Verfügbarkeit: An introduction to polymer science

An introduction to polymer science:

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Bibliographische Detailangaben
1. Verfasser:	Elias, Hans-Georg 1928- (VerfasserIn)
Format:	Buch
Sprache:	English
Veröffentlicht:	Weinheim [u.a.] VCH 2005
Ausgabe:	1. ed., 4. repr.
Schlagworte:	Polymere Lehrbuch
Online-Zugang:	Inhaltsverzeichnis
Beschreibung:	XXII, 470 S. Ill., graph. Darst.
ISBN:	3527287906

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245	1	0	\|a An introduction to polymer science \|c Hans-Georg Elias
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Datensatz im Suchindex

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adam_text	Contents Contents Preface ................................................. List of Symbols for Physical Quantities Contents ............................................... 1. Introduction ............................................................................................ 1 1.1. Fundamental Terms ....................................................................... 1 1.2. History ........................................................................................... 4 Chemistry 2. Chemical Structure ............................................................................... 10 2.1. Constitution ..................................................................................... 10 2.1.1. Nomenclature ................................................................... 10 2.1.2. Monomers for Polymers ................................................... 12 2.1.3. Process-Based Terms ........................................................ 12 2.1.4. Structure-Based Terms ..................................................... 14 2.1.5. One-, Two-and Three-Dimensional Macromolecules ........ 16 2.1.6. Branched Macromolecules ............................................... 20 2.2. Molar Mass and Molar Mass Distribution .................................... 23 2.2.1. Degree of Polymerization ............................................... 23 2.2.2. Molecular Mass, Molecular Weight, Molar Mass .............. 24 2.2.3. Distribution Functions ...................................................... 27 2.2.4. Experimental Methods ..................................................... 31 Mass Spectrometry ....................................................... 31 Size-Exclusion Chromatography .................................. 32 2.3. Configuration ................................................................................. 34 2.3.1. Stereoisomers ................................................................... 34 2.3.2. Ideal Tacticity ................................................................... 35 2.3.3. Real Tacticity ................................................................... 40 2.3.4. Experimental Methods ..................................................... 41 2.4. Conformation ................................................................................ 43 2.4.1. Microconformation .......................................................... 43 2.4.2. Macroconformation in Crystals ........................................ 45 2.4.3. Macroconformation in Melts and Solutions ..................... 46 3. Chain-Growth Polymerizations ................................................................ 50 3.1. Overview of Polymerizations ......................................................... 50 Contents XIII 3.1.1. Classes of Polymerizations ............................................... 50 3.1.2. Examples of Polymerizations ........................................... 52 3.1.3. Functionality .................................................................... 53 3.1.4. Experimental Investigations ............................................. 53 3.1.5. Kinetics and Statistics ....................................................... 54 3.2. Thermodynamics of Polymerizations ............................................ 54 3.2.1. Polymerization Equilibria ................................................ 54 3.2.2. Critical Polymerization Temperatures .............................. 55 3.2.3. Ceiling and Floor Temperatures ....................................... 56 3.2.4. Polymerization Enthalpies and Entropies ......................... 57 3.2.5. Chain and Ring Formation ............................................... 58 3.3. Statistics of Chain Polymerizations ................................................ 59 3.4. Anionie Polymerizations ............................................................... 63 3.4.1. Ion Equilibria ................................................................. 63 3.4.2. Monomers ....................................................................... 64 3.4.3. Initiators .......................................................................... 65 3.4.4. Living Polymerizations .................................................... 66 3.4.5. Termination and Chain Transfer ...................................... 68 3.4.6. Stereocontrol ................................................................... 70 3.5. Cationic Polymerizations ............................................................... 71 3.5.1. Monomers ....................................................................... 71 3.5.2. Initiators .......................................................................... 72 3.5.3. Propagation ..................................................................... 74 3.5.4. Termination and Chain Transfer ...................................... 75 3.6. Insertion Polymerizations ............................................................... 77 3.6.1. Introduction .................................................................... 77 3.6.2. Ziegler-Natta Polymerizations .......................................... 78 Heterogeneous Ziegler Catalysts ................................. 79 Homogeneous Ziegler Catalysts ................................. 81 Kinetics ...................................................................... 82 3.6.3. Metathesis Polymerizations .............................................. 83 Metatheses ................................................................. 83 Polyelimination of Aliphatic Olefins ........................... 84 Ring-Opening Polymerization of Cycloolefins ............ 84 3.6.4. Group Transfer Polymerizations ...................................... 85 3.7. Free-Radical Polymerizations ...................................................... 86 3.7.1. Introduction ..................................................................... 86 3.7.2. Formation of Free Radicals ............................................. 86 Self-Initiated Polymerizations ..................................... 86 Thermal Initiators ...................................................... 88 Redox Initiators ......................................................... 90 Photo Initiators .......................................................... 90 Contents 3.7.3. Initiation, Propagation and Termination .......................... 90 3.7.4. Steady State ..................................................................... 92 3.7.5. Ideal Kinetics ................................................................... 93 3.7.6. Allyl Polymerizations ...................................................... 96 3.7.7. Kinetic Chain Transfer ..................................................... 