Capillary gas chromatography - mass spectrometry in medicine and pharmacology:
Gespeichert in:
| Weitere Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Heidelberg ; Basel ; New York
Huethig
1987
|
| Schriftenreihe: | Chromatographic methods
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Literaturangaben |
| Beschreibung: | XIII, 309 S. graph. Darst. |
| ISBN: | 3778513753 |
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| adam_text | VII
CONTENTS
PREFACE V
1 RECENT ADVANCES IN GAS CHROMATO
GRAPHY
W. G. JENNINGS AND G. TAKEOKA 1
1.1 INTRODUCTION 1
1.2 SAMPLE INJECTION CONSIDERATIONS 2
1.3 COLUMN CONSIDERATIONS 6
1.4 STEREOSPECIFIC SEPARATIONS 9
1.5 IMPROVING SEPARATION 9
1.6 THE MEGABORE COLUMN 13
1.7 CONCLUSION 14
1.8 NOMENCLATURE AND SYMBOLS 14
2 DERIVATIZATION OF LODOTHYRONINES AT THE
PICOGRAM LEVEL FOR DETERMINATION BY
GC-ECD
A. SENTISSI, E. J. ROGERS, R. JOPPICH
KUHN, M. JOPPICH AND R. W. GIESE ... 19
2.1 INTRODUCTION 20
2.2 MATERIALS AND METHODS 21
2.2.1 CHEMICAL AND REAGENTS 21
2.2.2 PROCEDURES 22
2.2.2.1 HIGH PERFORMANCE LIQUID CHROMATOGRA
PHY 23
2.2.2.2 FLASH CHROMATOGRAPHY 24
2.2.2.3 THIN LAYER CHROMATOGRAPHY 24
2.2.2.4 GAS CHROMATOGRAPHY 24
2.2.2.5 SOLID PHASE EXTRACTION 25
2.2.2.6 SYNTHESIS 26
2.2.2.7 ANALYTICAL DERIVATIZATION 28
2.3 RESULTS AND DISCUSSION 29
HTTP://D-NB.INFO/870081667
VIII
CONTENTS
3 APPLICATION OF ENANTIOSELECTIVE CAPILLA
RY GAS CHROMATOGRAPHY TO STEREOCHE
MICAL ANALYSIS OF NATURAL COMPOUNDS
AND PHARMACEUTICALS
W. A. KOENIG 37
3.1 INTRODUCTION 37
3.2 MATERIALS AND METHODS 38
3.3 RESULTS AND DISCUSSION 39
3.3.1 CHIRAL POLYSILOXANES AND DERIVATIZATION
TECHNIQUES 39
3.3.2 STEREOCHEMICAL INVESTIGATIONS OF NATU
RAL COMPOUNDS 41
3.3.3 STEREOCHEMICAL INVESTIGATIONS OF CHIRAL
PHARMACEUTICALS 46
3.4 CONCLUDING REMARKS 50
4 ORGANIC ACIDS IN URINE AND SERUM OF PA
TIENTS WITH DIABETIC KETOACIDOSIS
H. M. LIEBICH 53
4.1 INTRODUCTION 53
4.2 METHODS 54
4.2.1 ANALYSIS OF THE ORGANIC ACIDS 54
4.2.2 ANALYSIS OF THE METHYL KETONES 54
4.3 RESULTS AND DISCUSSION 55
4.3.1 FATTY ACIDS 55
4.3.2 DICARBOXYLIC ACIDS 56
4.3.3 OXOCARBOXYLIC ACIDS 57
4.3.4 HYDROXYCARBOXYLIC ACIDS 61
4.4 CONCLUSIONS 65
5 SOME REMARKS ON SAMPLE PREPARATION
W. DQNGES 69
5.1 INTRODUCTION 69
5.2 EXTRACTION 70
5.3 ENRICHMENT AND DRYING OF ORGANIC EX
TRACTS 76
5.4 DERIVATIZATION 80
5.5 HANDLING AND PRACTICABILITY 81
5.6 AUTOMATION AND ROBOTICS 83
5.7 THE FUTURE OF BIOMEDICAL GC 84
6 APPLICATIONS OF CAPILLARY GLC AS A ROU
TINE ANALYTICAL TECHNIQUE IN BIOAVAIL
ABILITY INVESTIGATIONS
D. LUTZ AND H. JAEGER 91
6.1 INTRODUCTION 91
6.2 LORAZEPAM 92
6.3 HYDROCHLOROTHIAZIDE 95
6.4 ISOSORBIDE DINITRATE 96
CONTENTS
IX
6.5 NIFEDIPINE 98
6.6 VALPROIC ACID 102
7 GLASS CAPILLARY GLC-MS: APPLICATIONS
IN THE ANALYSIS OF DRUGS AND METABO
LITES IN BIOLOGICAL FLUIDS
N. P. E. VERMEULEN, N. ONKENHOUT, M.
VAN DER GRAAFF, B. J. XU, AND A. G. L.
