Handbook of RAFT polymerization:
Gespeichert in:
| Weitere Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Weinheim
WILEY-VCH
2008
|
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | XI, 543 S. Ill., graph. Darst. 240 mm x 170 mm |
| ISBN: | 9783527319244 3527319247 |
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| 245 | 1 | 0 | |a Handbook of RAFT polymerization |c ed. by Christopher Barner-Kowollik |
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Contents
List of Contributors ix
1 Introduction 1
Christopher Barner-Kowollik
2 Quantum-Chemical Studies of RAFT Polymerization: Methodology,
Structure-Reactivity Correlations and Kinetic Implications 5
Michelle L Coote, Elizabeth H. Krenske, Ekaterina I. Izgorodina
2.1 Introduction 5
2.2 Methodology 7
2.3 Computational Modeling of RAFT Kinetics 19
2.4 Structure-Reactivity Studies 34
2.5 Abbreviations 45
3 The Mechanism and Kinetics of the RAFT Process: Overview,
Rates, Stabilities, Side Reactions, Product Spectrum and
Outstanding Challenges 51
Graeme Moad, Christopher Barner-Kowollik
3.1 History 52
3.2 Preequilibrium Kinetics and Mechanism 59
3.3 Main Equilibrium Kinetics and Mechanism 83
3.4 Mechanisms for Rate Retardation/Inhibition - Outstanding
Questions 90
3.5 RAFT Copolymerization: Block and Statistical Copolymers 91
3.6 The Kinetics and Mechanism of Star and Graft Polymer
Formation Processes 94
3.7 Mechanism and Kinetics as a Guide for the Synthetic
Polymer Chemist 97
4 The RAFT Process as a Kinetic Tool: Accessing Fundamental
Parameters of Free Radical Polymerization 105
Thomasjunkers, Tara M. Lovestead, Christopher Barner-Kowollik
4.1 Introduction 105
4.2 Chain-Length-Dependent Termination: A Brief Overview 107
4.3 RAFT Chemistry as a Tool for Elucidating the Chain Length
Dependence of fct 109
4.4 Chain-Length-Dependent Propagation Rate Coefficients 144
5 The Radical Chemistry ofThiocarbonylthio Compounds: An Overview 151
SamirZ. Zard
5.1 Historical Overview and Early Chemistry 251
5.2 The Barton-McCombie Deoxygenation 153
5.3 A Minor Mechanistic Controversy 154
5.4 A New Degenerative Radical Process 156
5.5 Synthetic Routes to Thiocarbonylthio Derivatives 160
5.6 Some Synthetic Applications of the Degenerative Radical
Transfer to Small Molecules 168
5.7 Applications to Controlled Radical Polymerizations 177
5.8 Concluding Remarks 185
6 RAFT Polymerization in Bulk Monomer or in (Organic) Solution 189
Ezio Rizzardo, Graeme Moad, San H. Thang
6.1 Introduction 189
6.2 RAFT Agents 192
6.3 RAFT Polymerization 205
6.4 RAFT Polymerization Conditions 222
6.5 Abbreviations 225
7 RAFT Polymerization in Homogeneous Aqueous Media: Initiation Systems,
RAFT Agent Stability, Monomers and Polymer Structures 235
Andrew B. Lowe, Charles L McCormick
7.1 Introduction 235
7.2 Initiation Systems 236
7.3 RAFT Agent Stability 241
7.4 Suitable Monomers 248
7.5 Examples of Experimental Procedures 276
8 RAFT-Mediated Polymerization in Heterogeneous Systems 285
Carl N. Urbani, MichaelJ. Monteiro
8.1 Introduction 285
8.2 Effect of Ctr, raft on Mn and PDI in Homogeneous Systems 292
8.3 Raft in Heterogeneous Systems 293
8.4 Conclusion 321
9 Complex Architecture Design via the RAFT Process: Scope,
Strengths and Limitations 315
Martina H. Stenzel
9.1 Complex Polymer Architectures 315
9.2 Block Copolymers 325
9.3 Star Polymers via RAFT Polymerization 343
9.4 Comb Polymers 359
9.5 Other Complex Architectures 364
9.6 Conclusions 367
10 Macromolecular Design by Interchange of Xanthates: Background, Design,
Scope and Applications 373
Daniel Taton, Mathias Destarac, Samir Z. Zard
10.1 Introduction 373
10.2 History of MADIX Polymerization 374
10.3 Mechanism of MADIX Polymerization 379
10.4 Kinetics of MADIX Polymerization 383
10.5 Choice of MADIX Agents 387