96 3.7.8. Non-Ideal Kinetics ........................................................... 100 3.7.9. Industrial Polymerizations ................................................ 102 Reactors ..................................................................... 102 Polymerization in Bulk ............................................... 103 Polymerization in Solution and by Precipitation ......... 104 Polymerization in Suspension ..................................... 104 Polymerization in Emulsion ....................................... 105 3.8. Copolymerizations ......................................................................... 107 3.8.1. Introduction .................................................................... 107 3.8.2. Copolymerization Equation ............................................. 107 3.8.3. Sequence Statistics ........................................................... 110 3.8.4. Kinetics of Radical Copolymerizations ............................ Ill 3.8.5. Q.e-Scheme ..................................................................... 112 3.8.6. Ionic Copolymerizations ................................................. 114 Appendix to Chapters ............................................................................. 115 A 3-1: Equilibria ........................................................................ 115 A 3-2: Poisson Distribution ......................................................... 116 A 3-3 Stationary State ................................................................ 116 A 3-4: Schulz-Flory Distribution ................................................ 117 4. Step-Growth Polymerizations and Polymer Reactions ............................. 120 4.1. Polycondensations and Polyadditions ........................................... 120 4.1.1. Introduction .................................................................... 120 4.1.2. Chemistry of Bifunctional Polycondensations .................. 121 4.1.3. Equilibria of Bifunctional Polycondensations ..................124 Equilibrium Constants ............................................... 124 Number-Average Degrees of Polymerization .............. 124 Distributions of Degrees of Polymerization ................ 126 4.1.4. Kinetics of Bifunctional Reactions .................................. 127 4.1.5. Diffusion-Controlled Polycondensations ..........................129 4.1.6. Activated Polycondensations ...........................................130 4.1.7. Cyclizations ....................................................................131 Intramolecular Cyclizations ........................................ 131 Intramerar Cyclizations ..............................................132 4.1.8. Polyadditions .................................................................. 135 Polyurethanes PUR ....................................................135 Epoxy Resins EP ........................................................ 137 4.1.9 Branching Polycondensations .........................................138 Contents X V Hyperbranched Polymers .......................................... 139 Dendritic Polymers ..................................................... 139 Gel Point ................................................................... 139 Alkyd Resins .............................................................. 142 Phenol-Formaldehyde Resins (Phenolic Resins) PF ..... 142 Melamine Resins MF and Urea Resins UF .................... 144 4.2. Biological Polymerizations ........................................................... 145 4.2.1. Introduction .................................................................... 145 4.2.2. Nucleic Acids .................................................................. 146 4.2.3. Proteins ........................................................................... 148 Structure ................................................................... 148 Protein Syntheses ....................................................... 150 Enzymes .................................................................... 152 Silk ............................................................................ 153 Wool ........................................................................... 153 Collagen and Elastin ................................................... 154 4.2.4. Lignins ............................................................................ 155 4.2.5. Polysaccharides ............................................................... 156 Nomenclature ............................................................ 157 Biosyntheses ............................................................. 157 Celluloses ................................................................... 158 Amylose and Amylopectin ........................................ 159 Other Polysaccharides ................................................ 160 4.2.6. Polyesters ........................................................................ 161 4.2.7. Polyprenes ...................................................................... 161 4.3. Reactions of Macromolecules ........................................................ 162 4.3.1. Polymer Analog Reactions ............................................... 162 4.3.2. Chain Extensions ............................................................. 163 Block Formation ........................................................ 163 Grafting Reactions ......................................................164 4.3.3. Cross-Linking Reactions ................................................. 165 4.3.4. Degradation .................................................................... 166 Chain Scission ............................................................ 166 Depolymerization ...................................................... 167 Physical Chemistry 5 Size and Shape of Molecules ......................................................................170 5.1. Introduction ................................................................................... 170 5.2. Scattering Methods ....................................................................... 170 5.2.1. Static Light Scattering ..................................................... 171 Infinite Dilution .........................................................171 Concentration Dependence ........................................173 XVI Contents Angular Dependence ................................................. 173 5.2.2. Small Angle Х -Ray and Neutron Scattering ..................... 175 5.3. Ideal Coil Molecules ...................................................................... 176 5.3.1. Macroconformations ....................................................... 176 5.3.2. Random Coils .................................................................. 179 5.3.3. Steric Factor and Hindrance Parameter ............................181 5.3.4. Radius of Gyration .......................................................... 183 5.3.5. Coil Density ..................................................................... 184 5.4. Worm-Like Chains .......................................................................185 5.5. Real Coil Molecules ....................................................................... 186 5.5.1 Excluded Volume .......................................................... 