BURM 107
7.1 INTRODUCTION 107
7.2 FREE RELEASE STATIC COATING OF CAPILLARY
COLUMNS 108
7.3 IONIZATION TECHNIQUES FOR MASS SPEC
TROMETRY 109
7.3.1 ELECTRON-IMPACT IONIZATION (EL) 109
7.3.2 POSITIVE CHEMICAL IONIZATION (PCI) .... 110
7.3.3 NEGATIVE CHEMICAL IONIZATION 111
7.3.4 OTHER IONIZATION TECHNIQUES 113
7.4 APPLICATION OF GAS CHROMATOGRAPHY
MASS SPECTROMETRY 113
7.4.1 GC-MS APPARATUS 113
7.4.2 DISCRIMINATION BETWEEN REGIOISOMERIC
MERCAPTURIC ACIDS (MA S) WITH EI-MS .. 114
7.4.3 IDENTIFICATION OF FENTANYL AND METABO
LITES BY GC-MS 115
7.4.4 MASS FRAGMENTOGRAPHIC ANALYSIS OF
PSEUDORACEMIC HEXOBARBITAL AND ITS
MAJOR METABOLITES IN BLOOD AND URINE. 116
7.4.5 ESTIMATION OF DEUTERIUM CONTENTS IN
MERCAPTURIC ACIDS WITH EL- AND PCI-MS 121
7.4.6 MASS FRAGMENTOGRAPHIC DETERMINATION
OF DEUTERIUM-LABELED AND UNLABELED LI
DOCAINE AND BUPIVACAINE WITH EL- AND
PCI-GS-MS 123
7.4.7 NCI-MS OF MERCAPTURIC ACIDS (MA S) .. 130
7.4.8 NCL-GC-MS ANALYSIS OF MA S IN URINE . 132
7.5 SUMMARY AND CONCLUSION 134
8 QUANTIFICATION OF BIOLOGICALLY ACTIVE
COMPOUNDS USING STABLE ISOTOPES AND
CAPILLARY COLUMN GLC SELECTED ION MO
NITORING
W. J. A. VANDENHEUVEL, R. IN. WALKER,
AND J. R. CARLIN 139
9 MEASUREMENT OF ERGOTAMINE IN HUMAN
PLASMA BY TRIPLE STAGE QUADRUPOLE MS
WITH NICI
N. HARING, J. A. SETTLAGE, AND R. SCHU
BERT 165
X
CONTENTS
9.1 INTRODUCTION 165
9.2 EXPERIMENTAL 167
9.2.1 EXTRACTION 167
9.2.2 MEASUREMENT 167
9.2.3 ANALYTICAL PARAMETERS 170
9.3 RESULTS 171
10 HIGHLY SELECTIVE DETECTION OF TRACE
COMPOUNDS DURING CAPILLARY GAS CHRO
MATOGRAPHY-MASS SPECTROMETRY
H. M. LEITH AND S. J. GASKELL 175
10.1 INTRODUCTION 175
10.2 TECHNIQUE FOR HIGH-SENSITIVITY ANALYSIS 175
10.3 TRACE ANALYSIS OF STEROIDS IN BREAST TU
MOR TISSUE 179
11 CHROMATOGRAPHIC (GC OR LC) AND NON
CHROMATOGRAPHIC (FAB) MASS SPECTRO
METRIC TECHNIQUES FOR CLINICAL STEROID
ANALYSIS
C. SHACKLETON, S. GASKELL AND D. J.
LIBERATO 185
11.1 INTRODUCTION 186
11.2 EXPERIMENTAL 187
11.2.1 THE GAS CHROMATOGRAPHY OF STEROID
CONJUGATES 187
11.2.2 FAST ATOM BOMBARDMENT 188
11.2.3 THERMOSPRAY HPLC/MS 195
11.3 CONCLUSIONS 201
11.3.1 GAS CHROMATOGRAPHY 201
11.3.2 FAB MS 201
11.3.3 HPLC/MS 202
12 DETECTION OF SOLVENTEMIA IN EXPOSED
WORKERS
C. D. PFAFFENBERGER 205
12.1 INTRODUCTION 206
12.2 BACKGROUND 207
12.3 MATERIALS AND METHODS 210
12.3.1 VOLATILE/SEMI-VOLATILE ORGANIC COM
POUNDS IN ADIPOSE TISSUE 210
12.3.2 VOLATILE ORGANIC SOLVENTS IN HUMAN
BLOOD PLASMA 211
12.3.3 THE GC/MS/DS ANALYTICAL SYSTEM EM
PLOYED 211
12.3.4 INFORMED CONSENT 211
12.4 RESULTS AND DISCUSSION 212
CONTENTS XI
12.4.1 STUDENTS EXPOSED TO ORGANIC VAPORS
VIA THE CAMPUS ATMOSPHERE AS THE RE
SULT OF CHEMICAL REFINERIES BEING IN THE
PROXIMITY 212
12.4.2 SEVERAL DRY CLEANERS PERFORMING VARI
OUS OCCUPATIONAL TASKS 214
12.4.3 OFFICE PERSONNEL IN ROOMS ADJACENT TO
DEGREASING OPERATIONS 215
12.4.4 AIRCRAFT MACHINISTS EXPOSED TO SEVERAL
ORGANIC SOLVENTS 218
12.4.5 PESTICIDE FORMULATORS EXPOSED TO COM