10.6 Synthesis of MADIX Agents 390
10.7 Experimental Conditions in MADIX 391
10.8 Monomers Polymerizable by MADIX 393
10.9 MADIX Polymerization in Waterborne Dispersed Media 399
10.10 Macromolecular Engineering by MADIX 403
10.11 Methodologies to Remove the Dithiocarbonate End Groups 412
10.12 Applications of MADIX (co)polymers 414
11 Surface and Particle Modification via the RAFT Process: Approach and
Properties 423
Yu Li, Linda S. Schadler, Brian C. Benicewicz
11.1 Introduction 423
11.2 Approach 424
11.3 Properties 444
11.4 Conclusions 449
11.5 Abbreviations 450
11.6 Acknowledgment 451
12 Polymers with Weil-Defined EndCroupsvia RAFT-Synthesis, Applications
and Postmodifications 455
Leonie Barner, Sebastien Perrier
12.1 Introduction 455
12.2 Terminal Functionalities Introduced via the CTA 456
12.3 RAFT in Combination with Other Polymerization Techniques 467
12.4 Stability of the Thiocarbonylthio End Group and
Its Modification Postpolymerization 471
12.5 Conclusion 478
12.6 Abbreviations 478
13 Toward New Materials Prepared via the RAFT Process: From Drug Delivery
to Optoelectronics? 483
Arnaud Favier, Bertrand de Lambert, Marie-Therese Charreyre
13.1 Introduction 483
13.2 Bio-Related Applications 485
13.3 Polymer-Based Materials for Various Applications 508
13.4 Conclusions 526
Subject Index 537 |
| adam_txt |
Contents
List of Contributors ix
1 Introduction 1
Christopher Barner-Kowollik
2 Quantum-Chemical Studies of RAFT Polymerization: Methodology,
Structure-Reactivity Correlations and Kinetic Implications 5
Michelle L Coote, Elizabeth H. Krenske, Ekaterina I. Izgorodina
2.1 Introduction 5
2.2 Methodology 7
2.3 Computational Modeling of RAFT Kinetics 19
2.4 Structure-Reactivity Studies 34
2.5 Abbreviations 45
3 The Mechanism and Kinetics of the RAFT Process: Overview,
Rates, Stabilities, Side Reactions, Product Spectrum and
Outstanding Challenges 51
Graeme Moad, Christopher Barner-Kowollik
3.1 History 52
3.2 Preequilibrium Kinetics and Mechanism 59
3.3 Main Equilibrium Kinetics and Mechanism 83
3.4 Mechanisms for Rate Retardation/Inhibition - Outstanding
Questions 90
3.5 RAFT Copolymerization: Block and Statistical Copolymers 91
3.6 The Kinetics and Mechanism of Star and Graft Polymer
Formation Processes 94
3.7 Mechanism and Kinetics as a Guide for the Synthetic
Polymer Chemist 97
4 The RAFT Process as a Kinetic Tool: Accessing Fundamental
Parameters of Free Radical Polymerization 105
Thomasjunkers, Tara M. Lovestead, Christopher Barner-Kowollik
4.1 Introduction 105
4.2 Chain-Length-Dependent Termination: A Brief Overview 107
4.3 RAFT Chemistry as a Tool for Elucidating the Chain Length
Dependence of fct 109
4.4 Chain-Length-Dependent Propagation Rate Coefficients 144
5 The Radical Chemistry ofThiocarbonylthio Compounds: An Overview 151
SamirZ. Zard
5.1 Historical Overview and Early Chemistry 251
5.2 The Barton-McCombie Deoxygenation 153
5.3 A Minor Mechanistic Controversy 154
5.4 A New Degenerative Radical Process 156
5.5 Synthetic Routes to Thiocarbonylthio Derivatives 160
5.6 Some Synthetic Applications of the Degenerative Radical
Transfer to Small Molecules 168
5.7 Applications to Controlled Radical Polymerizations 177
5.8 Concluding Remarks 185
6 RAFT Polymerization in Bulk Monomer or in (Organic) Solution 189
Ezio Rizzardo, Graeme Moad, San H. Thang
6.1 Introduction 189
6.2 RAFT Agents 192
6.3 RAFT Polymerization 205
6.4 RAFT Polymerization Conditions 222
6.5 Abbreviations 225
7 RAFT Polymerization in Homogeneous Aqueous Media: Initiation Systems,
RAFT Agent Stability, Monomers and Polymer Structures 235
Andrew B. Lowe, Charles L McCormick
7.1 Introduction 235
7.2 Initiation Systems 236
7.3 RAFT Agent Stability 241
7.4 Suitable Monomers 248
7.5 Examples of Experimental Procedures 276
8 RAFT-Mediated Polymerization in Heterogeneous Systems 285
