSPORIN AND ITS METABOLITES - K-FR.
SEWING, U. CHRISTIANS, J. BLECK & S. STROHMEYER 201
#NCB-3 ASSAY OF FLEROXACIN - HERWIG EGGERS, PETER HEIZMANN & DENNIS DELL
203
#NCB-4 CHIRAL STATIONARY PHASES VERSUS CHIRAL DERIVATIZATION FOR THE
QUANTISATION OF OFLOXACIN ENANTIOMERS - K-H. LEHR & P. DAMM 205
#NCB-5 AN IMIDAZOLE DERIVATIVE WITH ANTIBACTERIAL ACTIVITY IN VITRO BUT
NOT IN VIVO - G. DEAN & C.W. VOSE 207
#NCB-6 METABOLISM OF THE IMIDAZOLE GROUP IN AN ANTI- INFECTIVE
TRICHLOROPHENYLHYDRAZONE DERIVATIVE -J. W. FIRTH, P. M. STEVENS, R. D.
BROWNSILL, N. LOPEZ, CM. WALLS & C.W. VOSE 211
#NCB-7 PROBLEMS WITH THE MEASUREMENT OF ANTIVIRAL DRUGS IN BODY FLUIDS -
R.J. SIMMONDS 215
#NCB-8 IN VITRO AND IN VIVO METABOLISM OF THE ANTI- HERPES AGENT
5-(2-CHLOROETHYL)-2 -DEOXYURIDINE - I. SZINAI, ZS. VERES, K. GANZLER, J.
HEGEDUS-VAJDA & E. DE CLERCQ 219
#NCB-9 DRUG SURVIVAL IN CLINICAL SAMPLES IRRADIATED AS AN ANTI-HIV
PRECAUTION- H. DE BREE & M.P. VAN BERKEL 221
#C APPROACHES FOR VARIOUS DRUGS AND METABOLITES 239
#C-1 ON THE SELECTIVITY OF SOME RECENTLY DEVELOPED RIA S - R.
WOESTENBORGHS, I. GEUENS, H. LENOIR, C. JANSSEN & J. HEYKANTS 241
#C-2 SOME RECENT DEVELOPMENTS IN HPLC AND KINDRED TECHNIQUES - R.J.
DOLPHIN 247
#C-3 BIOANALYTICAL SUPERCRITICAL FLUID CHROMATOGRAPHY - D.W. ROBERTS &
I.D. WILSON 257
#C-4 A FULLY AUTOMATED ANALYTICAL SYSTEM USING SOLID- PHASE EXTRACTION:
APPLICATION TO THE DETERMINATION OF CARBAMAZEPINE AND TWO METABOLITES IN
PLASMA - J.B. LECAILLON, M.C. ROUAN, J. CAMPESTRINI & J.P. DUBOIS 265
IMAGE 5
X CONTENTS
#C-5 IMPROVEMENTS IN THE HPLC MEASUREMENT OF DRUG AND METABOLITE LEVELS
IN BIOLOGICAL FLUIDS - A. NICOLAS, P. LEROY, D. DECOLIN & G. SIEST 271
#C-6 HPLC-EC ANALYSIS OF HYOSCINE (SCOPOLAMINE) IN URINE - R. WHELPTON &
PETER R. HURST 279
#C-7 AN INVESTIGATION OF DIFFERENT ANALYTICAL TECHNIQUES FOR DETERMINING
LOW LEVELS OF LACIDIPINE IN PLASMA - G.L. EVANS, J. AYRTON, P. GROSSI,
M. PELLEGATTI, J. MALTAS & A.J. HARKER 285
#C-8 SOME APPLICATIONS OF MASS SPECTROMETRY IN DRUG DETECTION AND
METABOLISM STUDIES IN THE HORSE - E. HOUGHTON, P. TEALE, M.C. DUMASIA,
A. GINN, D. MARSHALL & D.B. GOWER 291
#NCC NOTES AND COMMENTS RELATING TO THE FOREGOING TOPICS 303 INCLUDING
NOTES ON:
#NCC-L SOLID-PHASE EXTRACTION AND GC-MS IDENTIFICATION OF PROPRANOLOL
AND ITS METABOLITES FROM HORSE URINE - M.C. DUMASIA, E. HOUGHTON & P.
TEALE 305
#NCC-2 THE USE OF GC-MS-MS DETECTION OF DETOMIDINE METABOLITES IN HORSE
URINE - M.A. SEYMOUR, P. TEALE & M.W. HORNER 309
#NCC-3 SOME PAST FORUM PRESENTATIONS, ESPECIALLY ON METABOLITES - E.
REID 313
#NCC-4 THE METABOLISM OF A NEW PERIPHERAL BLOOD FLOW ENHANCER - I.
SZINAI, K. GANZLER, J. HEGEDUS-VAJDA, E. GACS-BAITZ & S. HOLLY .317
#NCC-5 19 F- AND *H-NMR STUDIES OF THE METABOLISM OF
4-TRIFLUOROMETHYLBENZOIC ACID IN THE RAT - FARIDA Y.K. GHAURI, IAN D.
WILSON & JEREMY K. NICHOLSON 321
#NCC-6 THE USE OF ^N-NMR IN STUDYING THE METABOLISM OF 15 N-LABELLED
XENOBIOTICS, EXEMPLIFIED BY 15 N-ANILINE - K.E. WADE, I.D. WILSON, &
J.K. NICHOLSON 325
#NCC-7 BIOSENSORS, AN APPROACH TO DRUG ANALYSIS? - PRELIMINARY STUDIES
ON THE DEVELOPMENT OF A WARFARIN ASSAY - R. HYLAND, J. MCBRIDE, G.W.
