Structural analysis of point defects in solids: an introduction to multiple magnetic resonance spectroscopy
Gespeichert in:
| Hauptverfasser: | , , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin ; Heidelberg ; New York ; London ; Paris ; Tokyo ; Hong Kong ; Barcelona ; Budapest
Springer
1992
|
| Schriftenreihe: | Springer series in solid-state sciences
43 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XI, 367 S. graph. Darst. |
| ISBN: | 3540536159 0387536159 |
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TABLE OF CONTENTS
1. INTRODUCTION . 1
1.1 STRUCTURE OF POINT DEFECTS. 2
1.2 BASIC CONCEPTS OF DEFECT STRUCTURE DETERMINATION
BY ELECTRON PARAMAGNETIC RESONANCE. 4
1.3 SUPERHYPERFINE AND ELECTRONIC STRUCTURES
OF DEFECTS IN SOLIDS. 8
2. FUNDAMENTALS OF ELECTRON PARAMAGNETIC RESONANCE. 11
2.1 MAGNETIC PROPERTIES OF ELECTRONS AND NUCLEI. 11
2.2 ELECTRONS AND NUCLEI IN AN EXTERNAL MAGNETIC FIELD. 12
2.3 SOME USEFUL RELATIONS FOR
ANGULAR MOMENTUM OPERATORS . 14
2.4 TIME DEPENDENCE OF ANGULAR MOMENTUM
OPERATORS AND MACROSCOPIC MAGNETIZATION. 15
2.5 BASIC MAGNETIC RESONANCE EXPERIMENT. 17
2.6 SPIN-LATTICE RELAXATION. 20
2.7 RATE EQUATIONS FOR A TWO-LEVEL SYSTEM. 22
2.8 BLOCH EQUATIONS. 26
2.9 CONVENTIONAL DETECTION OF
ELECTRON PARAMAGNETIC RESONANCE AND ITS SENSITIVITY. 31
3. ELECTRON PARAMAGNETIC RESONANCE SPECTRA. 35
3.1 SPIN HAMILTONIAN. 35
3.2 ELECTRON ZEEMAN INTERACTION. 38
3.3 ^-FACTOR SPLITTING OF EPR SPECTRA . 42
3.4 FINE-STRUCTURE SPLITTING OF EPR SPECTRA. 45
3.5 HYPERFINE SPLITTING OF EPR SPECTRA. 53
3.6 SUPERHYPERFINE SPLITTING OF EPR SPECTRA. 62
3.7 INHOMOGENEOUS LINE WIDTHS OF EPR LINES . 72
4. OPTICAL DETECTION OF ELECTRON PARAMAGNETIC RESONANCE. 77
4.1 OPTICAL TRANSITIONS OF DEFECTS IN SOLIDS. 78
BIBLIOGRAFISCHE INFORMATIONEN
HTTP://D-NB.INFO/920899455
VIII
TABLE OF CONTENTS
4.2 SPECTRAL FORM OF OPTICAL TRANSITIONS OF
DEFECTS IN SOLIDS . 80
4.3 EPR DETECTED WITH
MAGNETIC CIRCULAR DICHROISM OF ABSORPTION METHOD. 86
4.4 MCDA EXCITATION SPECTRA OF ODEPR LINES
(MCDA "TAGGED" BY EPR). 96
4.5 SPATIALLY RESOLVED MCDA AND ODEPR SPECTRA.102
4.6 MEASUREMENT OF SPIN-LATTICE RELAXATION TIME T\ WITH MCDA
METHOD .105
4.7 DETERMINATION OF SPIN STATE WITH MCDA METHOD.106
4.8 EPR OF GROUND AND EXCITED STATES
DETECTED WITH OPTICAL PUMPING.112
4.9 EPR OPTICALLY DETECTED IN
DONOR-ACCEPTOR PAIR RECOMBINATION LUMINESCENCE.122
4.10 OPTICALLY DETECTED EPR OF TRIPLET STATES.129
4.11 ODEPR OF TRAPPED EXCITONS WITH
MCDA METHOD.133
4.12 SENSITIVITY OF ODEPR MEASUREMENTS.135
5. ELECTRON NUCLEAR DOUBLE RESONANCE .139
5.1 THE RESOLUTION PROBLEM, A SIMPLE MODEL.139
5.2 TYPE OF INFORMATION FROM EPR AND NMR SPECTRA.141
5.3 INDIRECT DETECTION OF NMR, DOUBLE RESONANCE.143
5.4 EXAMPLES OF ENDOR SPECTRA.150
5.5 RELATIONS BETWEEN EPR AND ENDOR SPECTRA,
ENDOR-INDUCED EPR.154
5.6 ELECTRON NUCLEAR NUCLEAR TRIPLE RESONANCE
(DOUBLE ENDOR).160
5.7 TEMPERATURE DEPENDENCE AND
PHOTO-EXCITATION OF ENDOR SPECTRA.163
5.7.1 TEMPERATURE DEPENDENCE OF ENDOR SPECTRA.163
5.7.2 PHOTO-EXCITATION OF ENDOR SPECTRA.166
6. DETERMINATION OF DEFECT SYMMETRIES FROM
ENDOR ANGULAR DEPENDENCES .169
6.1 DEFINITION OF NEIGHBOR SHELLS.170
6.2 NEIGHBOR SHELLS AND TRANSFORMATION OF