Carl N. Urbani, MichaelJ. Monteiro
8.1 Introduction 285
8.2 Effect of Ctr, raft on Mn and PDI in Homogeneous Systems 292
8.3 Raft in Heterogeneous Systems 293
8.4 Conclusion 321
9 Complex Architecture Design via the RAFT Process: Scope,
Strengths and Limitations 315
Martina H. Stenzel
9.1 Complex Polymer Architectures 315
9.2 Block Copolymers 325
9.3 Star Polymers via RAFT Polymerization 343
9.4 Comb Polymers 359
9.5 Other Complex Architectures 364
9.6 Conclusions 367
10 Macromolecular Design by Interchange of Xanthates: Background, Design,
Scope and Applications 373
Daniel Taton, Mathias Destarac, Samir Z. Zard
10.1 Introduction 373
10.2 History of MADIX Polymerization 374
10.3 Mechanism of MADIX Polymerization 379
10.4 Kinetics of MADIX Polymerization 383
10.5 Choice of MADIX Agents 387
10.6 Synthesis of MADIX Agents 390
10.7 Experimental Conditions in MADIX 391
10.8 Monomers Polymerizable by MADIX 393
10.9 MADIX Polymerization in Waterborne Dispersed Media 399
10.10 Macromolecular Engineering by MADIX 403
10.11 Methodologies to Remove the Dithiocarbonate End Groups 412
10.12 Applications of MADIX (co)polymers 414
11 Surface and Particle Modification via the RAFT Process: Approach and
Properties 423
Yu Li, Linda S. Schadler, Brian C. Benicewicz
11.1 Introduction 423
11.2 Approach 424
11.3 Properties 444
11.4 Conclusions 449
11.5 Abbreviations 450
11.6 Acknowledgment 451
12 Polymers with Weil-Defined EndCroupsvia RAFT-Synthesis, Applications
and Postmodifications 455
Leonie Barner, Sebastien Perrier
12.1 Introduction 455
12.2 Terminal Functionalities Introduced via the CTA 456
12.3 RAFT in Combination with Other Polymerization Techniques 467
12.4 Stability of the Thiocarbonylthio End Group and
Its Modification Postpolymerization 471
12.5 Conclusion 478
12.6 Abbreviations 478
13 Toward New Materials Prepared via the RAFT Process: From Drug Delivery
to Optoelectronics? 483
Arnaud Favier, Bertrand de Lambert, Marie-Therese Charreyre
13.1 Introduction 483
13.2 Bio-Related Applications 485
13.3 Polymer-Based Materials for Various Applications 508
13.4 Conclusions 526
Subject Index 537 |
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| isbn | 9783527319244 3527319247 |
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| spelling | Handbook of RAFT polymerization ed. by Christopher Barner-Kowollik Weinheim WILEY-VCH 2008 XI, 543 S. Ill., graph. Darst. 240 mm x 170 mm txt rdacontent n rdamedia nc rdacarrier Addition polymerization RAFT Polymerisation (DE-588)7626327-7 gnd rswk-swf RAFT Polymerisation (DE-588)7626327-7 s DE-604 Barner-Kowollik, Christopher 1973- (DE-588)121637514 edt text/html http://deposit.dnb.de/cgi-bin/dokserv?id=2973617&prov=M&dok_var=1&dok_ext=htm Inhaltstext HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016500827&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Handbook of RAFT polymerization Addition polymerization RAFT Polymerisation (DE-588)7626327-7 gnd |
| subject_GND | (DE-588)7626327-7 |
| title | Handbook of RAFT polymerization |
| title_auth | Handbook of RAFT polymerization |
| title_exact_search | Handbook of RAFT polymerization |
| title_exact_search_txtP | Handbook of RAFT polymerization |
| title_full | Handbook of RAFT polymerization ed. by Christopher Barner-Kowollik |
| title_fullStr | Handbook of RAFT polymerization ed. by Christopher Barner-Kowollik |
| title_full_unstemmed | Handbook of RAFT polymerization ed. by Christopher Barner-Kowollik |
| title_short | Handbook of RAFT polymerization |
| title_sort | handbook of raft polymerization |
| topic | Addition polymerization RAFT Polymerisation (DE-588)7626327-7 gnd |
| topic_facet | Addition polymerization RAFT Polymerisation |
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