186 5.5.2. Dependence on Molar Mass ............................................187 5.5.3. Branched Polymers .........................................................189 5.5.4. Tethered Chains .............................................................. 191 5.6. Euclidian Bodies ........................................................................... 191 5.6.1. Spheres and Spheroids ....................................................191 5.6.2. Rods ............................................................................... 192 5.6.3. Excluded Volume ...........................................................193 5.7. Scaling ..........................................................................................195 5.7.1. Self-Similarity ................................................................. 195 5.7.2. Overlap of Coils .............................................................. 196 5.7.3. Fractals ........................................................................... 198 5.8. Viscosimetric Dimensions ..............................................................200 5.8.1. Introduction ....................................................................200 5.8.2. Concentration Dependence ..............................................201 5.8.3. Molar Mass Dependence .................................................203 5.8.4. Hydrodynamic Volumes .................................................205 5.9. Interpretation of [η] =f(M) ..........................................................206 5.9.1. Unperturbed Coils ...........................................................206 5.9.2. Flory Constant of Flexible Molecules ..............................207 5.9.3. Pertutbed Coils ................................................................210 5.9.4. Rods ................................................................................211 5.9.5. Branched Polymers ........................................................211 Appendix to Chapter 5 .............................................................................213 A 5-1: End-to-End Distances of Freely Rotating Chains ...........213 A 5-2: End-to-End Distance and Radius of Gyration ................214 A 5-3: Chains with Persistence ...................................................216 6 Solution Thermodynamics ........................................................................218 6.1. Phenomena ...................................................................................218 Contents XVII 6.1.1. Introduction ....................................................................218 6.1.2. Concentration Ranges ......................................................219 6.1.3. Solubility Parameters ......................................................220 6.2. Statistical Thermodynamics ..........................................................223 6.2.1. Types of Solutions ...........................................................223 6.2.2. Lattice Theory ................................................................224 Enthalpy of Mixing ....................................................225 Entropy of Mixing .....................................................226 Gibbs Energy of Mixing ............................................227 6.2.3. Phase Separation .............................................................227 Solutions of Amorphous Polymers ............................227 Polymer Blends .........................................................230 Critical Solution Temperatures ...................................231 Solutions of Crystalline Polymers ..............................232 6.3. Osmotic Pressure ...........................................................................233 6.3.1. Fundamentals .................................................................233 6.3.2. Membrane Osmometry ...................................................235 6.3.3. Vapor Phase Osmometry ..................................................236 6.3.4. Virial Coefficients ...........................................................237 6.3.5. Overlap Concentrations ...................................................239 6.4. Association ....................................................................................241 6.4.1. Open Associations ...........................................................242 6.4.2. Closed Associations ........................................................243 6.4.3. Gels .................................................................................245 7. Polymer Hydrodynamics .........................................................................247 7.1. Introduction ..................................................................................247 7.2. Diffusion in Solution ......................................................................247 7.2.1. Mutual Diffusion ............................................................247 7.2.2. Frictional Coefficients ....................................................248 7.2.3. Spring-and-Bead Models .................................................250 7.3. Sedimentation in Solution ..............................................................252 7.3.1. Fundamentals ..................................................................252 7.3.2. Sedimentation Rate ..........................................................253 7.3.3. Sedimentation Equilibrium .............................................255 7.4. Viscosity of Solutions and Melts ....................................................256 7.4.1. Introduction ....................................................................256 7.4.2. Viscometry ......................................................................256 7.4.3. Newtonian Viscosities .....................................................259 7.4.4. Non-Newtonian Viscosities ..............................................261 7.4.5. Flow Curves .....................................................................263 7.4.6. Extensional Viscosities ....................................................265 Худі Contents 7.5. Molecular Dynamics of Melts .......................................................266 7.5.1. Diffusion .........................................................................266 7.5.2. Viscosity .........................................................................267 Appendix to Chapter 7 ..............................................................................271 A 7-1: Hydrodynamically Effective Volume ..............................271 Physics 8. Polymer Assemblies .................................................................................273 8.1. Introduction .................................................................................273 8.2. Melts and Amorphous States ........................................................274 8.3. Crystalline Polymers ....................................................................275 8.3.1. Introduction ...................................................................275 8.3.2. Х -Ray Diffraction ...........................................................276 8.3.3. Crystal Structures ............................................................279 8.3.4. Macroconformation and Packing ....................................281 8.3.5. Chain Folding .................................................................284 8.3.6. Morphology ...................................................................286 8.3.7. Orientation .....................................................................288 