Chemical test methods of analysis:
Gespeichert in:
| Hauptverfasser: | , , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Amsterdam <<[u.a.]>>
Elsevier
2002
|
| Ausgabe: | 1. ed. |
| Schriftenreihe: | Wilson and Wilson's Comprehensive analytical chemistry
36 |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVII, 317 S. graph. Darst. |
| ISBN: | 0444502610 |
Internformat
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| 100 | 1 | |a Zolotov, Jurij A. |d 1932- |e Verfasser |0 (DE-588)11947929X |4 aut | |
| 245 | 1 | 0 | |a Chemical test methods of analysis |c Yu. A. Zolotov ; V. M. Ivanov ; V. G. Amelin |
| 250 | |a 1. ed. | ||
| 264 | 1 | |a Amsterdam <<[u.a.]>> |b Elsevier |c 2002 | |
| 300 | |a XVII, 317 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Wilson and Wilson's Comprehensive analytical chemistry : 36 | |
| 700 | 1 | |a Ivanov, V. M. |e Verfasser |4 aut | |
| 700 | 1 | |a Amelin, V. G. |e Verfasser |4 aut | |
| 830 | 0 | |a Wilson and Wilson's Comprehensive analytical chemistry |v 36 |w (DE-604)BV000900805 |9 36 | |
| 856 | 4 | 2 | |m HBZ Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018335752&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 999 | |a oai:aleph.bib-bvb.de:BVB01-018335752 | ||
Datensatz im Suchindex
| _version_ | 1804140306106417152 |
|---|---|
| adam_text | Titel: Chemical test methods of analysis
Autor: Zolotov, Jurij A
Jahr: 2002
Contents
Series Editor s Preface.............................xv
Authors Preface...............................xvii
Chapter 1. General Features of Test Systems..........................1
1.1 Fields of use and advantages of test systems, terminology.....1
1.1.1 Terminology..........................1
1.1.2 Fields of use and advantages of test methods........2
1.2 Some history.............................5
1.3 Classification of test methods....................7
1.4 General requirements and metrology................8
1.5 Limitations of test methods.....................10
References.................................10
Chapter 2. Chemical Principles of Test Methods: Reactions and Reagents . . 13
2.1 Selection of reactions and reagents.................13
2.1.1 Some general remarks...................13
2.1.1.1 Acid-base reactions................14
2.1.1.2 Oxidation-reduction reactions..........15
2.1.1.3 Reactions of complex formation.........16
2.1.1.4 Reactions of organic synthesis..........21
2.2 Variants of reagent applications..................23
2.2.1 Preliminary prepared solutions...............23
2.2.2 Auxiliary agents.......................23
2.2.3 Reagents on solid matrices.................24
2.2.3.1 Reagents on papers................24
2.2.3.2 Reagents immobilized on synthetic organic
polymers.....................26
2.2.3.3 Reagents on silica gels..............28
2.2.3.4 Selection of optimum conditions of testing ... 29
2.3 Immobilization of chemical reagents. Matrices and methods... 30
2.3.1 Immobilization through physical adsorption (physical
immobilization).......................31
2.3.1.1 Supports......................32
2.3.1.2 Support adsorption capacity...........34
2.3.1.3 Selectivity.....................36
ix
2.3.1.4 Reversed-phase silica gels modified with
various groups..................
2.3.1.5 Xerogel sorbents .... ............
2.3.2 Chemical immobilization..... ............
2.4 Catalytic reactions........................
2.4.1 Enzymes..........................
2.4.2 Catalytic non-enzymatic reactions ............
2.5 Immunoassay procedures.....................
References.................................
Chapter 3. Methods and Tools for Analysis of Liquid Samples...........
3.1 Paper Strips and Their Analogues.................
3.1.1 Indicator papers for determining the concentration
by immersing into the solution and measuring the
results............................
3.1.2 Preconcentration of the reaction products.........
3.1.3 Paper chromatography...................
3.1.4 Reaction rate measurements................
3.1.5 Test titrations with papers.................
3.1.6 Colorimetry with indicator papers.............
3.2 Indicator powders..........................
3.3 Indicator tubes...........................
3.4 Tablets and similar forms.....................
3.5 Regular ampoules and droppers...... ...........
3.6 Self-filling ampoules........................
3.7 Titration kits................ ...........
3.8 Other tools.............................
References................................
Chapter 4. Systems of Measurements and Registration................
4.1 Requirements for methods of analysis of liquids.........
4.2 Visual methods...........................
4.3 Colorimetric visual methods....................
4.4 Use of more sophisticated but still compact instruments ....
4.5 Measurement of colour......................
4.6 Titrimetric methods........................
4.7 Chemical dosimeters........................
4.8 Mini devices with built-in software methods...........
4.9 Test concentrators incorporating indicator powders.......
References.................................
Chapter 5. Methodology and Application Areas of Test Systems.........
