Inorganic chemistry in focus III:
Gespeichert in:
| Weitere Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH
2006
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XLVI, 329 S. Ill., graph. Darst. |
| ISBN: | 9783527315109 3527315101 |
Internformat
MARC
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| 245 | 1 | 0 | |a Inorganic chemistry in focus III |c ed. by Gerd Meyer ... |
| 264 | 1 | |a Weinheim |b Wiley-VCH |c 2006 | |
| 300 | |a XLVI, 329 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
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| 999 | |a oai:aleph.bib-bvb.de:BVB01-020019889 | ||
Datensatz im Suchindex
| _version_ | 1804142547701858304 |
|---|---|
| adam_text | XI
Contents
Dedicated V
In Praise of Synthesis
VII
Preface XIX
List of Contributors
XXI
Biographical Sketches
XXV
Ί
Inter-electron Repulsion and Irregularities in the Chemistry
of Transition Series
1
David A. Johnson
1.1
Introduction: Irregularities in
Lanťhanide
Chemistry
1
1.2
A General Principle of
Lanťhanide
Chemistry
4
1.3
Extensions of the First Part of the Principle
6
1.4
Extensions of the Second Part of the Principle
8
1.5
The Tetrad Effect
9
1.6
The Diad Effect
11
References
13
2
Stereochemical Activity of Lone Pairs in Heavier Main-group Element
Compounds
25
Anja-Verena
Mudrmg
2.1
Introduction
15
2.2
When Does a Lone Pair of Electrons Become Stereochemically
Active?
-
Observations
16
2.3
Theoretical Concepts
17
2.3.1
Molecular/Complex Compounds
18
2.3.2
Solid Materials
20
2.4
Conclusions
25
Acknowledgments
26
References
26
ХИ
I Contents
3
How Close to Close Packing?
29
Hideo
Imoto
3.1
Introduction
29
3.2
Essential Features of Close Packing
30
3.3
Parameter Definitions
30
3.4
Correlation Between
D
and
N 33
3.5
Transformation of Close-packing Arrangements
35
3.6
Close-pacMng of Cations or of Anions?
38
3.7
What Determines the Structure?
41
Appendix. ICSD Codes,
D
and
N
Parameters of the Structures
Used
42
References
44
4
Forty-five Years of Praseodymium Di-iodide, Prl2
45
Gerd
Meyer and Andriy Palasyuk
Foreword
45
4.1
Introduction
46
4.2
Phases and Structures in the System Praseodymium-Iodine
47
4.2.1
Synthesis Generalities
47
4.2.2
Structural Principles
48
4.3
Prl2: Phases and Phase Analysis
51
4.4
Conclusions
58
Acknowledgments
59
References
59
5
Centered Zirconium Clusters: Mixed-halide Systems
61
Martin
Köckerling
Foreword
61
5.1
The Basics of Zirconium Cluster Chemistry
61
5.2
Motivation
62
5.3
Mixed-Chloride-Iodide Zirconium Cluster Phases
with a
6:
12-Metal
:
Halide Ratio
63
5.4
Mixed Chloride-Iodide Zirconium Cluster Phases
with a
6:13
Metal
:
Halide Ratio
64
5.5
Mixed Chloride-Iodide Zirconium Cluster Phases
with a
6:14
Metal
:
Halide Ratio
67
5.6
Mixed Chloride-Iodide Zirconium Cluster Phases
with a
6:15
Metal
:
Halide Ratio
71
5.7
Mixed Chloride-Iodide Zirconium Cluster Phases
with a
6:18
Metal:Halide Ratio
-
Products from Solid-state Reactions
76
5.8
Outlook
77
Acknowledgments
77
References
77
Contents
XIII
6
Titanium Niobium Oxychlorides: Ligand Combination Strategy
for the Preparation of Low-dimensional Metal Cluster Materials
79
Ekater ma V. Anokhina and Abdessadek Lachgar
Abstract
79
6.1
Introduction
79
6.1.1
Cluster Connectivity and Framework Dimension
Sí
6.1.2
The Ligand Combination Approach to Creating
Anisotropie
Frameworks
82
6.2
Overview of the Chemistry of Niobium Chloride
and Niobium Oxide Cluster Compounds
83
6.2.1
Synthesis and Chemical Properties
83
6.2.2
Electronic Structure,
