Analytical Chemistry of low concentrations:
Gespeichert in:
| 1. Verfasser: | |
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| Format: | Buch |
| Sprache: | Undetermined |
| Veröffentlicht: |
1968
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| Online-Zugang: | Inhaltsverzeichnis |
Internformat
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Datensatz im Suchindex
| _version_ | 1804140175796731904 |
|---|---|
| adam_text | I M Korenman
ANALYTICAL CHEMISTRY
OF LOW CONCENTRATIONS
Translated from Russian by F Schmorak
Israel Program for Scientific Translations
Jerusalem 1968
TABLEOFCONTENTS
Page
Listofabbreviationsv
Annotationvi
Prefacevii
I INTRODUCTION 1
Bibliography5
II CERTAIN PROPERTIES OF VERY DILUTE OLUTIONS S
Ionic strength of solutions S
Reaction of dilute aqueous solutions of st;ong acids and strong bases 10
Reaction of solutions of acid salts 13
Degree of dissociation of weak acids and bases 14
Degree of hydrolysis of salts 16
Bibliography13
»
III SENSITIVITY OF REACTIONS AND ME THODS 19
Sensitivity of reaction and experimental ;rror 20
Effect of background on the sensitivity 21
Precipitation reactions 22
Color reactions 27
Fluorescence reactions 32
Catalytic reactions 33
Titrimetric methods 34
Polarography 37
Radiochemical methods 38
Emission spectroscopic analysis 39
Flame photometry 39
Improving the sensitivity of analytical methods 41
Bibliography42
IV CONCENTRATION METHODS 48
Evaporation 49
Distillation 50
iii
Page
Coprecipitation 51
Cementation 54
Electrolysis 54
Chromatography 55
The sinking particle method 57
Concentration on oxycellulose 58
Concentration on glass wool 60
Extraction 60
Systematic concentration procedure 63
Procedure for the concentration of nicK el 64
Procedure for the isolation of zinc during analysis of high-purity
gallium 64
Procedure for a systematic separation nf the most important
cations by extraction 65
Bibliography67
V FLUCTUATIONS IN CONCENTRATIONS Ol VERY DILUTE SOLUTIONS 74
Hydrolysis 74
Effect of atmospheric oxygen 76
Effect of carbon dioxide 76
Effect of light 77
Effect of microorganisms 77
Effect of laboratory vessel material 78
Effect of other factors 83
Bibliography83
VI SOURCES OF MATERIAL LOSSES AND CONTAMINATION 87
Losses by evaporation 87
Losses on ignition 90
Losses by spattering 94
Filtration losses 96
Contamination during filtration 99
Contamination during comminution of san ple 100
Contamination by burners 100
Contamination by laboratory vessels 101
Atmospheric contamination 102
Contamination by reagents 104
Other sources of contamination 106
Bibliography106
VII PURIFICATION OF A NUMBER OF REAGENTS AND SOLVENTS 110
Bibliography 116
iv
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| spelling | Korenman, Izrail' Mironovic Verfasser aut Analytical Chemistry of low concentrations 1968 txt rdacontent n rdamedia nc rdacarrier HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018204047&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Korenman, Izrail' Mironovic Analytical Chemistry of low concentrations |
| title | Analytical Chemistry of low concentrations |
| title_auth | Analytical Chemistry of low concentrations |
| title_exact_search | Analytical Chemistry of low concentrations |
| title_full | Analytical Chemistry of low concentrations |
| title_fullStr | Analytical Chemistry of low concentrations |
| title_full_unstemmed | Analytical Chemistry of low concentrations |
| title_short | Analytical Chemistry of low concentrations |
| title_sort | analytical chemistry of low concentrations |
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