5.1 Fields of use..........................
5.2 Attestation of methods and their official endorsement......
37
41
48
53
53
55
56
59
. 69
69
69
73
74
89
89
90
90
94
100
105
108
108
111
112
119
119
119
120
121
130
131
132
134
137
138
139
139
140
x
5.3 Sample screening.........................143
References.................................145
Chapter 6. Determination of Inorganic Components in Water and Soil.... 147
6.1 Sum parameters..........................148
6.1.1 Water hardness......................148
6.1.2 Total alkalinity and acidity of water...........151
6.1.3 Total contents of heavy metals..............152
6.1.4 Active chlorine.......................155
6.1.5 pH measurement of water solutions...........158
6.2 Cations...............................159
6.2.1 Silver............................159
6.2.2 Aluminium.........................160
6.2.3 Ammonium.........................161
6.2.4 Arsenic...........................163
6.2.5 Beryllium..........................163
6.2.6 Bismuth..........................163
6.2.7 Calcium...........................163
6.2.8 Cadmium..........................164
6.2.9 Cobalt............................167
6.2.10 Chromium.........................169
6.2.11 Copper...........................169
6.2.12 Iron.............................173
6.2.13 Germanium........................178
6.2.14 Mercury..........................178
6.2.15 Indium...........................182
6.2.16 Potassium.........................182
6.2.17 Manganese.........................182
6.2.18 Molybdenum........................183
6.2.19 Sodium...........................184
6.2.20 Nickel............................184
6.2.21 Lead............................186
6.2.22 Palladium.........................189
6.2.23 Titanium..........................189
6.2.24 Uranium..........................190
6.2.25 Zinc.............................190
6.3 Anions...............................191
6.3.1 Bromides..........................191
6.3.2 Chlorides..........................192
6.3.3 Cyanides..........................194
6.3.4 Chromates.........................195
6.3.5 Fluorides..........................195
6.3.6 Iodides...........................196
6.3.7 Nitrates and nitrites....................197
xi
6.3.8 Phosphates.........................203
6.3.9 Sulphides..........................
6.3.10 Thiocyanates........................
6.3.11 Silicates ..........................
6.3.12 Sulphates..........................
6.3.13 Sulphites..........................
6.4 Other Inorganic Components...................^6
6.4.1 Hydrazine.........................
6.4.2 Hydrogen peroxide.....................
6.4.3 Oxygen...........................^09
6.4.4 Ozone............................
References.................................
Chapter 7. Determination of Organic Components in Water and Soil.....215
7.1 Sum parameters..........................215
7.1.1 Chemical oxygen demand (COD).............215
7.1.2 Biochemical oxygen demand (BOD)............217
7.1.3 Total organic carbon (TOO)................217
7.1.4 Total nitrogen.......................218
7.1.5 Adsorbable organically bound halogens (AOX)......218
7.2 Petroleum hydrocarbons......................219
7.3 Polyaromatic hydrocarbons (PAH)................222
7.4 Organochlorine compounds....................223
7.5 Polychlorinated biphenyls (PCB).................224
7.6 Various pesticides.........................226
7.7 Other organic compounds.....................229
7.7.1 Phenols...........................229
7.7.2 1-Naphthol.........................231
7.7.3 Nitrophenols........................232
7.7.4 Anionic surfactants....................232
7.7.5 Cationic surfactants....................233
7.7.6 Non-ionic surfactants...................234
7.7.7 Aniline...........................235
7.7.8 Sum total content of sulphur-containing reductants. . . 235
7.7.9 Organomercury compounds................235
7.7.10 Diethylhydroxylamine...................236
References.................................237
Chapter 8. Analysis of Air and Vapours............................239
8.1 Analysis using indicator tubes..................239
8.1.1 Principles of operation and design of indicator tubes . . 240
8.1.2 Chemical composition of indicator powders.......241
8.1.3 Methods of concentration determination.........243
8.1.4 Air samplers..................... . 245
xii
8.1.5 Indicator tube kits and their applications........246
8.2 Application of pocket analysers..................253
References.................................255
Chapter 9. Detection of Alcohol Vapours, Narcotics, Chemical Weapons
and Explosives..............................................257
9.1 Alcohol vapours..........................257
9.2 Narcotics..............................261
9.3 Chemical weapons.........................263
9.4 Explosives.............................270
References.................................273
Chapter 10. Use of Test Methods in Medicine........................275
10.1 Determination of glucose.....................276
10.2 Testing for cholesterol.......................281
10.3 Other medical applications of test methods...........283
10.4 Drug control............................286
References.................................290
Chapter 11. Some Other Applications of Test Methods.................293
11.1 Determination of gold and silver by the touchstone.......293
11.1.1 The touchstone and test needles.............294
11.1.2 Reagents..........................294
11.2 Use of Test Methods In Education................297
References.................................301
Chapter 12. Conclusions and Perspectives...........................303
Appendix: Producers and Suppliers of Test Kits......................305
About the Authors..............................311
Index.....................................313
|
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| indexdate | 2024-07-09T21:57:53Z |
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| isbn | 0444502610 |
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| spelling | Zolotov, Jurij A. 1932- Verfasser (DE-588)11947929X aut Chemical test methods of analysis Yu. A. Zolotov ; V. M. Ivanov ; V. G. Amelin 1. ed. Amsterdam <<[u.a.]>> Elsevier 2002 XVII, 317 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Wilson and Wilson's Comprehensive analytical chemistry : 36 Ivanov, V. M. Verfasser aut Amelin, V. G. Verfasser aut Wilson and Wilson's Comprehensive analytical chemistry 36 (DE-604)BV000900805 36 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018335752&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Zolotov, Jurij A. 1932- Ivanov, V. M. Amelin, V. G. Chemical test methods of analysis Wilson and Wilson's Comprehensive analytical chemistry |
| title | Chemical test methods of analysis |
| title_auth | Chemical test methods of analysis |
| title_exact_search | Chemical test methods of analysis |
| title_full | Chemical test methods of analysis Yu. A. Zolotov ; V. M. Ivanov ; V. G. Amelin |
| title_fullStr | Chemical test methods of analysis Yu. A. Zolotov ; V. M. Ivanov ; V. G. Amelin |
| title_full_unstemmed | Chemical test methods of analysis Yu. A. Zolotov ; V. M. Ivanov ; V. G. Amelin |
| title_short | Chemical test methods of analysis |
| title_sort | chemical test methods of analysis |
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