Three-dimensional free-radical polymerization: cross-linked and hyper-branched polymers
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin [u.a.]
Springer
2009
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XV, 270 S. graph. Darst. |
| ISBN: | 9783540875666 |
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| 245 | 1 | 0 | |a Three-dimensional free-radical polymerization |b cross-linked and hyper-branched polymers |c Korolev, Gennadij V. ; Mogilevič, Michail M. |
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Datensatz im Suchindex
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| adam_text | CONTENTS PART I THREE-DIMENSIONAL FREE-RADICAL POLYMERIZATION.
CROSS-LINKED POLYMERS 1 MICROHETEROGENEOUS MECHANISM OF
THREE-DIMENSIONAL FREE-RADICAL POLYMERIZATION . . . . . . . . . . . . .
. . . 3 1.1 MICROHETEROGENEOUS MODEL OF POLYMERIZATION PROCESS . . . . .
. . . . . . 4 1.2 POLYMERIZATION PROCESS: STAGES OF FORMATION OF THE
MICROHETEROGENEOUS STRUCTURE FOR CROSS-LINKED POLYMERS . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . 5 1.2.1 FORMATION OF POLYMER GRAINS AT THE INITIAL STAGE OF
POLYMERIZATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . 5 1.2.2 GROWTH OF POLYMER GRAINS DURING POLYMERIZATION . .
. . . . . . 7 1.2.3 ACCRETION OF POLYMER GRAINS AT THE FINAL STAGES OF
POLYMERIZATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . 12 1.3 STRUCTURAL AND PHYSICAL PROCESSES TAKING PLACE
DURING THREE-DIMENSIONAL FREE-RADICAL POLYMERIZATION . . . . . . . . . .
. . . . . . 17 1.3.1 MICROSYNERESIS OF LIQUID COMPONENTS IN REACTION
MEDIUM 17 1.3.2 MICROREDISTRIBUTION OF SUBSTANCES DISSOLVED IN LIQUID
COMPONENTS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. 20 1.3.3 LOCAL GLASS TRANSITION OF HIGHLY CROSS-LINKED MICRO-VOLUMES
OF POLYMER . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
1.4 MICROHETEROGENEOUS STRUCTURE OF CROSS-LINKED POLYMERS . . . . . . .
. . 25 1.4.1 INTERLAYERS BETWEEN POLYMER GRAINS . . . . . . . . . . . .
. . . . . . . . 27 1.4.2 POLYMER GRAINS . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . 30 REFERENCES . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . 31 2 KINETIC FEATURES OF THREE-DIMENSIONAL
FREE-RADICAL POLYMERIZATION . 33 2.1 KINETIC FEATURES OF INDIVIDUAL
STAGES OF POLYMERIZATION . . . . . . . . . . 34 2.1.1 INITIAL STAGE OF
POLYMERIZATION . . . . . . . . . . . . . . . . . . . . . . . . . 34
2.1.2 STAGES OF AUTO-ACCELERATION AND AUTO-DECELERATION . . . . . . . 41
2.2 INHIBITED POLYMERIZATION . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . 46 2.3 POLYMERIZATION IN SOLUTIONS . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51 2.4
POLYMERIZATION IN FILMS UNDER THE CONDITIONS OF OXYGEN DIFFUSION 54 IX X
CONTENTS 2.4.1 VINYL COMPOUNDS . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . 55 2.4.2 ALLYL COMPOUNDS . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . 66 2.5
THREE-DIMENSIONAL FREE-RADICAL POLYMERIZATION AS A TOOL FOR
MACROMOLECULAR DESIGN OF CROSS-LINKED POLYMERS . . . . . . . . . . . 75
REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . 78 3 LIVING CHAIN
THREE-DIMENSIONAL RADICAL POLYMERIZATION . . . . . . . . . . . 81 3.1
LIVING CHAINS IN FREE-RADICAL POLYMERIZATION . . . . . . . . . . . . . .
. . . . 82 3.2 IMPLEMENTATION OF LIVING CHAINS CONDITIONS IN THREE-
DIMENSIONAL FREE-RADICAL POLYMERIZATION . . . . . . . . . . . . . . . .
. . . . . . 86 3.2.1 COPOLYMERIZATION OF STYRENE WITH DIMETHACRYLATES IN
THE PRESENCE OF ALKOXYAMINES . . . . . . . . . . . . . . . . . . . . . .
. 87 3.2.2 POLYMERIZATION OF TRI(ETHYLENE GLYCOL) DIMETHACRYLATE
(TEGDMA) IN THE PRESENCE OF COMPLEX CUBR2 WITH
TETRAMETHYL-TIURAMDISULFIDE . . . . . . . . . . . . . . . . . . . . . .
