Fundamentals of analytical chemistry:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | Undetermined |
| Veröffentlicht: |
New York <<[u.a.]>>
Saunders
1988
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| Ausgabe: | 5. ed. |
| Schriftenreihe: | Saunders golden sunburst series
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVI, 894 S. |
Internformat
MARC
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Datensatz im Suchindex
| _version_ | 1804140393342697472 |
|---|---|
| adam_text | FUNDAMENTALSOF
Analytical Chemistry
FIFTHEDITION
DOUGLASASKOOG
Stanford University
DONALDMWEST
San Jose State University
FJAMESHOLLER
University of Kentucky
H
Saunders Golden Sunburst Series
Saunders College Publishing
New York Chicago San Francisco
Philadelphia Montreal Toronto
London Sydney Tokyo
Contents Overview
Introduction i
Evaluation of Analytical Data 6
Gravimetric Methods of Analysis 57
Titrimetric Methods of Analysis 84
A Review of Aqueous-Solution Chemistry 103
The Application of Equilibrium Calculations to Complex Systems 135
Precipitation Titrations 164
Titration Curves for Simple Acid/Base Systems 182
Titration Curves for Complex Acid/Base Systems 211
Applications of Neutralization Titrations 233
Complex-Formation Titrations 257
An Introduction to Oxidation!Reduction Equilibria and Electrochemical
Theory 282
Theory of Oxidation/Reduction Titrations 315
Applications of Oxidation!Reduction Titrations 331
Potentiometric Methods 357
Electrogravimetric and Coulometric Methods 393
Voltammetry and Polarography 424
An Introduction to Spectroscopic Methods of Analysis 457
Instruments for Optical Spectroscopy 481
Molecular Spectroscopy 505
Atomic Spectroscopy Based on Ultraviolet and Visible Radiation 554
Kinetic Methods of Analysis 578
An Introduction to Chromatographic Methods 598
Gas-Liquid Chromatography 626
High-Performance Liquid Chromatography 644
The Analysis of Real Samples 667
Preparing Samples for Analysis 678
Decomposing and Dissolving the Sample 692
Eliminating Interferences 702
Chemicals, Apparatus, and Unit Operations of Analytical Chemistry 719
Selected Methods of Analysis 757
ix
X/l CONTENTS
7 Precipitation Titrations 164
7A Titration Curves in Titrimetric Methods 164
7B Titration Curves for Precipitation Reactions 165
7C Applications of Precipitation Titrations 177
8 Titration Curves for Simple Acid/Base Systems 182
8A Solutions and Indicators for Neutralization Titrations 182
8B Titration Curves for Strong Acids and Strong Bases 185
8C Properties of Weak Acid and Weak Base Systems 188
8D Properties of Buffer Solutions 193
8E Titration Curves for Weak Acids 197
8F Titration Curves for Weak Bases 202
8G Common Types of Acid/Base Indicators 204
9 Titration Curves for Complex Acid/Base Systems 2 1 1
9A Mixtures of Strong and Weak Acids or Strong and Weak Bases 211
9B Equilibrium Calculations for Compounds with Multiple Acidic or Basic
Functional Groups 214
9C Titration Curves for Polyprotic Acids and Their Conjugate Bases 221
9D The Composition of a Solution of a Polyprotic Acid as a Function of pH 227
10 Applications of Neutralization Titrations 233
1QA Reagents for Neutralization Reactions 233
JOB Typical Applications of Neutralization Titrations 238
IOC Application of Neutralization Titrations in Nonaqueous Media 245
11 Complex-Formation Titrations 257
11A Complex-Formation Reactions 257
11B Titrations with Aminopolycarboxylic Acids 259
11C Titrations with Inorganic Complexing Agents 277
12 An Introduction to Oxidation/Reduction Equilibria
and Electrochemical Theory 282
12A Oxidation/Reduction Processes 282
12B Electrochemical Cells 284
12C Electrode Potentials 288
12D Applications of Electrode Potentials 299
13 Theory of Oxidation/Reduction Titrations 315