INTERACTION TENSORS.171
6.3 INTERACTION TENSOR SYMMETRIES AND
ENDOR ANGULAR DEPENDENCE.173
6.4 NEIGHBOR SHELL SYMMETRIES AND
ENDOR ANGULAR DEPENDENCES.175
6.4.1 SIMPLE EXAMPLE.175
6.4.2 GENERAL CASE.178
TABLE OF CONTENTS
IX
6.4.3 DEFECT STRUCTURE AND SYMMETRY MATRICES.182
6.5 LOW SYMMETRY DEFECTS IN
HIGHER SYMMETRY ENVIRONMENTS.194
6.6 WAYS TO DISTINGUISH BETWEEN
HIGH AND LOW SYMMETRY DEFECTS.200
6.7 ROLE OF EPR SPECTRUM FOR AN ENDOR ANALYSIS.204
6.8 SOLUTION OF THE SPIN HAMILTONIAN.207
6.8.1 CONCEPT OF EFFECTIVE SPIN.207
6.8.2 NUCLEAR SPIN HAMILTONIAN.208
6.8.3 CALCULATION OF EFFECTIVE SPIN.214
6.8.4 MUTUAL INTERACTIONS BETWEEN NEIGHBOR NUCLEI.215
6.8.5 LARGE HF OR SHF INTERACTION FOR ONE NUCLEUS.218
6.8.6 NUMERICAL CALCULATION OF EPR ANGULAR DEPENDENCES . 218
6.8.7 FITTING OF FREE PARAMETERS IN A SIMULATED
ENDOR ANGULAR DEPENDENCE.220
6.8.8 EXAMPLES OF RESULTS OBTAINED FROM ANALYSIS OF
ENDOR ANGULAR DEPENDENCES .222
6.9 SOFTWARE TREATMENT OF ENDOR SPECTRA.225
7. THEORETICAL INTERPRETATION OF SUPERHYPERFINE AND
QUADRUPOLE INTERACTIONS.231
7.1 STRUCTURES OF POINT DEFECTS.231
7.1.1 IMPURITIES IN INSULATORS.232
7.1.2 COLOR CENTERS.233
7.1.3 DEFECTS IN SEMICONDUCTORS.233
7.2 ORIGIN OF ZEEMAN, HYPERFINE AND
QUADRUPOLE INTERACTIONS.234
7.2.1 ORIGIN OF THE HAMILTONIAN.234
7.2.2 WIGNER-ECKART THEOREM.236
7.2.3 ZEEMAN INTERACTION.236
7.2.4 HYPERFINE INTERACTION.237
7.2.5 QUADRUPOLE INTERACTION.238
7.2.6 TOTAL HAMILTONIAN .239
7.3 CENTRAL ION HYPERFINE STRUCTURE.239
7.3.1 FREE ION ELECTRONIC STRUCTURE .240
7.3.2 CRYSTAL FIELD SPLITTING.243
7.3.3 SPIN HAMILTONIAN.244
7.4 COVALENCY AND SUPERHYPERFINE INTERACTION .247
7.4.1 MOLECULAR ORBITALS AND CONFIGURATION MIXING .248
7.4.2 SUPERHYPERFINE INTERACTION.249
7.4.3 LIGAND CORE POLARIZATION.253
7.4.4 LIGAND QUADRUPOLE INTERACTION .254
7.4.5 PSEUDOPOTENTIALS.256
7.4.6 LATTICE DYNAMICAL EFFECTS.258
X
TABLE OF CONTENTS
7.5 ORTHOGONALIZED ENVELOPE FUNCTIONS.258
7.5.1 WANNIER'S THEOREM AND EFFECTIVE-MASS THEORY . 259
7.5.2 CONTINUUM MODELS.260
7.5.3 POINT-ION MODEL AND ION-SIZE CORRECTIONS.261
7.5.4 GREEN'S FUNCTION METHOD FOR DEEP-LEVEL IMPURITIES . . 262
7.5.5 ORTHOGONALIZATION TO CORE ORBITALS.263
7.6 SIMPLE APPROXIMATIONS AND ILLUSTRATIONS FOR
INTERPRETATION OF SHF AND QUADRUPOLE INTERACTIONS.264
7.6.1 POINT DIPOLE-DIPOLE INTERACTION.265
7.6.2 CALCULATION OF ISOTROPIC SHF CONSTANTS WITH
ORTHOGONALIZED ENVELOPE FUNCTION .270
7.6.3 TRANSFERRED SHF INTERACTIONS.271
7.6.4 CALCULATION OF ANISOTROPIC SHF CONSTANT B WITH
ORTHOGONALIZED ENVELOPE FUNCTION .273
7.6.5 DYNAMICAL CONTRIBUTIONS TO SHF INTERACTIONS.275
7.6.6 QUADRUPOLE INTERACTIONS.277
8. TECHNOLOGY OF ENDOR SPECTROMETERS .281
8.1 EXPERIMENTAL CONSTRAINTS FOR CONVENTIONAL ENDOR.282
8.1.1 MODULATION FREQUENCY.282
8.1.2 SENSITIVITY.282
8.1.3 TEMPERATURE.282
8.1.4 MICROWAVE AND RADIO-FREQUENCY FIELD INTENSITIES . . . 283
8.1.5 MICROWAVE AND ENDOR FREQUENCY.284
8.1.6 STATIC MAGNETIC FIELD.285
8.1.7 MODULATION OF PARAMETERS.285
8.2 ENDOR SPECTROMETER DESIGN.286
8.3 COMPONENTS OF ENDOR SPECTROMETER.291
8.3.1 SIGNAL PRE-AMPLIFIER.291
8.3.2 MICROWAVE DETECTOR.292
8.3.3 MICROWAVE SOURCES.297
8.3.4 ENDOR MICROWAVE CAVITIES.301