93 3.2.3 POLYMERIZATION OF DIMETHACRYLATES OF POLY(ETHYLENE GLYCOL)S IN
THE PRESENCE OF COMPLEX CUBR WITH ORGANIC LIGANDS . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97 3.3
LIVING CHAIN THREE-DIMENSIONAL FREE-RADICAL POLYMERIZATION AS A TOOL FOR
MACROMOLECULAR DESIGN OF CROSS-LINKED POLYMERS . . . . . 99 REFERENCES .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . 109 4 KINETIC FEATURES OF
THREE-DIMENSIONAL FREE-RADICAL COPOLYMERIZATION . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 111
4.1 KINETIC FEATURES OF THREE-DIMENSIONAL COPOLYMERIZATION OF OLIGOMER
AND VINYL MONOMERS . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . 111 4.2 VARIATION OF COPOLYMER COMPOSITION DURING THREE-DIMENSIONAL
FREE-RADICAL COPOLYMERIZATION OF OLIGOMERS AND VINYL MONOMER . 118
REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . 127 5 CRITICAL CONVERSION
(GEL POINT) IN THREE-DIMENSIONAL FREE-RADICAL POLYMERIZATION . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 129 5.1
INAPPLICABILITY OF KNOWN CRITICAL CONVERSION CALCULATION METHODS TO
THREE-DIMENSIONAL FREE-RADICAL POLYMERIZATION . . . . . . 131 5.2 NOVEL
APPROACH TO CALCULATING CRITICAL CONVERSION IN THREE- DIMENSIONAL
FREE-RADICAL POLYMERIZATION . . . . . . . . . . . . . . . . . . . . . .
133 5.3 RESULTS OF CRITICAL CONVERSION CALCULATION FOR DIFFERENT CASES
OF THREE-DIMENSIONAL FREE-RADICAL POLYMERIZATION . . . . . . . . . . . .
. . . . 136 5.3.1 LIVING CHAINS THREE-DIMENSIONAL POLYMERIZATION AND
COPOLYMERIZATION (WITHOUT CHAIN TERMINATION) . . . . . . . 136 5.3.2
THREE-DIMENSIONAL POLYMERIZATION AND COPOLYMERIZATION WITH QUADRATIC OR
LINEAR CHAIN TERMINATION . . . . . . . . . . . . . . 143 5.3.3
THREE-DIMENSIONAL POLYMERIZATION WITH *PENDENT* DOUBLE BONDS TAKEN INTO
ACCOUNT (CHAIN TERMINATION BY DISPROPORTIONATION) . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . 145 CONTENTS XI 5.3.4 SUMMARY
OF RESULTS OF THEORETICAL CALCULATIONS FOR CRITICAL CONVERSION. . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . 150 5.4 COMPARISON
OF RESULTS OF THEORETICAL CALCULATIONS FOR CRITICAL CONVERSION WITH
EXPERIMENTAL DATA . . . . . . . . . . . . . . . . . . . . . . . . . . .
152 5.4.1 INHIBITED POLYMERIZATION OF DIMETHACRYLATES . . . . . . . . .
. . . . 152 5.4.2 COPOLYMERIZATION OF DIVINYL BENZENE ( M -DVB) WITH
STYRENE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . 154 REFERENCES . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 155 6
PROPERTIES OF CROSS-LINKED POLYMERS AND COPOLYMERS . . . . . . . . . . .
. . 157 6.1 CROSS-LINKED POLY(ACRYLATES). PHYSICAL AND MECHANICAL
PROPERTIES . 157 6.1.1 INFLUENCE OF CHEMICAL STRUCTURE OF OLIGOMERS UPON
PHYSICAL AND MECHANICAL PROPERTIES OF CROSS-LINKED POLY(ACRYLATES) . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
158 6.1.2 INFLUENCE OF PHYSICAL NETWORK DENSITY UPON PHYSICAL AND
MECHANICAL PROPERTIES OF CROSS-LINKED POLY(ACRYLATES) . . . . 166 6.2
CROSS-LINKED COPOLYMERS. PHYSICAL AND MECHANICAL PROPERTIES . . . . 172
6.2.1 MECHANISM OF COPOLYMERS TRANSITION INTO FORCED-ELASTIC STATE . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . 172 6.2.2
INFLUENCE OF CYCLIZATION ON PHYSICAL AND MECHANICAL PROPERTIES OF
COPOLYMERS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 181
6.3 CROSS-LINKED COPOLYMERS. THERMO-MECHANICAL PROPERTIES . . . . . . .
. 185 6.3.1 MECHANISM OF COPOLYMERS TRANSITION INTO HIGH-ELASTIC STATE .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . 185 6.3.2 COMPARISON OF TRANSITIONS INTO
HIGH-ELASTIC STATE WITH THOSE INTO FORCED-ELASTIC STATE . . . . . . . .