HANLON, A.J. HUTT & C.J. OLLIFF 333
#NCC-8 FACILE PREPARATION OF CHIRAL HPLC COLUMNS BY INJECTION OF CHIRAL
ISOCYANATES DIRECTLY ONTO AMINOPROPYL COLUMNS - ROBIN WHELPTON & DENNIS
G. BUCKLEY 337
#NCC-9 HPLC ANALYSIS OF 3-HYDROXYPYRIDIN-4-ONES: NOVEL ORALLY ACTIVE
IRON CHELATORS - R.O. EPEMOLU, R.C. HIDER & L.A. DAMANI 341
IMAGE 6
CONTENTS XI
#NCC-10 PROBLEMS IN THE HPLC OF SOME METAL-CHELATING COMPOUNDS - R.J.
RUANE, D.W. ROBERTS & I.D. WILSON 343
#NCC-LL RADIO-TLC OF LI4 C-PARACETAMOL AND ITS METABOLITES WITH OFF-LINE
IDENTIFICATION USING FAB-MS WITHOUT ANALYTE ELUTION - TRACER SPURWAY,
PAUL J. PHILLIPS, IAN D. WILSON & ALAN WARRANDER 347
#NCC-12 THE POTENTIAL USE OF A TLC-FAB-MS INTERFACE IN DRUG DEVELOPMENT
- G.C. BOLTON, G.D. ALLEN, M. NASH & H.E. PROUD 353
#NCC-13 LASER-INDUCED FLUORESCENCE AS A DETECTION MODE IN COLUMN LIQUID
CHROMATOGRAPHY - H. LINGEMAN, R.J. VAN DE NESSE, U.A.TH. BRINKMAN, C.
GOOIJER & N.H. VELTHORST 355
#NCC-14 THE USE OF IMMOBILIZED ANTIBODIES FOR AUTOMATED ON-LINE SAMPLE
PRE-TREATMENT IN HPLC - A. FARJAM, H. LINGEMAN, P. TIMMERMAN, A.
SOLDAAT, A. BRUGMAN, N. VAN DE MERBEL, G.J. DE JONG, R.W. FREI &
U.A.TH. BRINKMAN 365
ANALYTE INDEX 375
GENERAL INDEX 380
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| spelling | Analysis for drugs and metabolites, including anti-infective agents [based on proceedings of the eighth International Bioanalytical Forum entitled "Analysis for drugs and metabolites, including anti-infective agents", held September 5 - 8, 1989 in Guildford, UK] ed. by Eric Reid ... London Royal Soc. of Chemistry 1990 XIV, 386 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Methodological surveys in biochemistry and analysis 20 Reid, Eric edt International Bioanalytical Forum 8 1989 Guildford Sonstige (DE-588)5222131-3 oth Methodological surveys in biochemistry and analysis 20 (DE-604)BV026512457 20 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022117655&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Analysis for drugs and metabolites, including anti-infective agents [based on proceedings of the eighth International Bioanalytical Forum entitled "Analysis for drugs and metabolites, including anti-infective agents", held September 5 - 8, 1989 in Guildford, UK] Methodological surveys in biochemistry and analysis |
| title | Analysis for drugs and metabolites, including anti-infective agents [based on proceedings of the eighth International Bioanalytical Forum entitled "Analysis for drugs and metabolites, including anti-infective agents", held September 5 - 8, 1989 in Guildford, UK] |
| title_auth | Analysis for drugs and metabolites, including anti-infective agents [based on proceedings of the eighth International Bioanalytical Forum entitled "Analysis for drugs and metabolites, including anti-infective agents", held September 5 - 8, 1989 in Guildford, UK] |
| title_exact_search | Analysis for drugs and metabolites, including anti-infective agents [based on proceedings of the eighth International Bioanalytical Forum entitled "Analysis for drugs and metabolites, including anti-infective agents", held September 5 - 8, 1989 in Guildford, UK] |
| title_full | Analysis for drugs and metabolites, including anti-infective agents [based on proceedings of the eighth International Bioanalytical Forum entitled "Analysis for drugs and metabolites, including anti-infective agents", held September 5 - 8, 1989 in Guildford, UK] ed. by Eric Reid ... |
| title_fullStr | Analysis for drugs and metabolites, including anti-infective agents [based on proceedings of the eighth International Bioanalytical Forum entitled "Analysis for drugs and metabolites, including anti-infective agents", held September 5 - 8, 1989 in Guildford, UK] ed. by Eric Reid ... |
| title_full_unstemmed | Analysis for drugs and metabolites, including anti-infective agents [based on proceedings of the eighth International Bioanalytical Forum entitled "Analysis for drugs and metabolites, including anti-infective agents", held September 5 - 8, 1989 in Guildford, UK] ed. by Eric Reid ... |
| title_short | Analysis for drugs and metabolites, including anti-infective agents |
| title_sort | analysis for drugs and metabolites including anti infective agents based on proceedings of the eighth international bioanalytical forum entitled analysis for drugs and metabolites including anti infective agents held september 5 8 1989 in guildford uk |
| title_sub | [based on proceedings of the eighth International Bioanalytical Forum entitled "Analysis for drugs and metabolites, including anti-infective agents", held September 5 - 8, 1989 in Guildford, UK] |
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