MERCIAL AROMATIC SOLVENT 220
12.4.6 A PATIENT WHO DEVELOPED BLADDER CAN
CER AND BILATERAL NEUROPATHY AFTER
WORKING SEVERAL YEARS IN AN AREA
KNOWN TO BE SEVERELY POLLUTED BY ORGA
NIC CHEMICALS RESULTING FROM SPILLS .. 221
12.4.7 A WORKER OF A CARIBBEAN CHEMICAL
PLANT WHO WAS ADMITTED TO THE EMER
GENCY ROOM OF A MIAMI, FLORIDA HOSPI
TAL WITH TOTALLY UNSTABILIZED BLOOD
PRESSURE FOLLOWING HIS USUAL WORK
WEEK 222
13 AUTOMATION OF GAS CHROMATOGRAPHIC
ANALYSIS
H. FRANK 231
13.1 INTRODUCTION 231
13.2 METHODOLOGICAL PREREQUISITES AND TECH
NICAL SOLUTIONS 233
13.3 CONCLUSIONS 238
14 RESULTS ON AUTOMATIC OPTIMIZATION OF
GAS CHROMATOGRAPHY (SELECTIVITY OPTI
MIZATION) BY CLOSED LOOP ON-LINE COM
PUTER USE
R. E. KAISER AND R. I. RIEDER 241
14.1 INTRODUCTION 241
14.2 FUNDAMENTALS 245
14.3 EXPERIMENTAL 251
15 APPLICATION OF CAPILLARY GAS CHROMATO
GRAPHY IN CLINICAL CHEMISTRY
K. JACOB 261
15.1 INTRODUCTION 261
15.2 QUANTITATION OF PHYTANIC ACID IN SERUM 262
15.2.1 GAS CHROMATOGRAPHIC DETERMINATION.. 262
15.2.2 MASS FRAGMENTOGRAPHIC DETERMINATION 264
XII
CONTENTS
15.3 DETERMINATION OF ACIDIC CATECHOLAMINE
METABOLITES IN URINE 266
15.3.1 GAS CHROMATOGRAPHIC METHOD 266
15.3.2 MASS FRAGMENTOGRAPHIC METHOD 266
15.4 QUANTITATION OF HVA AND VMA IN SERUM
AND CEREBROSPINAL FLUID 268
16 DETERMINATION OF NITROGLYCERIN AND ITS
METABOLITES IN HUMAN PLASMA
K. MICHAELIS, J. A. SETTLAGE, AND H.
JAEGER 273
16.1 INTRODUCTION 273
16.2 METHOD 275
16.2.1 MASS SPECTROMETRY 275
16.2.2 EXTRACTION PROCEDURE 276
16.2.3 RESULTS AND DISCUSSION 277
16.3 CLINICAL STUDIES 280
17 POSTERS
QUANTITATIVE DETERMINATION OF PHENYL
ETHYLAMINE IN BIOLOGICAL EXTRACTS WITH
AN AUTOMATED CAPILLARY GC-CIMS DATA
SYSTEM
J. LAUBER, P. WALDMEIER 285
SIMULTANEOUS ANALYSIS OF ACIDIC, NEU
TRAL, AND BASIC DRUGS IN A WIDE BORE
CAPILLARY GC COLUMN
P. H. SILVIS, R. E. SHIREY, R. J. BARTRAM 287
DETERMINATION OF THE MYCOTOXIN DIACET
OXYSCIRPENOL AND TWO OF ITS METABOLITES
IN
SWINE SERUM AND URINE
M. GAREIS, J. BAUER, B. GEDEK 289
PHARMACOKINETIC EVALUATIONS WITH HIGH
LY SOPHISTICATED ANALYTICAL METHODS
M. NIEDER, H. JAEGER, D. LUTZ, N. HSRING,
J. M. MAURETTE, J. KAPPLER 291
QUANTITATIVE ANALYSIS OF NIFEDIPINE IN
SERUM - EXPERIENCE WITH CAPILLARY GAS
CHROMATOGRAPHY
R. KUTSCHER, H. RAMEIS 293
IDENTIFICATION OF NF-CAROBOXYMETHY I LY
SINE, A NEW AMINO ACID METABOLITE IN
RAT URINE
R. LIARDON, D. DE WEEK, S. LEDERMANN 295
CONTENTS XIII
BLOOD SAMPLES AS THE BASIS FOR RELIABLE
PHARMACOKINETIC STUDIES
W. GIELSDORF, H. JAEGER, Z. SALAMA, J.
KAPPLER 297
QUANTITATIVE CAPILLARY GAS CHROMATO
GRAHPIC PROFILING (QCGCP) OF URINARY
STEROIDS IN PEDIATRICS
J. HOMOKI, W. M. TELLER 299
GS-MS STUDIES OF ORAL ANTICOAGULANTS
J. X. DE VRIES 300
A NEW SYSTEM FOR CAPILLARY GC AND
MULTIDIMENSIONAL CAPILLARY GC
O. HELSZ 301
PERFORMING BV-(BA/BE)STUDIESWITHHIGH
LY SOPHISTICATED ANALYTICAL METHODS -
PRACTICAL EXAMPLES
H. JAEGER, W. GIELSDORF, S. W. SANDERS,