. . . . . . . . . . . . . 193 6.4 DIFFUSION-SORPTION PROPERTIES OF
COPOLYMERS . . . . . . . . . . . . . . . . . . . 195 REFERENCES . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . 199 PART II THREE-DIMENSIONAL FREE-RADICAL
POLYMERIZATION. HYPER-BRANCHED POLYMERS 7 SYNTHESIS OF HYPER-BRANCHED
POLYMERS . . . . . . . . . . . . . . . . . . . . . . . . . . . 203 7.1
CLASSIFICATION OF REACTIONS FOR HYPER-BRANCHED POLYMER SYNTHESIS . 203
7.2 SYNTHESIS OF HYPER-BRANCHED POLYMERS VIA THREE-DIMENSIONAL
FREE-RADICAL (CO)POLYMERIZATION WITH REGULATION OF POLYMER CHAIN LENGTH
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . 205 7.2.1 REGULATION OF CHAIN LENGTH THROUGH
INITIATION RATE VARIATION . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . 206 7.2.2 REGULATION OF CHAIN LENGTH BY
CHAIN TRANSFER AGENTS AND CHAIN TRANSFER CATALYSTS . . . . . . . . . . .
. . . . . . . . . . . . . . . 211 7.2.3 REGULATION OF CHAIN LENGTH
THROUGH THE USE OF INTRACHAIN REACTIONS OF CHAIN CARRIER RADICALS . . .
. . . . . . . . . . . . . . . . . 226 7.2.4 REGULATION OF CHAIN LENGTH
THROUGH THE USE OF MOLECULAR OXYGEN AS AN INHIBITOR . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . 230 XII CONTENTS 7.3
SYNTHESIS OF HYPER-BRANCHED POLYMERS VIA LIVING CHAINS FREE-RADICAL
THREE-DIMENSIONAL POLYMERIZATION . . . . . . . . . . . . . . . . 231
7.3.1 LIVING CHAINS FREE-RADICAL THREE-DIMENSIONAL POLYMERIZATION AS
REACTION FOR HYPER-BRANCHED POLYMERS SYNTHESIS . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . 231 7.3.2 LIVING CHAINS
POLYMERIZATION OF VINYL MONOMERS WITH DIETHYLDITHIOCARBAMATE GROUPS . .
. . . . . . . . . . . . . . . . . . 233 REFERENCES . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . 239 8 PROPERTIES AND APPLICATION OF HYPER-BRANCHED POLYMERS
. . . . . . . . . . . 243 8.1 *STRUCTURE*PROPERTY* RELATIONSHIP AND
PURPOSEFUL GENERATION OF HYPER-BRANCHED POLYMER PROPERTIES THAT ARE IN
DEMAND IN PRACTICE. . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . 244 8.2 HYPER-BRANCHED POLYMERS AS MODIFIERS OF POLYMERIC
MATERIALS . . . . 248 8.3 MAJOR FIELDS FOR HYPER-BRANCHED POLYMERS
APPLICATION . . . . . . . . . . 250 8.4 HBP: MAIN ACHIEVEMENTS AND
PROBLEMS TO BE SOLVED WITHOUT DELAY . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 253
REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . 254 9 METHODS FOR STUDYING
THREE-DIMENSIONAL FREE-RADICAL POLYMERIZATION AND CROSS-LINKED POLYMERS
. . . . . . . . . . . . . . . . . . . . . . . 257 9.1 CALORIMETRY . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . 257 9.2 IR SPECTROSCOPY . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . 258 9.3 OTHER
METHODS OF KINETIC MEASUREMENTS . . . . . . . . . . . . . . . . . . . .
