Infrared and Raman characteristic group frequencies: tables and charts
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Chichester [u.a.]
Wiley
2006
|
| Ausgabe: | 3. ed., reprinted as paperback |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Hier auch später erschienene, unveränderte Nachdrucke |
| Beschreibung: | XV, 347 S. graph. Darst. |
| ISBN: | 9780470093078 |
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| adam_text | Contents List of Charts and Figures xi List of Tables xiii Symbols Used xvi Preface xvii 1 2 3 Introduction Spurious Bands in Infrared and Raman Spectra Spurious Bands at Any Position Spurious Bands at Specific Positions Positive and Negative Spectral Interpretation Negative Spectral Interpretation Positive Spectral Interpretation Regions for Preliminary Investigation Preliminary Regions to Examine Confirmation Chemical Modification Collections of Reference Spectra Final Comment References 1 4 5 9 9 10 10 10 10 14 14 14 48 48 Alkane Group Residues: C-H Group Alkane Functional Groups Alkane C-H Stretching Vibrations Alkane C-H Deformation Vibrations Alkane C-C Vibrations: Skeletal Vibrations References 50 50 50 51 53 67 Alkenes, Oximes, Imines, Amidines, Azo Compounds: C=C, C=N, N=N Groups Alkene Functional Group, ^C=C^ 68 68 Alkene ^C=C^ Stretching Vibrations Alkene C-H Stretching Vibrations Alkene C-H Deformation Vibrations Alkene Skeletal Vibrations Oximes, ^C=N—OH, Iminės, ^C=N— , Amidines, / 4 69 69 69 78 N-C=N—, etc. Azo Compounds, -N=NReferences 80 81 Triple Bond Compounds: -C=C-, -C^N, -NsC, _N=N Groups Alkyne Functional Group, -C=CAlkyne CsC Stretching Vibrations Alkyne C-H Vibrations Alkyne Skeletal Vibrations Nitriles, -C=N Isonitriles, ֊NsC Nitrile V-oxides, -CsN -֊» О 82 Cyanamides, 5 68 N— C^N 82 82 82 82 84 85 85 86 Diazonium Salts, Aryl-NsN+X՜ References 86 86 Cumulated Doubie-bond Compounds: X=Y=Z Group Allenes, ^C=C=C^ 88 Isocyanates, -N=C=0, and Cyanates Isothiocyanates, -N=C=S 88 89 88
Contents VI 6 Thiocyanates, -S-C=N Selenocyanates and Isoselenocyanates Azides, -N=N+=N~ Diazo Compounds, ^C=N+=N~ 89 90 90 90 Carbodi-imides, -N=C=NReferences 93 93 Hydroxyl Group Compounds: O-H Group Alcohols, R-OH Alcohol O-H Stretching Vibrations Alcohol C-0 Stretching Vibrations Alcohol О-H Deformation Vibrations Phenols References 94 94 94 94 95 99 99 7 Ethers: G,-0-G2 Group References 101 104 8 Peroxides and Hydroperoxides: -O-O-Group References 105 106 9 Amines, Iminės, and Their Hydrohalides Amine Functional Groups Amine N-H Stretching Vibrations Amine N-H Deformation Vibrations Amine C-N Stretching Vibrations . Amine ^N—CH3 and N— CH2— Absorptions Other Amine Bands Amine Hydrohalides, -NH3+, ^NH2+, —NH+ and 107 107 107 107 107 The Carbonyl Group: C=0 Introduction Ketones, ^C=0 Ketone C=0 Stretching Vibrations Methyl and Methylene Deformation Vibrations in Ketones Ketone Skeletal and Other Vibrations О Quinones у |] and 115 115 117 117 117 117 122 о Aldehydes, -CHO Aldehyde C=0 Stretching Vibrations Aldehydic C-H Vibrations Other Aldehyde Bands Carboxylic Acids, -COOH Carboxylic Acid О-H Stretching Vibrations Carboxylic Acid C=0 Stretching Vibrations Other Vibrations of Carboxylic Acids Carboxylic Acid Salts Carboxylic Acid Anhydrides, -CO-O-COCarboxylic Acid Halides, -CO-X Diacyl Peroxides, R-CO-O-O-CO-R, (Acid Peroxides), and Peroxy Acids, -CO-OO-H Esters, -CO-О-, Carbonates, -0-C0-0-, and Haloformates, -0-CO-X Ester C=0 Stretching Vibrations Ester C-O-C Stretching Vibrations Other Ester Bands Lactones, )c֊(cQ -CO 122 122 122 123 125 125 125 125 129 130 130
130 132 132 133 134 142 108 108 108 Imine Hydrohalides, ^C=NH+— Amine Hydrohalide N-H+ Stretching Vibrations Amine Hydrohalide N-H+ Deformation Vibrations Amine and Imine Hydrohalides: Other Bands References 10 108 109 113 113 Amides, —CO—N Amide N-H Stretching Vibrations Amide C=0 Stretching Vibrations: Amide I Band Amide N-H Deformation and C-N Stretching Vibrations: Amide II Band Other Amide Bands Hydroxamic Acids, -CO-NHOH Hydrazides, -CO֊NH-NH2 and -CO-NH-NH-CO- 143 143 143 144 145 145 148