N. WIRING, N. MICHAELIS, J. RASPER.... 302
SUBJECT INDEX
305
|
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| genre_facet | Konferenzschrift 1985 Neu-Ulm |
| id | DE-604.BV024833668 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T22:22:06Z |
| institution | BVB |
| isbn | 3778513753 |
| language | English |
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| owner_facet | DE-11 |
| physical | XIII, 309 S. graph. Darst. |
| publishDate | 1987 |
| publishDateSearch | 1987 |
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| publisher | Huethig |
| record_format | marc |
| series2 | Chromatographic methods |
| spelling | Capillary gas chromatography - mass spectrometry in medicine and pharmacology ed. by Halvor Jaeger Heidelberg ; Basel ; New York Huethig 1987 XIII, 309 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chromatographic methods Literaturangaben Pharmakologie (DE-588)4045687-0 gnd rswk-swf Glaskapillargaschromatographie (DE-588)4157443-6 gnd rswk-swf GC-MS (DE-588)4414891-4 gnd rswk-swf (DE-588)1071861417 Konferenzschrift 1985 Neu-Ulm gnd-content Glaskapillargaschromatographie (DE-588)4157443-6 s DE-604 Pharmakologie (DE-588)4045687-0 s GC-MS (DE-588)4414891-4 s Jaeger, Halvor edt DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=019511535&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Capillary gas chromatography - mass spectrometry in medicine and pharmacology Pharmakologie (DE-588)4045687-0 gnd Glaskapillargaschromatographie (DE-588)4157443-6 gnd GC-MS (DE-588)4414891-4 gnd |
| subject_GND | (DE-588)4045687-0 (DE-588)4157443-6 (DE-588)4414891-4 (DE-588)1071861417 |
| title | Capillary gas chromatography - mass spectrometry in medicine and pharmacology |
| title_auth | Capillary gas chromatography - mass spectrometry in medicine and pharmacology |
| title_exact_search | Capillary gas chromatography - mass spectrometry in medicine and pharmacology |
| title_full | Capillary gas chromatography - mass spectrometry in medicine and pharmacology ed. by Halvor Jaeger |
| title_fullStr | Capillary gas chromatography - mass spectrometry in medicine and pharmacology ed. by Halvor Jaeger |
| title_full_unstemmed | Capillary gas chromatography - mass spectrometry in medicine and pharmacology ed. by Halvor Jaeger |
| title_short | Capillary gas chromatography - mass spectrometry in medicine and pharmacology |
| title_sort | capillary gas chromatography mass spectrometry in medicine and pharmacology |
| topic | Pharmakologie (DE-588)4045687-0 gnd Glaskapillargaschromatographie (DE-588)4157443-6 gnd GC-MS (DE-588)4414891-4 gnd |
| topic_facet | Pharmakologie Glaskapillargaschromatographie GC-MS Konferenzschrift 1985 Neu-Ulm |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=019511535&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT jaegerhalvor capillarygaschromatographymassspectrometryinmedicineandpharmacology |