. . . 259 9.4 LIGHT SCATTERING . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . 260 9.5 EPR . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . 260 9.5.1 STUDYING THE KINETICS OF FREE-RADICAL
ACCUMULATION IN NONSTATIONARY MODE . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . 260 9.5.2 STUDYING THE KINETICS OF DECAY OF
ACCUMULATED FREE RADICALS . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . 261 9.5.3 METHOD OF
SYNCHRONOUS COMPARISON OF CONTINUOUSLY RECORDED KINETIC CURVES [ R * ] =
F1 ( T ) AND W = F2 ( T ) . . . . . . . 262 9.5.4 STRUCTURAL AND
PHYSICAL STUDIES USING EPR . . . . . . . . . . . . . . . 262 9.6 NMR . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . 263 9.7 PHYSICOMECHANICAL AND
THERMO-MECHANICAL METHODS . . . . . . . . . . . 263 9.8 VOLUMETRIC
METHOD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . 264 9.9 COMPLEX METHODS . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . 264 REFERENCES . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . 265 INDEX . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . 267
|
| any_adam_object | 1 |
| author | Korolev, Gennadij V. Mogilevič, Michail M. |
| author_facet | Korolev, Gennadij V. Mogilevič, Michail M. |
| author_role | aut aut |
| author_sort | Korolev, Gennadij V. |
| author_variant | g v k gv gvk m m m mm mmm |
| building | Verbundindex |
| bvnumber | BV025521690 |
| classification_rvk | UV 2100 VE 8000 VK 8000 |
| ctrlnum | (OCoLC)304402472 (DE-599)BVBBV025521690 |
| dewey-full | 547.28 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 547 - Organic chemistry |
| dewey-raw | 547.28 |
| dewey-search | 547.28 |
| dewey-sort | 3547.28 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik |
| format | Book |
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| id | DE-604.BV025521690 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T22:35:53Z |
| institution | BVB |
| isbn | 9783540875666 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-020129964 |
| oclc_num | 304402472 |
| open_access_boolean | |
| owner | DE-11 |
| owner_facet | DE-11 |
| physical | XV, 270 S. graph. Darst. |
| publishDate | 2009 |
| publishDateSearch | 2009 |
| publishDateSort | 2009 |
| publisher | Springer |
| record_format | marc |
| spelling | Korolev, Gennadij V. Verfasser aut Three-dimensional free-radical polymerization cross-linked and hyper-branched polymers Korolev, Gennadij V. ; Mogilevič, Michail M. Berlin [u.a.] Springer 2009 XV, 270 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Verzweigte Verbindungen (DE-588)4320667-0 gnd rswk-swf Radikalische Polymerisation (DE-588)4325747-1 gnd rswk-swf Polymeres Netzwerk (DE-588)4307122-3 gnd rswk-swf Polymere (DE-588)4046699-1 gnd rswk-swf Polymeres Netzwerk (DE-588)4307122-3 s Radikalische Polymerisation (DE-588)4325747-1 s DE-604 Polymere (DE-588)4046699-1 s Verzweigte Verbindungen (DE-588)4320667-0 s Mogilevič, Michail M. Verfasser aut SWB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020129964&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Korolev, Gennadij V. Mogilevič, Michail M. Three-dimensional free-radical polymerization cross-linked and hyper-branched polymers Verzweigte Verbindungen (DE-588)4320667-0 gnd Radikalische Polymerisation (DE-588)4325747-1 gnd Polymeres Netzwerk (DE-588)4307122-3 gnd Polymere (DE-588)4046699-1 gnd |
| subject_GND | (DE-588)4320667-0 (DE-588)4325747-1 (DE-588)4307122-3 (DE-588)4046699-1 |
| title | Three-dimensional free-radical polymerization cross-linked and hyper-branched polymers |
| title_auth | Three-dimensional free-radical polymerization cross-linked and hyper-branched polymers |
| title_exact_search | Three-dimensional free-radical polymerization cross-linked and hyper-branched polymers |
| title_full | Three-dimensional free-radical polymerization cross-linked and hyper-branched polymers Korolev, Gennadij V. ; Mogilevič, Michail M. |
| title_fullStr | Three-dimensional free-radical polymerization cross-linked and hyper-branched polymers Korolev, Gennadij V. ; Mogilevič, Michail M. |
| title_full_unstemmed | Three-dimensional free-radical polymerization cross-linked and hyper-branched polymers Korolev, Gennadij V. ; Mogilevič, Michail M. |
| title_short | Three-dimensional free-radical polymerization |
| title_sort | three dimensional free radical polymerization cross linked and hyper branched polymers |
| title_sub | cross-linked and hyper-branched polymers |
| topic | Verzweigte Verbindungen (DE-588)4320667-0 gnd Radikalische Polymerisation (DE-588)4325747-1 gnd Polymeres Netzwerk (DE-588)4307122-3 gnd Polymere (DE-588)4046699-1 gnd |
| topic_facet | Verzweigte Verbindungen Radikalische Polymerisation Polymeres Netzwerk Polymere |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020129964&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT korolevgennadijv threedimensionalfreeradicalpolymerizationcrosslinkedandhyperbranchedpolymers AT mogilevicmichailm threedimensionalfreeradicalpolymerizationcrosslinkedandhyperbranchedpolymers |