vii Contents Lactams _ХЦ/р Згг։ (Cyclic Amides) Overtone and Combination Bands C=C and C=N Stretching Vibrations Ring C-H Deformation Vibrations Other Bands Pyridine JV-Oxides Other Comments 149 Imides, -CO-NH-COUreas, ^N—CO—(Carbamides) 149 151 Urethanes, 4N—CO—O— (Carbamates) 154 References 154 Quinolines, and Isoquinolines, 168 168 169 169 169 169 173 N 11 Aromatic Compounds Aromatic C-H Stretching Vibrations Aromatic In-plane C-H Deformation Vibrations Aromatic Out-of-plane C-H Deformation Vibrations and Ring Out-of-plane Vibrations in the Region 900-650 cm՜1 Aromatic C=C Stretching Vibrations Overtone and Combination Bands Aromatic Ring Deformation Below 700 cm՜1 Polynuclear Aromatic Compounds Naphthalenes, Anthracenes, Pyrimidines, 157 158 159 159 173 173 160 161 161 165 176 165 and Phenanthrenes, 177 NH2 165 Melamines, References 167 Six-membered Ring Heterocyclic Compounds 168 Pyridine Derivatives, 168 13 12 173 N 168 N^ N 179 Λ X H2N N NH2 References 179 Five-membered Ring Heterocyclic Compounds 181 Pyrroles, N Aromatic C-H Stretching Vibrations ■Լ Ծ Ծ and Indoles, N Pyrrolines, N Չ 181 181
Contents Vlil Furans, 0 JJ 181 О |Լ j 183 Imidazoles, [[ j) N Pyrazoles, Il iL 187 Thiophenes, 189 189 Organic Nitrogen Compounds Nitro Compounds, -NO2 Nitroso Compounds, -N=0, (and Oximes, ^C=N֊OH) 191 191 193 Covalent Nitrates, -ONO2 Nitrites, -0-N=0 References 195 195 197 Organic Halogen Compounds Organic Halogen Compounds, -^C—X (where X=F, 198 Cl, Br, I) Organic Fluorine Compounds Organic Chlorine Compounds Organic Bromine Compounds Organic Iodine Compounds Aromatic Halogen Compounds References Sulphur and Selenium Compounds Mercaptans, -SH C-S and S-S Vibrations: Organic Sulphides, ^s Mercaptans, -SH, Disulphides, -Տ-Տ֊, and Polysulphides, -(-S-S-),,Compounds containing S=0: Organic Sulphoxides, ^Տ=0 and Sulphites, -0-Տ0-0- 201 Sulphonyl Halides, ՏՕշ-X 216 Covalent Sulphonates, R-S02-0R Organic Sulphates, ֊Օ-ՏՕշ-ՕSulphonic Acids, -SO3H, and Salts, ЅОз~М+ Thiocarbonyl Compounds, ^C=S 218 219 220 222 Reviews Organic Selenium Compounds 224 224 Selenoamides, / N—CSe— 224 The Se=0 Stretching Vibration The P=Se Stretching Vibration References 227 227 227 17 Organic Phosphorus Compounds P-H and P-C Vibrations P-OH and P-0 Vibrations P-O-C Vibrations P=0 Vibrations Other Bands References 229 229 229 229 229 240 240 18 Organic Silicon Compounds Si-H Vibrations Methyl-Silicon Compounds, S1-CH3 Ethyl-Silicon Compounds Alkyl-Silicon Compounds Aryl-Silicon Compounds Si-0 Vibrations Silicon-Nitrogen Compounds Silicon-Halide Compounds Hydroxyl-Silicon Compounds References 241 241 241 241 241 241 246 246 246 246 246 19 Boron Compounds References 247 253 198 198 198 215
Sulphonamides, —ՏՕշ-216 N References Organic Sulphones, /ՏՕշ 205 207 207 209 209 209 211
__ ______ Contents 20 21 The Near Infrared Region Carbon-Hydrogen Groups Oxygen-Hydrogen Groups Carbonyl Groups Nitrogen-Hydrogen Groups Polymers Biological, Medical, and Food Applications References Polymers - Macromolecules Introduction Pretreatment of Samples Sample Preparation Basic Techniques - Liquid, Solution, Dispersion Dispersive Techniques Films, Solvent Cast, Hot Press, Microtome Attenuated Total Reflection, Multiple Internal Reflection and Other Reflection Techniques Pyrolysis, Microscope, etc. Other Techniques Theoretical Aspects - Simplified Explanations General Introduction Crystalline Polymers Non-crystalline Polymers Band Intensities Applications - Some Examples Introduction Stereoregularity, Configurations and Conformations Morphology ֊ Lamellae and Spherulites C=C Stretching Band Thermal and Photochemical Degradation Polyethylene and Polypropylene Polystyrenes Polyvinylchloride, Polyvinylidenechloride, Polyvinylfluoride, and Polytetrafluoroethylene Polyesters, Polyvinylacetate Polyamides and Polyimides Polyvinyl Alcohol Polycarbonates Polyethers Polyetherketone and Polyetheretherketone Polyethersulphone and Polyetherethersulphone 254 254 255 255 255 257 257 258 259 259 261 262 262 262 262 263 263 263 263 263 