Crystalline cellulose and derivatives: characterization and structures
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin [u.a.]
Springer
2008
|
| Schriftenreihe: | Springer series in wood science
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Literaturangaben |
| Beschreibung: | X, 285 S. Ill., graph. Darst. |
| ISBN: | 9783540739333 3540739335 |
Internformat
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| 245 | 1 | 0 | |a Crystalline cellulose and derivatives |b characterization and structures |c Peter Zugenmaier |
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Datensatz im Suchindex
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| adam_text | Contents
1 Introduction................................................ 1
General Literature............................................ 5
2 History of Cellulose Research.................................. 7
2.1 The Concept of Cellulose.................................. 7
2.2 Concepts in Structural Research of Cellulose................... 8
2.3 Arrangements of the Cellulose Molecules in the Solid State....... 16
2.4 Chemical Constitution of Cellulose as a Macromolecule.......... 21
2.4.1 Linkage of Cellulose - the Chain Structure of Cellulose
(Freudenberg, Haworth)............................. 22
2.4.2 Macromolecule Formation - Size of the Chains
(Staudinger)...................................... 24
2.5 Historical Development of X-ray Models for Native Cellulose..... 27
References.................................................. 46
3 Background................................................ 53
3.1 Diffraction.............................................. 53
3.2 Model Building.......................................... 60
3.3 Spectroscopy............................................ 64
3.3.1 Optical Spectroscopy............................... 65
3.3.2 NMR Spectroscopy................................. 68
3.4 Convention for the Description of Cellulosic (Chiral) Structures ... 72
References.................................................. 74
4 Model Compounds........................................... 77
4.1 Conformation and Packing Analysis......................... 77
4.2 Monomers and Dimers.................................... 78
4.3 Trimers and Tetramers.................................... 83
4.3.1 Conformations.................................... 83
4.3.2 Packing Arrangements.............................. 87
4.4 Acetyl Derivatives........................................ 94
References.................................................. 98
x Contents
5 Cellulose................................................... 101
5.1 Cellulose Polymorphy..................................... 101
5.2 Characterization......................................... 103
5.2.1 X-ray Characterization.............................. 103
5.2.2 Spectroscopic Characterization....................... 105
5.3 Molecular and Crystal Structure............................. 112
5.3.1 Cellulose Iß....................................... 113
5.3.2 Cellulose la...................................... 122
5.3.3 Cellulose II....................................... 129
5.3.4 Cellulose HI...................................... 138
5.3.5 Cellulose IV...................................... 143
5.4 Cellulose Solvent Complexes............................... 151
5.4.1 Cellulose II-Hydrazine Complex...................... 151
5.4.2 Cellulose II Hydrate................................ 152
5.4.3 Cellulose I-Ammonia I Complex...................... 156
5.4.4 Cellulose I-Ethylenediamine Complex................. 160
5.5 Sodium Cellulose........................................ 164
5.5.1 Sodium Cellulose I................................. 165
5.5.2 Sodium Cellulose IV................................ 169
References.................................................. 171
6 Cellulose Derivatives......................................... 175
6.1 Characterization......................................... 175
6.1.1 Cellulose Triacetate................................ 175
6.1.2 Experimental Data for Cellulose Tripropionate and Cellulose
Acetate Dipropionate and Further Cellulose Esters........ 179
6.2 Conformation and Packing Arrangement of CTA I,
CTAII and CTA-N....................................... 185
6.3 Conformation and Packing Arrangement of CDAP.............. 197
6.4 Conformation and Packing Arrangement of Cellulose
Tribenzoate............................................. 199
6.5 Trimethyl Cellulose and 6-0-Acetyl-2,3-di-0-methyl Cellulose___200
References.................................................. 204
7 Morphology................................................ 207
7.1 Crystalline Domain Sizes.................................. 207
7.2 Microfibrils............................................. 207
7.3 Microfibrils and Fibrils.................................... 212
7.4 Parallel and Antiparallel Packing Arrangements of Microfibils..... 216
References.................................................. 220
Appendix...................................................... 223
Index......................................................... 281
|
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| dewey-sort | 3620.12 |
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| discipline | Chemie / Pharmazie Biologie |
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| institution | BVB |
| isbn | 9783540739333 3540739335 |
| language | English |
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| physical | X, 285 S. Ill., graph. Darst. |
| publishDate | 2008 |
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| spelling | Zugenmaier, Peter Verfasser aut Crystalline cellulose and derivatives characterization and structures Peter Zugenmaier Berlin [u.a.] Springer 2008 X, 285 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Springer series in wood science Literaturangaben Cellulosederivate (DE-588)4147460-0 gnd rswk-swf Kristallstruktur (DE-588)4136176-3 gnd rswk-swf Cellulose (DE-588)4147454-5 gnd rswk-swf Cellulose (DE-588)4147454-5 s Kristallstruktur (DE-588)4136176-3 s DE-604 Cellulosederivate (DE-588)4147460-0 s HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020133553&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Zugenmaier, Peter Crystalline cellulose and derivatives characterization and structures Cellulosederivate (DE-588)4147460-0 gnd Kristallstruktur (DE-588)4136176-3 gnd Cellulose (DE-588)4147454-5 gnd |
| subject_GND | (DE-588)4147460-0 (DE-588)4136176-3 (DE-588)4147454-5 |
| title | Crystalline cellulose and derivatives characterization and structures |
| title_auth | Crystalline cellulose and derivatives characterization and structures |
| title_exact_search | Crystalline cellulose and derivatives characterization and structures |
| title_full | Crystalline cellulose and derivatives characterization and structures Peter Zugenmaier |
| title_fullStr | Crystalline cellulose and derivatives characterization and structures Peter Zugenmaier |
| title_full_unstemmed | Crystalline cellulose and derivatives characterization and structures Peter Zugenmaier |
| title_short | Crystalline cellulose and derivatives |
| title_sort | crystalline cellulose and derivatives characterization and structures |
| title_sub | characterization and structures |
| topic | Cellulosederivate (DE-588)4147460-0 gnd Kristallstruktur (DE-588)4136176-3 gnd Cellulose (DE-588)4147454-5 gnd |
| topic_facet | Cellulosederivate Kristallstruktur Cellulose |
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