13A Electrode Potentials for Redox Titration Systems 315
13B Oxidation/Reduction Indicators 325
13C Potentiometric End Points 329
14 Applications of Oxidation/Reduction Titrations 331
14A Auxiliary Oxidizing and Reducing Reagents 331
14B Applications of Standard Oxidants 334
14C Volumetric Applications of Reductants 341
14D Some Specialized Oxidants 344
CONTENTS xiii
15 Potentiometric Methods 357
15A Reference Electrodes 357
15B Indicator Electrodes 359
15C Instruments for the Measurement of Cell Potentials 374
15D Direct Potentiometric Measurements 376
15E Potentiometric Titrations 384
16 Electrogravimetric and Couiometric Methods 393
16A The Effect of Current on Cell Potentials 393
16B The Potential Selectivity of Electrolytic Methods 398
16C Electrogravimetric Methods of Analysis 399
16D Couiometric Methods of Analysis 407
17 Voitammetry and Polarography 424
17A Polarographic Measurements 424
17B Polarographic Currents 428
17C Half-Wave Potentials 431
17D Instrumentation 435
17E Applications of Polarography 438
17F Modified Voltammetric Methods 442
18 An Introduction to Spectroscopic Methods of Analysis 457
18A Properties of Electromagnetic Radiation 457
18B The Electromagnetic Spectrum 460
18C Absorption of Radiation 460
18D Emission of Electromagnetic Radiation 473
19 Instruments for Optical Spectroscopy 48i
19A Instrument Components 481
19B Spectroscopic Instruments 498
20~ Molecular Spectroscopy 505
20A Ultraviolet and Visible Absorption Spectroscopy 505
20B Infrared Absorption Spectroscopy 528
20C Molecular Fluorescence Methods 534
20D Automation of Photometric and Spectrophotometry Methods 538
21 Atomic Spectroscopy Based on Ultraviolet and Visible Radiation 554
21A A Comparison of Atomic and Molecular Spectroscopic Methods 554
21B Atomic Spectroscopy Based on Flame Atomization 555
21C Atomic Absorption Methods with Electrothermal Atomizers 570
21D Atomic Emission Methods Based on Atomization in Plasmas 571
22 Kinetic Methods of Analysis 578
22A Rates of Chemical Reactions; Rate Laws 578
22B The Determination of Reaction Rates 588
22C Applications of Kinetic Methods 593
xiv CONTENTS
23 An Introduction to Chromatographic Methods 598
23A A General Description of Chromatography 598
23B Migration Rates of Solutes 602
23C Band Shapes and Band Broadening 605
23D Optimization of Column Performance 614
23E A Summary of Important Relationships for Chromatography 620
23F Applications of Chromatography 620
24 Gas-Liquid Chromatography 626
24A Principles of Gas-Liquid Chromatography 627
24B Instruments for Gas-Liquid Chromatography 627
24C Liquid Phases for Gas-Liquid Chromatography 637
24D Applications of Gas-Liquid Chromatography 638
24E Typical Applications of Gas Chromatography 639
25 High-Performance Liquid Chromatography 644
25A Instruments for High-Performance Liquid Chromatography 645
25B High-Performance Partition Chromatography 648
25C High-Performance Adsorption Chromatography 650
25D High-Performance Ion-Exchange Chromatography 652
25E High-Performance Size-Exclusion Chromatography 655
25F A Comparison of High-Performance Liquid Chromatography and Gas-Liquid
Chromatography 657
25G Supercritical-Fluid Chromatography 658
25H Planar Chromatography 662
26 The Analysis of Real Samples 667
26A Choice of Method for the Analysis of Real Samples 669
26B The Accuracy Obtainable in the Analysis of Complex Materials 674
27 Preparing Samples for Analysis 678
27A Sampling 678
27B Moisture in Samples 685
27C Determination of Water in Samples 689
28 Decomposing and Dissolving the Sample 692
28A Some General Considerations 692
28B Aqueous Reagents for Dissolving or Decomposing Samples 693
28C Decomposition of Samples by Fluxes 694
28D Decomposition of Organic Compounds for Elemental Analysis 697
29 Eliminating Interferences 702