8.4. Liquid Crystals ............................................................................290 8.4.1. Introduction ...................................................................290 8.4.2. Mesogens and Mesophases ..............................................290 8.4.3. Thermotropic Liquid Crystals .........................................292 8.4.4. Lyotropic Liquid Crystals ..............................................293 8.5. Block Copolymers ........................................................................294 8.6. Ionomers .....................................................................................297 9. Transitions and Relaxations ....................................................................299 9.1. Introduction ..................................................................................299 9.2. Thermal Properties .......................................................................299 9.2.1. States and Methods ..........................................................299 9.2.2. Thermal Expansion .........................................................301 9.2.3. Heat Capacities ...............................................................302 9.2.4. Heat Conductivity ...........................................................303 9.3. Crystallization ..............................................................................304 9.3.1. Nucleation ......................................................................304 9.3.2. Crystallization Rate .........................................................306 9.4. Melting Temperature ....................................................................309 9.4.1. Phenomena ....................................................................309 9.4.2. Effector Molar Mass ......................................................310 Contents XIX 9.4.3. Effect of Crystallite Size ..................................................311 9.4.4. Effect of Constitution .....................................................311 9.5. Thermal Transitions and Relaxations ...........................................313 9.6. Glass Temperatures ...................................................................... 315 9.6.1. Static Glass Temperature .................................................315 9.6.2. Dynamic Glass Temperatures ..........................................316 9.6.3. Effects of Constitution ...................................................317 9.6.4. Plasticization ...................................................................319 9.7. Diffusion and Permeation ............................................................. 321 9.7.1. Permeation of Gases ........................................................321 9.7.2. Permeation of Liquids ....................................................322 10. Solid State Properties ..............................................................................325 10.1. Introduction .................................................................................325 10.2. Deformation .................................................................................326 10.2.1. Introduction ...................................................................326 10.2.2. Tensile Tests ...................................................................326 10.2.3. Tensile Behavior ..............................................................329 10.2.4. Moduli and Poisson Ratios ..............................................330 10.3. Energy Elasticity ..........................................................................333 10.3.1. Introduction ....................................................................333 10.3.2. Theoretical and Experimental Moduli .............................333 10.4. Entropy Elasticity .......................................................................... 336 10.4.1. Chemical Thermodynamics ............................................336 10.4.2. Structure of Networks .....................................................337 10.4.3. Statistical Thermodynamics ............................................338 10.4.4. Models ...........................................................................339 10.4.5. Uniaxial Stretching ......................................................... 340 10.4.6. Real Stress-Strain Behavior ..............................................342 10.4.7. Shearing .........................................................................342 10.5. Viscoelasticity ...............................................................................344 10.5.1. Fundamentals .................................................................344 10.5.2. Models ............................................................................344 10.5.3. Stress Relaxation .............................................................346 10.5.4. Creep Experiment ............................................................348 10.5.5. Boltzmann Superposition Principle .................................349 10.5.6. Dynamic Measurements .................................................351 10.5.7. Shear Moduli of Melts ....................................................354 10.6. Failure ..........................................................................................356 10.6.1. Fracture Phenomena .......................................................356 10.6.2. Theoretical Fracture Strengths .........................................357 XX Contents 10.6.3. Failure Strengths .............................................................358 10.6.4. Fracture Strengths of Brittle Materials .............................359 10.6.5. Fracture Strength of Ductile Polymers .............................362 10.6.6. Impact Strengths .............................................................363 10.6.7. Stress Crazing .................................................................365 10.7. Surface Properties .......................................................................366 10.7.1. Surface Tension ..............................................................366 10.7.2. Hardness ........................................................................367 10.7.3. Friction ..........................................................................367 10.7.4. Abrasion .........................................................................368 10.8. Electrical Properties .....................................................................369 10.8.1. Introduction ...................................................................369 10.8.2. Relative Permittivity ........................................................369 10.8.3. Resistivities .....................................................................370 10.8.4. Dissipation Factors .........................................................371 10.8.5. Electrostatic Charging .....................................................373 10.8.6. Electrically Conducting Polymers ...................................373 10.9. Optical Properties ........................................................................375 10.9.1. Refractive Index .............................................................375 10.9.2. Light Transmission and Gloss ........................................376 Technology 11. Polymer Auxiliaries ................................................................................379 11.1. Polymer Systems ...........................................................................379 11.2. Formulation .................................................................................380 11.3. Stabilizers ....................................................................................381 11.3.1. Antioxidants ...................................................................381 11.3.2. Light Stabilizers .............................................................383 11.3.3. Heat Stabilizers ..............................................................384 11.3.4. Flame Retardants ............................................................384 11.4. Colorants .....................................................................................385 11.5. Fillers ............................................................................................385 11.6. Emigration of Auxiliaries .............................................................386 12. Elastomers ................................................................................................388 12.1. Introduction ..................................................................................388 12.2. Processing ....................................................................................388 12.3 Rubber Types ..............................................................................389 12.4. Vulcanization ..............................................................................390 Contents XXI 12.5. Properties ...................................................................................391 12.6. Reclaiming ...................................................................................392 13. Fibers ........................................................................................................394 13.1. Introduction .................................................................................394 13.2. Production ...................................................................................395 13.3. Fiber Spinning ..............................................................................396 13.4. Textile Fibers ...............................................................................399 13.5. Industrial Fibers ..........................................................................402 13.6. Recycling .....................................................................................403 14. Plastics ......................................................................................................404 14.1. Introduction .................................................................................404 14.2. Processing ....................................................................................405 14.2.1. Overview .........................................................................405 14.2.2. Processing Steps .............................................................406 14.2.3. Processing of Viscous Materials .......................................408 14.2.4. Processing of Viscoelastic Materials ................................409 14.3. Thermoplastics ............................................................................411 14.4. Thermosets ...................................................................................414 14.5. Filled and Reinforced Plastics ......................................................417 14.5.1. Mixing Rules .................................................................418 14.5.2. Moduli ..........................................................................418 14.5.3. Interlayers ......................................................................420 14.5.4. Strengths and Elongations ..............................................421 14.5.5. Thermal Properties ........................................................423 14.6. Polymer Blends ............................................................................425 14.6.1. Mechanical Mixing ........................................................426 14.6.2. In-situ Polymerizations ..................................................427 14.6.3. Rubber-Modified Thermoplastics ...................................428 14.7. Disposal ........................................................................................430 14.7.1. Landfills .........................................................................431 14.7.2. Biological Degradation ...................................................431 14.7.3. Recycling .......................................................................432 15. Appendix .....................................................................................436 15.1. Physical Quantities and Units .......................................................436 Table 15-1 Names and Symbols for Physical Quantities ..............436 XXII Contents Table 15-2 Important SI Derived Units ........................................437 Table 15-3 SI Prefixes .................................................................437 Table 15-4 Older Non-SI Units ...................................................438 Table 15-5 Fundamental Constants ..............................................439 Table 15-6 Conversion of Out-Dated and Anglo-Saxon Units ......439 15.2. Concentrations .............................................................................444 15.3. Ratios of Physical Quantities .......................................................444 15.4. Abbreviations of Plastics, Fibers, Elastomers, etc .........................445 15.5. Generic and Trade Names of Fibers and Plastics .........................447 16. Index ........................................................................................................449
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author	Elias, Hans-Georg 1928-
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author_facet	Elias, Hans-Georg 1928-
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discipline	Chemie / Pharmazie Werkstoffwissenschaften Chemie Chemie-Ingenieurwesen
edition	1. ed., 4. repr.
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spelling	Elias, Hans-Georg 1928- Verfasser (DE-588)128433426 aut An introduction to polymer science Hans-Georg Elias 1. ed., 4. repr. Weinheim [u.a.] VCH 2005 XXII, 470 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Polymere (DE-588)4046699-1 gnd rswk-swf (DE-588)4123623-3 Lehrbuch gnd-content Polymere (DE-588)4046699-1 s DE-604 Digitalisierung UB Regensburg application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017296762&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis
spellingShingle	Elias, Hans-Georg 1928- An introduction to polymer science Polymere (DE-588)4046699-1 gnd
subject_GND	(DE-588)4046699-1 (DE-588)4123623-3
title	An introduction to polymer science
title_auth	An introduction to polymer science
title_exact_search	An introduction to polymer science
title_full	An introduction to polymer science Hans-Georg Elias
title_fullStr	An introduction to polymer science Hans-Georg Elias
title_full_unstemmed	An introduction to polymer science Hans-Georg Elias
title_short	An introduction to polymer science
title_sort	an introduction to polymer science
topic	Polymere (DE-588)4046699-1 gnd
topic_facet	Polymere Lehrbuch
url	http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017296762&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
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