Redox
and Magnetic Properties
84
6.3
Niobium Oxychloride Cluster Compounds
85
6.3.1
One-dimensional Cluster Frameworks
85
6.3.1.1
Frameworks Built from Clusters with Five Oxygen ligands
85
6.3.1.2
Frameworks Built of Clusters with Six Oxygen Ligands
86
6.3.2
Two-dimensional Cluster Frameworks
88
6.3.2.1
2D Oxychloride Frameworks with a Honeycomb-like Structure
88
6.3.2.2
Pillared 2D Oxychloride Frameworks
90
6.3.2.3
2D Framework with Graphite-like Cluster Connectivity
90
6.4
Summary of Crystallographic Data on Titanium Niobium
Oxychlorides
93
6.4.1
Effect of the Total Number of Ligands
93
6.4.2
Cluster Configuration
95
6.4.2.1
Relationships Between Ligand Arrangement and Direct Inter-cluster
Linkages
95
6.4.2.2
Relationships Between the Ligand Arrangement and Inter-cluster
Linkages via Counter-ions
96
6.4.3
Anion
Segregation
97
6.4.4
Structure-determining Factors in the Absence of Hard Cations
97
6.5
Electronic Configuration of Niobium Oxychloride Clusters
99
6.6
Conclusion and Outlook
100
References
101
7
Trinuclear Molybdenum and Tungsten Cluster Chalcogenides:
From Solid State to Molecular Materials
105
Rosa Uusar and
Cristian Vicent
7.1
Introduction
105
7.2
Synthesis and Structure of Molecular M3Q4 and M3Q7 Cluster
Complexes
107
7.2.1
Solid-state Synthesis: Dimensional Reduction
108
7.2.2
Solution Routes: Excision
109
7.2.3
Ligand Exchange Reactions
112
7.2.3.1
M3Q4 Cluster Complexes
112
7.2.3.2
M3Q7 Ouster Complexes
313
XIV
I Contents
7.3
Trinudear Clusters as Building Units
115
7.3.1
Molecular Conductors Based on M3Q7 Cluster Complexes
115
7.3.2
Formation of Supramolecular Adducts
117
Acknowledgments
119
References
ÎÎ9
8
Current State on (B,C,N) Compounds of Calcium
and Lanthanum
121
H.
-Jürgen
Meyer
8.1
Introduction
121
8.2
Problems and Pitfalls of some Calcium Compounds with (mixed)
B,C,N Anions
121
8.2.1
Borides of Calcium and Lanthanum
123
8.2.2
The CaC2 Problem and
СазСЬСз
124
8.2.3
Calcium Nitride and Calcium Carbodiimides
126
8.2.4
Calcium Nitridoborates
126
8.2.5
A Comparison of Caj(BN2)2 and Sr3(BN2)2 Structures
126
8.3
Metal-nitridoborates
129
8.3.1
Electronic Considerations
129
8.4
Lanthanum Nitridoborates
131
Compounds in Ca-B-N and La-B-N systems
132
8.4.1
Nitridoborate Ions
133
8.4.2
Structures of Lanthanum Nitridoborates
134
8.5
Outlook
137
Acknowledgments
138
References
138
9
Compositional, Structural and Bonding Variations in Ternary Phases
of Lithium with Main-group and Late-transition Elements
141
Claude H.
Beim,
Monique Tillará
9.1
Introduction
141
9.2
Tuning Structures and Properties in Lithium Binary and Ternary
Systems
142
9.3
Clustering in Condensed lithium Ternary Phases: A Way Towards
Quasicrystals
143
9.4
Exploration of New Lithium Ternary Systems Containing Ag, Zn,
Al,
Si, Ge
144
9.4.1
Background
144
9.4.2
The System Ii-Al-Ag
145
9.4.3
Compositional and Structural Variations in the System li-Al-Si
146
9.4.4
The Tetragonal Compound
IÌ9AISÌ3,
a Good Anodic Material
148
9.5
The Intermetallic Ii-Zn-Ge System, from Electron-poor
to Electron-rich Phases
149
9.5.1
The Electron-poor Hexagonal Phase LiZnGe
249
9.5.2
The True Cubic Configuration of the Compound
Ii2ZnGe
150
Contents
XV
9.5.3
The Li-rich Compound
Li8Zn2Ge3
with an Open-layered
Anionie
Framework
152
9.6
Concluding Remarks
154
References
154
10
Polar Intermetallics and Zintl Phases along the Zintl Border
157
Arnold M. Cu/oy
10.1
First comes the synthesis
... -
J.D. Corbett
157
10.2
What are Intermetallics?