8.3.5 RADIO-FREQUENCY GENERATORS.306
9. EXPERIMENTAL ASPECTS OF OPTICALLY DETECTED EPR AND ENDOR . . 309
9.1 SENSITIVITY CONSIDERATIONS.309
9.1.1 MAGNETIC CIRCULAR DICHROISM OF ABSORPTION.310
9.1.2 OPTICALLY DETECTED EPR.311
9.2 ODMR SPECTROMETERS MONITORING LIGHT EMISSION.312
9.3 ODMR SPECTROMETERS MONITORING
MAGNETIC CIRCULAR PROPERTIES OF ABSORPTION AND EMISSION . . . 314
9.3.1 GENERAL DESCRIPTION OF THE SPECTROMETER.314
9.3.2 MEASUREMENT OF
MAGNETIC CIRCULAR DICHROISM OF ABSORPTION.316
TABLE OF CONTENTS XI
9.3.3 MEASUREMENT OF
MAGNETIC CIRCULAR POLARIZATION OF EMISSION.319
9.4 EXPERIMENTAL DETAILS OF THE COMPONENTS
OF AN MCDA/MCPE ODMR SPECTROMETER.320
9.4.1 LIGHT SOURCES.321
9.4.2 MONOCHROMATORS.321
9.4.3 IMAGING SYSTEMS.322
9.4.4 LINEAR POLARIZERS.322
9.4.5 PHOTO-ELASTIC MODULATOR.322
9.4.6 DETECTORS.323
9.4.7 CRYOSTAT.323
9.4.8 MAGNET .324
9.4.9 MICROWAVE SYSTEM AND CAVITY.325
9.4.10 RADIO-FREQUENCY SYSTEM FOR ODENDOR.327
9.4.11 CONTROL AND REGISTRATION ELECTRONICS.328
APPENDICES.329
A. NUCLEAR (/-FACTORS, QUADRUPOLE CONSTANTS, NMR FREQUENCIES . . 329
B. THE CAYLEY TRANSFORMATION FORMULA.333
C. ALGORITHM FOR THE SUBTRACTION OF AN UNKNOWN BACKGROUND . . . 334
D. DIGITAL FILTERS FOR APPLICATION IN ENDOR SPECTRA.335
E. DECONVOLUTION OF ENDOR SPECTRA.336
F. PEAK SEARCH ALGORITHM.337
G. SIMULATION OF EPR SPECTRA.338
H. VALUES OF I/ NS(0) AND R-3 NP FOR SELECTED IONS.340
REFERENCES .341
SUBJECT INDEX .357 |
| any_adam_object | 1 |
| author | Spaeth, Johann-Martin Niklas, Jürgen R. Bertram, Ralph 1975- |
| author_GND | (DE-588)130652644 |
| author_facet | Spaeth, Johann-Martin Niklas, Jürgen R. Bertram, Ralph 1975- |
| author_role | aut aut aut |
| author_sort | Spaeth, Johann-Martin |
| author_variant | j m s jms j r n jr jrn r b rb |
| building | Verbundindex |
| bvnumber | BV025860209 |
| classification_rvk | UP 1100 UP 2100 UQ 2400 |
| ctrlnum | (OCoLC)260212922 (DE-599)BVBBV025860209 |
| discipline | Physik |
| format | Book |
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| id | DE-604.BV025860209 |
| illustrated | Illustrated |
| indexdate | 2024-10-09T16:24:48Z |
| institution | BVB |
| isbn | 3540536159 0387536159 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-019107934 |
| oclc_num | 260212922 |
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| owner | DE-11 |
| owner_facet | DE-11 |
| physical | XI, 367 S. graph. Darst. |
| publishDate | 1992 |
| publishDateSearch | 1992 |
| publishDateSort | 1992 |
| publisher | Springer |
| record_format | marc |
| series | Springer series in solid-state sciences |
| series2 | Springer series in solid-state sciences |
| spelling | Spaeth, Johann-Martin Verfasser aut Structural analysis of point defects in solids an introduction to multiple magnetic resonance spectroscopy Johann-Martin Spaeth ; Jürgen R. Niklas ; Ralph H. Bertram Berlin ; Heidelberg ; New York ; London ; Paris ; Tokyo ; Hong Kong ; Barcelona ; Budapest Springer 1992 XI, 367 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Springer series in solid-state sciences 43 Spinresonanz (DE-588)4173286-8 gnd rswk-swf ENDOR (DE-588)4152185-7 gnd rswk-swf Festkörper (DE-588)4016918-2 gnd rswk-swf