264 265 265 266 266 267 267 267 268 268 269 269 270 270 271 271 271 271 271 Polyconjugated Molecules Resins Coatings and Alkyd Resins Elastomers Plasticisers Strongest Band(s) in the Infrared Spectrum Strongest bands near 2940 cm՜1 (~3.40pm) and 1475 cm՜1 (~6.78pm) Strongest band near 1000cm՜1 (~10.00pm) Strongest band near 1100 cm՜1 (~9.09pm)
Strongest band in the region 835-715 cm՜ (11.98-13.99 pm) Characteristic Absorption Patterns of Functional Groups Present in Plasticisers Carbonyl groups Carboxylic acids Carboxylic acid salts Ort/io-Phthalates Aliphatic esters Aromatic esters Sulphonamides, sulphates and sulphonates Sulphonic acid esters Characteristic Bands of Other Commonly Found Substances Common Inorganic Additives and Fillers Carbonates Sulphates Talc Clays Titanium Dioxide Silica Antimony Trioxide Infrared Flowcharts References 22 Inorganic Compounds and Coordination Complexes Ions Coordination Complexes Isotopic Substitution Coordination of Free Ions having Tetrahedral Symmetry Coordination of Free Ions having Trigonal-Planar ix 272 272 273 273 273 273 274 274 274 274 274 274 274 274 274 275 276 276 276 276 276 276 277 277 277 278 278 278 278 281 283 284 292 299 299 299
Contents x Symmetry Coordination of Free Ions having Pyramidal Structure Coordinate Bond Vibration Modes Structural Isomerism Cis-trans isomerism Lattice Water and Aquo Complexes Metal-Alkyl compounds Metal Halides Metal-jr-Bond and Metal-a-Bond Complexes - Alkenes, Alkynes, etc. Alkenes Alkynes Cyclopentadienes Metal-Cyano and Nitrile Complexes Ammine, Amido, Urea and Related Complexes Metal Carbonyl Compounds Metal-Acetylacetonato Compounds, Carboxylate Complexes and Complexes Involving the Carbonyl Group Carboxylate Complexes and other Complexes Involving Carbonyl Groups Nitro- (-NO?) and Nitrito- (-ONO) Complexes Thiocyanato- (-SCN) and Isothiocyonato- (-NCS) Complexes Isocyanates, M-NCO Nitrosyl Complexes Azides, M-N3, Dinitrogen and Dioxygen Complexes and Nitrogen Bonds Hydrides Metal Oxides and Sulphides Glasses Carbon Clusters References 23 300 300 301 301 301 302 303 304 304 307 308 309 309 314 317 317 320 320 320 320 321 321 323 325 327 327 Biological Molecules - Macromolecules Introduction Sample Preparation Carbohydrates Cellulose and its Derivatives Amino Acids Free Amino Acid -NH3+ Vibrations Free Amino Acid Carboxyl Bands Amino Acid Hydrohalides Amino Acid Salts Nucleic Acids 328 328 328 328 329 329 332 332 332 332 333 Amido Acids, 333 CO---- COOH Proteins and Peptides Lipids Bacteria Food, Cells and Tissues References Appendix Index Further Reading 333 335 338 339 340 341 343
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| language | English |
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| spellingShingle | Socrates, George Infrared and Raman characteristic group frequencies tables and charts Infrarotspektroskopie (DE-588)4135411-4 gnd Raman-Spektroskopie (DE-588)4176916-8 gnd |
| subject_GND | (DE-588)4135411-4 (DE-588)4176916-8 |
| title | Infrared and Raman characteristic group frequencies tables and charts |
| title_auth | Infrared and Raman characteristic group frequencies tables and charts |
| title_exact_search | Infrared and Raman characteristic group frequencies tables and charts |
| title_full | Infrared and Raman characteristic group frequencies tables and charts George Socrates |
| title_fullStr | Infrared and Raman characteristic group frequencies tables and charts George Socrates |
| title_full_unstemmed | Infrared and Raman characteristic group frequencies tables and charts George Socrates |
| title_short | Infrared and Raman characteristic group frequencies |
| title_sort | infrared and raman characteristic group frequencies tables and charts |
| title_sub | tables and charts |
| topic | Infrarotspektroskopie (DE-588)4135411-4 gnd Raman-Spektroskopie (DE-588)4176916-8 gnd |
| topic_facet | Infrarotspektroskopie Raman-Spektroskopie |
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Inhaltsverzeichnis
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