157
10.3
The Zintl-Klemm Concept
160
10.4
Electron-poor Polar Intermetallics
161
10.5
Intermetallic
π
-Systems
162
10.6
Some Final Remarks
268
References
169
Π
Rare-earth Zintl Phases:
Novel Magnetic and Electronic Properties
173
Susan M. Kauzlarich and JiongJiang
11.1
Introduction
173
11.2
Structure
174
11.3
Resistivity
177
11.4
Magnetic Properties
178
11.5 Magnetoresistance 179
11.6
Summary
180
Acknowledgments
181
References
181
12
Understanding Structure-forming Factors
and Theory-guided Exploration of Structure-Property Relationships
in Intermetallics
183
Dong
-Щип
Seo,
Li-Ming Wu and Sang-Hwan Kim
12.1
Introduction
183
12.2
Mn14Alsfrt.xGe3.x
(x-O.OO,
0.32, 0.61) 184
12.3
Las.xCaxGe4
(ж=3.37,
3.66, 3.82)
and Ce5.xCaxGe4
(jc=3.00,
3.20, 3.26) 188
12
A Concluding Remarks
191
Acknowledgments
393
References
192
13
Ternary and Quaternary Niobium Arsenide Zintl Phases
195
Franck
Cascoin and
Slavi
С.
Sevov
13.1
Introduction
195
13.2
New Main-group Arsenides
397
13.3
Compounds Based on Isolated [NbAs4] Tetrahedral Centers
399
XVI
I Contents
13.4
Compounds Based on Edge-sharing Dimers
of
[NbAs4] Tetrahedra
204
References
206
14
The Building-block Approach to Understanding Main-group-metal
Complex Structures
-
More than just Attempting to Hew Blocks
with a Razor
209
Peter K. Dorhout
14.1
Introduction
209
14.2
The Building-block Approach
210
14.2.1
Quaternary Rare-earth Metal Chalcophosphates
210
14.2.2
Quaternary Rare-earth Metal Chalcoarsenites and Antimonites
213
14.2.3
Quaternary Rare-earth Metal Chalcotrielates and Tetrelates
215
14.3
Summary
221
References
222
15
Cation-deficient Quaternary Thiospinels
225
Ashok K. Canguli, Shalabh Gupta and Cunjan Carg
15.1
Introduction
225
15.2
Cu5.5SiD1.5Fe4Sn12S32
227
15.3
Cu5.47Fe2.9Sn13
ЛЅ32
233
15.4
Cu7.38Mn4Sn12S32
(1)
and
Cu7.o7NÍ4Sn12S32
(2) 235
15.5
Conclusions
236
References
236
16
A New Class of Hybrid Materials via Salt-inclusion Synthesis
239
Shiou-Jyh Hwu
16.1
Introduction
239
16.2
General Approach to Salt-inclusion Synthesis
241
16.3
Examples and Discussion
242
16.3.1
Zeolite-like Transition Metal Containing Porous Compounds
242
16.3.2
Non-centrosyrnmetric Solids {NCSs)
244
16.3.3
Solids Containing Periodic Arrays of Transition-metal
Nanostructures
247
16.4
Final Remarks
248
Acknowledgments
249
References
249
17
Layered Perrhenate and Vanadate Hybrid Solids:
On the Utility of Structural Relationships
251
Paul A. Maggard and Bangbo Yan
17.1
Introduction
251
17.2
Heterometallic Perrhenates
252
17.2.1
Background: Molecular and Condensed Metal-perrhenates
252
17.2.2
Copper- and Silver-perrhenate Hybrids
253
Contents
XVII
17.2.3
Metal-coordinated Pillars in Perrhenate Hybrids
256
17.3
Heterometallic Vanadates
259
17.3.1
Background: Layered Vanadate Species
259
17.3.2
Layered Heterometallic Vanadates: Charge Density Matching
261
17.3.3
Heterometallic Reduced Layered Vanadates
262
17.4
Conclusions
265
Acknowledgments
265
References
265
18
Hydrogen Bonding in Metal Halides:
Lattice Effects and Electronic Distortions
267
James
D. Martin
18.1
Introduction
267
18.2
A Hierarchy of Structure-directing Forces
268
18.3
Hydrogen Bond Influence on Melts and Crystallization
269
18.4
Electronic Implications of Hydrogen Bonding
272
18.5
Conclusions
275
Acknowledgments
276
References
276
19
Syntheses and Catalytic Properties
of Titanium Nitride Nanoparticles
279
Stefan Kaskel
19.1
Introduction
279
19.2
Synthesis of TiN Nanoparticles
280
19.3
Titanium Nitride Nanoparticles in Hydrogen Storage
Applications
285
19.4
Catalytic Properties of TiN Nanoparticles in Solution
288
19.5
Catalytic Properties
289
References
292
20
Solventless Thermolysis: A Possible Bridge Between Crystal Structure
and Nanosynthesis?