29A The Nature of the Separation Process 702
29B Separation by Precipitation 703
29C Extraction Methods 706
29D Applications of Extraction Procedures 710
29E Ion-Exchange Separations 715
29F The Separation of Inorganic Species by Distillation 716
CONTENTS XV
30 The Chemicals, Apparatus, and Unit Operations
ofAnalyticalChemistry7i9
30A The Selection and Handling of Reagents and Other Chemicals 719
30B The Cleaning and Marking of Laboratory Ware 721
30C The Evaporation of Liquids 721
30D The Measurement of Mass 722
30E The Equipment and Manipulations Associated with Weighing 731
30F Weight Titrations 734
30G The Equipment and Manipulations for Filtration and Ignition 735
30H The Measurement of Volume 742
301 The Calibration of Volumetric Ware 750
30J The Laboratory Notebook 753
30K Safety in the Laboratory 754
31 Selected Methods of Analysis 757
31A Gravimetric Methods of Analysis 758
31B Precipitation Titrations 762
31C Neutralization Titrations 765
31D Complex-Formation Titrations with EDTA 771
31E Oxidation/Reduction Titrations with Potassium Permanganate 773
31F lodimetric Titrations 779
31G lodometric Methods of Analysis 781
31H Titrations with Potassium Bromate 784
311 Potentiometric Methods 786
31J Electrogravimetric Methods 791
31K Couiometric Titrations 792
31L Voltammetry 794
31M Methods Based on the Absorption of Radiation 796
31N Molecular Fluorescence 800
310 Atomic Spectroscopy 801
31P Separation of Cations by Ion Exchange 803
31Q Gas-Liquid Chromatography 805
Appendix 1 Selected References to the Literature of Analytical Chemistry 807
Appendix 2 Some Standard and Formal Electrode Potentials 81 /
Appendix 3 Solubility-Product Constants 815
Appendix 4 Dissociation Constants for Acids 817
Appendix 5 Dissociation Constants for Bases 818
Appendix 6 Stepwise Formation Constants 819
Appendix 7 Designations and Porosities for Filtering Crucibles 821
Appendix 8 Designations Carried by Ashless Filter Papers 822
XVI CONTENTS
Appendix 9 Volumetric Calculations Using Normality and Equivalent Weight 823
Appendix 10 The Potentiometer 831
Appendix 11 The Method of Successive Approximations 833
Appendix 12 Compounds Recommended for the Preparation of Standard Solutions of Some
Common Elements 835
Answers to Questions and Problems 837
Index 873
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| spelling | Skoog, Douglas A. 1918-2008 Verfasser (DE-588)172376971 aut Fundamentals of analytical chemistry Douglas A. Skoog ; Donald M. West ; F. James Holler 5. ed. New York <<[u.a.]>> Saunders 1988 XVI, 894 S. txt rdacontent n rdamedia nc rdacarrier Saunders golden sunburst series Analytische Chemie (DE-588)4129906-1 gnd rswk-swf 1\p (DE-588)4123623-3 Lehrbuch gnd-content Analytische Chemie (DE-588)4129906-1 s 2\p DE-604 West, Donald M. Sonstige oth Holler, F. James Sonstige (DE-588)1045691720 oth HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018399157&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
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| title | Fundamentals of analytical chemistry |
| title_auth | Fundamentals of analytical chemistry |
| title_exact_search | Fundamentals of analytical chemistry |
| title_full | Fundamentals of analytical chemistry Douglas A. Skoog ; Donald M. West ; F. James Holler |
| title_fullStr | Fundamentals of analytical chemistry Douglas A. Skoog ; Donald M. West ; F. James Holler |
| title_full_unstemmed | Fundamentals of analytical chemistry Douglas A. Skoog ; Donald M. West ; F. James Holler |
| title_short | Fundamentals of analytical chemistry |
| title_sort | fundamentals of analytical chemistry |
| topic | Analytische Chemie (DE-588)4129906-1 gnd |
| topic_facet | Analytische Chemie Lehrbuch |
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