Thermal analysis of polymers: fundamentals and applications
Saved in:
| Format: | Book |
|---|---|
| Language: | English |
| Published: |
Hoboken, NJ
Wiley
2009
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis Klappentext |
| Physical Description: | X, 688 S. Ill., graph. Darst. |
| ISBN: | 9780471769170 |
Staff View
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| adam_text | CONTENTS
PREFACE
ix
1
INTRODUCTION
1
Joseph
D.
Menczel,
R.
Bruce Prime and Patrick K. Gallagher
2
DIFFERENTIAL SCANNING CALORIMETRY (DSC)
7
Joseph D. Menczel, Lawrence
Judovits,
R.
Bruce Prime,
Harvey E. Bair, Mike Reading, and Steven Swier
2.1.
Introduction
/ 7
2.2.
Elements of Thermodynamics in DSC
/ 9
2.3.
The Basics of DifferentialScanning Calorimetry
/ 18
2.4.
Purity Determination of Low-Molecular-Mass Compounds by
DSC
/ 37
2.5.
Calibration of Differential Scanning Calorimeters
/ 41
2.6.
Measurement of Heat Capacity
/ 52
2.7.
Phase Transitions in Amorphous and Crystalline Polymers
/ 58
2.8.
Fibers
/ 115
2.9.
Films
/ 123
2.10.
Thermosets
/ 130
2.11.
Differential Photocalorimetry (DPC)
/ 154
2.12.
Fast-Scan DSC
/ 162
2.13.
Modulated Temperature Differential Scanning Calorimetry
(MTDSC)
/ 168
2.14.
How to Perform DSC Measurements
/ 208
2.15.
Instrumentation
/ 217
Appendix
/ 225
Abbreviations
/ 225
References
/ 229
Learn how to take full advantage of a
broad range of thermal analysis techniq
Thermal Analysis of Polymers: Fundamentals and Applications emphasizes the practical uses of
thermal analysis, enabling readers to take full advantage of its capabilities as a polymer character¬
ization tool in their laboratories. The book offers essential theoretical background; however, it fo¬
cuses on how to perform a broad range of thermal analysis measurements and tests, with detailed
coverage of methods, applications, instrumentation, and calibration. Moreover, it helps readers
correctly interpret their results.
This book features a team of authors whose expertise spans all the thermal analysis techniques and
applications covered in the book. Their advice is based not only on thorough knowledge of the litera¬
ture, but also their own hands-on experience working in the lab. Among the topics covered are:
Differential scanning calorimetry
Thermogravimetric analysis
Thermomechanical analysis and thermodilatometry
Dynamic mechanical analysis
Dielectric analysis
Micro- and
nano-scale
local thermal analysis
Each chapter guides readers through the applications of thermal analysis for polymer char¬
acterization, with detailed examples that show how to perform each step. References guide
readers to the primary literature for further investigation into each topic.
Following this book s step-by-step guidance, chemists and engineers new to thermal analysis techniques,
whether in industry, government or
academia,
can quickly learn to use them to generate high-quality re¬
sults. For more experienced researchers, the book enables them to expand their repertoire to include a
broader range of sophisticated techniques and applications.
JOSEPH D. MENCZEL, PhD, a recognized expert in thermal analysis of polymers with some thir¬
ty years of industrial and academic experience, is Assistant Technical Director at Alcon Labo¬
ratories. He has researched more than
120
polymeric systems in which he studied calibration
of DSCs, glass transition, nucleation, crystallization, melting, stability, mechanical and micro-
mechanical properties of polymers, and polymer-water interactions. Dr. Menczel holds six pat¬
ents and is the author of seventy scholarly papers. He is the author of two chapters in the book
Thermal Characterization of Polymeric Materials. In conducting DSC experiments, Dr. Menczel
found a crystal/amorphous interface in semicrystalline polymers, which later became known as the
rigid amorphous phase. He is also credited with developing the temperature calibration of DSCs for
cooling experiments.
R. BRUCE PRIME, PhD, is a consultant to industry and government and a recognized authority on the
cure and properties of cross-linked polymer systems. During his thirty-year career with IBM, he led
teams responsible for developing and implementing polymer applications for printer and informa¬
tion storage technologies. He holds four patents and is the author of more than fifty technical pa¬
pers and the chapter on
thermosets
in Thermal Characterization of Polymeric Materials. Dr. Prime
is a Fellow of
SPE
and
NATAS
and was the
1989
recipient of the Mettler-Toledo Award in Thermal
Analysis. He maintains the Web site www.primethermosets.com.
|
| adam_txt |
CONTENTS
PREFACE
ix
1
INTRODUCTION
1
Joseph
D.