295
Ling Chen and Li-M mg Wu
20.1
Introduction
295
20.2
Synthesis Methods
295
20.3
Solventless Thermolysis and Some Examples
296
20.3.1
Cu2S Nanodisks
297
20.3.2
NiS Nanorods and Nanotrigonal Prisms
297
20.3.3
Bi2S3 Nanowires, Rods and Fabric
298
20.3.4
PbjOzCb Nanobelts
298
20.4
Control of the Nanoproduct Morphology Through the State
of the Precursor
299
XVIII
Contents
20.5
Crystal
Structure
of the Precursor versus the Morphology
and Distribution of the As-synthesized Nanoproduct:
A Possible Bridge Between these Two?
300
20.6
Conclusion and Prospects
302
Acknowledgment
302
References
303
21
New Potential Scintillation Materials in Borophosphate Systems
305
Jing-Tai Zhao and Cheng-Jun Duan
21.1
Introduction
305
21.2
Recent Studies on the Scintillation Luminescence Properties
of Borophosphates
306
21.2.1
The Crystal Structures of Ba3BP3Oi2, BaBPO5 and Ba3BPO7
306
21.2.2
The Preparation and X-ray-excited Intrinsic Scintillation
Luminescence Properties of
Ва3ВРзО12, ВаВРО5
and
Ва3ВРО7
308
21.2.3
The X-ray-excited Luminescence Properties of Ce3+-activated
Ba3BP3O12, BaBPOs and Ba3BPO7
316
21.2.4
Potential Scintillation Material of Ba3BP3Oi2:
Eu2 1
318
21.3
Outlook
322
References
323
Subiect
Index
325
|
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| indexdate | 2024-07-09T22:33:30Z |
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| language | English |
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| spelling | Inorganic chemistry in focus III ed. by Gerd Meyer ... Weinheim Wiley-VCH 2006 XLVI, 329 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Anorganische Chemie (DE-588)4002145-2 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Anorganische Chemie (DE-588)4002145-2 s DE-604 Meyer, Gerd 1949- (DE-588)131930915 edt Digitalisierung UB Regensburg application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020019889&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Inorganic chemistry in focus III Anorganische Chemie (DE-588)4002145-2 gnd |
| subject_GND | (DE-588)4002145-2 (DE-588)4143413-4 |
| title | Inorganic chemistry in focus III |
| title_auth | Inorganic chemistry in focus III |
| title_exact_search | Inorganic chemistry in focus III |
| title_full | Inorganic chemistry in focus III ed. by Gerd Meyer ... |
| title_fullStr | Inorganic chemistry in focus III ed. by Gerd Meyer ... |
| title_full_unstemmed | Inorganic chemistry in focus III ed. by Gerd Meyer ... |
| title_short | Inorganic chemistry in focus III |
| title_sort | inorganic chemistry in focus iii |
| topic | Anorganische Chemie (DE-588)4002145-2 gnd |
| topic_facet | Anorganische Chemie Aufsatzsammlung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020019889&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT meyergerd inorganicchemistryinfocusiii |