Elektronenspinresonanz (DE-588)4132116-9 gnd rswk-swf Strukturanalyse (DE-588)4183787-3 gnd rswk-swf Störstelle (DE-588)4193400-3 gnd rswk-swf Festkörper (DE-588)4016918-2 s Störstelle (DE-588)4193400-3 s Elektronenspinresonanz (DE-588)4132116-9 s DE-604 ENDOR (DE-588)4152185-7 s Strukturanalyse (DE-588)4183787-3 s Spinresonanz (DE-588)4173286-8 s Niklas, Jürgen R. Verfasser aut Bertram, Ralph 1975- Verfasser (DE-588)130652644 aut Springer series in solid-state sciences 43 (DE-604)BV000016582 43 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=019107934&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Spaeth, Johann-Martin Niklas, Jürgen R. Bertram, Ralph 1975- Structural analysis of point defects in solids an introduction to multiple magnetic resonance spectroscopy Springer series in solid-state sciences Spinresonanz (DE-588)4173286-8 gnd ENDOR (DE-588)4152185-7 gnd Festkörper (DE-588)4016918-2 gnd Elektronenspinresonanz (DE-588)4132116-9 gnd Strukturanalyse (DE-588)4183787-3 gnd Störstelle (DE-588)4193400-3 gnd |
| subject_GND | (DE-588)4173286-8 (DE-588)4152185-7 (DE-588)4016918-2 (DE-588)4132116-9 (DE-588)4183787-3 (DE-588)4193400-3 |
| title | Structural analysis of point defects in solids an introduction to multiple magnetic resonance spectroscopy |
| title_auth | Structural analysis of point defects in solids an introduction to multiple magnetic resonance spectroscopy |
| title_exact_search | Structural analysis of point defects in solids an introduction to multiple magnetic resonance spectroscopy |
| title_full | Structural analysis of point defects in solids an introduction to multiple magnetic resonance spectroscopy Johann-Martin Spaeth ; Jürgen R. Niklas ; Ralph H. Bertram |
| title_fullStr | Structural analysis of point defects in solids an introduction to multiple magnetic resonance spectroscopy Johann-Martin Spaeth ; Jürgen R. Niklas ; Ralph H. Bertram |
| title_full_unstemmed | Structural analysis of point defects in solids an introduction to multiple magnetic resonance spectroscopy Johann-Martin Spaeth ; Jürgen R. Niklas ; Ralph H. Bertram |
| title_short | Structural analysis of point defects in solids |
| title_sort | structural analysis of point defects in solids an introduction to multiple magnetic resonance spectroscopy |
| title_sub | an introduction to multiple magnetic resonance spectroscopy |
| topic | Spinresonanz (DE-588)4173286-8 gnd ENDOR (DE-588)4152185-7 gnd Festkörper (DE-588)4016918-2 gnd Elektronenspinresonanz (DE-588)4132116-9 gnd Strukturanalyse (DE-588)4183787-3 gnd Störstelle (DE-588)4193400-3 gnd |
| topic_facet | Spinresonanz ENDOR Festkörper Elektronenspinresonanz Strukturanalyse Störstelle |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=019107934&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV000016582 |
| work_keys_str_mv | AT spaethjohannmartin structuralanalysisofpointdefectsinsolidsanintroductiontomultiplemagneticresonancespectroscopy AT niklasjurgenr structuralanalysisofpointdefectsinsolidsanintroductiontomultiplemagneticresonancespectroscopy AT bertramralph structuralanalysisofpointdefectsinsolidsanintroductiontomultiplemagneticresonancespectroscopy |