Menczel,
R.
Bruce Prime and Patrick K. Gallagher
2
DIFFERENTIAL SCANNING CALORIMETRY (DSC)
7
Joseph D. Menczel, Lawrence
Judovits,
R.
Bruce Prime,
Harvey E. Bair, Mike Reading, and Steven Swier
2.1.
Introduction
/ 7
2.2.
Elements of Thermodynamics in DSC
/ 9
2.3.
The Basics of DifferentialScanning Calorimetry
/ 18
2.4.
Purity Determination of Low-Molecular-Mass Compounds by
DSC
/ 37
2.5.
Calibration of Differential Scanning Calorimeters
/ 41
2.6.
Measurement of Heat Capacity
/ 52
2.7.
Phase Transitions in Amorphous and Crystalline Polymers
/ 58
2.8.
Fibers
/ 115
2.9.
Films
/ 123
2.10.
Thermosets
/ 130
2.11.
Differential Photocalorimetry (DPC)
/ 154
2.12.
Fast-Scan DSC
/ 162
2.13.
Modulated Temperature Differential Scanning Calorimetry
(MTDSC)
/ 168
2.14.
How to Perform DSC Measurements
/ 208
2.15.
Instrumentation
/ 217
Appendix
/ 225
Abbreviations
/ 225
References
/ 229
Learn how to take full advantage of a
broad range of thermal analysis techniq
Thermal Analysis of Polymers: Fundamentals and Applications emphasizes the practical uses of
thermal analysis, enabling readers to take full advantage of its capabilities as a polymer character¬
ization tool in their laboratories. The book offers essential theoretical background; however, it fo¬
cuses on how to perform a broad range of thermal analysis measurements and tests, with detailed
coverage of methods, applications, instrumentation, and calibration. Moreover, it helps readers
correctly interpret their results.
This book features a team of authors whose expertise spans all the thermal analysis techniques and
applications covered in the book. Their advice is based not only on thorough knowledge of the litera¬
ture, but also their own hands-on experience working in the lab. Among the topics covered are:
Differential scanning calorimetry
Thermogravimetric analysis
Thermomechanical analysis and thermodilatometry
Dynamic mechanical analysis
Dielectric analysis
Micro- and
nano-scale
local thermal analysis
Each chapter guides readers through the applications of thermal analysis for polymer char¬
acterization, with detailed examples that show how to perform each step. References guide
readers to the primary literature for further investigation into each topic.
Following this book's step-by-step guidance, chemists and engineers new to thermal analysis techniques,
whether in industry, government or
academia,
can quickly learn to use them to generate high-quality re¬
sults. For more experienced researchers, the book enables them to expand their repertoire to include a
broader range of sophisticated techniques and applications.
JOSEPH D. MENCZEL, PhD, a recognized expert in thermal analysis of polymers with some thir¬
ty years of industrial and academic experience, is Assistant Technical Director at Alcon Labo¬
ratories. He has researched more than
120
polymeric systems in which he studied calibration
of DSCs, glass transition, nucleation, crystallization, melting, stability, mechanical and micro-
mechanical properties of polymers, and polymer-water interactions. Dr. Menczel holds six pat¬
ents and is the author of seventy scholarly papers. He is the author of two chapters in the book
Thermal Characterization of Polymeric Materials. In conducting DSC experiments, Dr. Menczel
found a crystal/amorphous interface in semicrystalline polymers, which later became known as the
rigid amorphous phase. He is also credited with developing the temperature calibration of DSCs for
cooling experiments.
R. BRUCE PRIME, PhD, is a consultant to industry and government and a recognized authority on the
cure and properties of cross-linked polymer systems. During his thirty-year career with IBM, he led
teams responsible for developing and implementing polymer applications for printer and informa¬
tion storage technologies. He holds four patents and is the author of more than fifty technical pa¬
pers and the chapter on
thermosets
in Thermal Characterization of Polymeric Materials. Dr. Prime
is a Fellow of
SPE
and
NATAS
and was the
1989
recipient of the Mettler-Toledo Award in Thermal
Analysis. He maintains the Web site www.primethermosets.com. |
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| title | Thermal analysis of polymers fundamentals and applications |
| title_auth | Thermal analysis of polymers fundamentals and applications |
| title_exact_search | Thermal analysis of polymers fundamentals and applications |
| title_exact_search_txtP | Thermal analysis of polymers fundamentals and applications |
| title_full | Thermal analysis of polymers fundamentals and applications ed. by Joseph D. Menczel ... |
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| title_short | Thermal analysis of polymers |
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| title_sub | fundamentals and applications |
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