Lipidomics and bioactive lipids: Specialized analytical methods and lipids in disease:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Amsterdam [u.a.]
Elsevier, Acad. Press
2007
|
| Schriftenreihe: | Methods in enzymology
433 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XLII, 249 S. Ill., graph. Darst. |
| ISBN: | 9780123739667 0123739667 |
Internformat
MARC
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| 245 | 1 | 0 | |a Lipidomics and bioactive lipids: Specialized analytical methods and lipids in disease |c ed. by H. Alex Brown |
| 264 | 1 | |a Amsterdam [u.a.] |b Elsevier, Acad. Press |c 2007 | |
| 300 | |a XLII, 249 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Methods in enzymology |v 433 | |
| 650 | 4 | |a Lipids |x Analysis | |
| 650 | 4 | |a Lipids |x Spectra | |
| 650 | 4 | |a Lipids |x analysis | |
| 650 | 4 | |a Mass Spectrometry |x methods | |
| 650 | 4 | |a Mass spectrometry | |
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| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-016168966 | |
Datensatz im Suchindex
| _version_ | 1807322158071808000 |
|---|---|
| adam_text |
Contents
Contributors
xi
Preface
xv
Volumes in Series
xvii
1.
Liquid Chromatography Mass Spectrometry for Quantifying Plasma
Lysophospholipids: Potential Biomarkers for Cancer Diagnosis
ι
Mandi Murph,
Tamotsu Tanaka, Jihai Pang, Edward Felix, Shuying Liu,
Rosanne Trost,
Andrew K. Godwin, Robert Newman, and Gordon Mills
ι.
Introduction
2
2.
Procedure
6
3.
Liquid Chromatography/Mass Spectrometry/Mass Spectrometry
7
4.
Discussion
9
5.
Challenges to the Development of a Clinically Applicable
Screening Assay
19
Acknowledgments
21
References
21
г.
Measurement of Eicosanoids in Cancer Tissues
27
Dingzhi Wang and Raymond
N.
DuBois
1.
Introduction
28
2.
Quantitative Measurement of Eicosanoids
32
3.
Preparation of Samples
33
4.
Eicosanoids Extraction
35
5. Chromatographie
Separation of Eicosanoids
36
6.
Quantitative Analysis of Eicosanoids
39
Acknowledgments
45
References
45
3.
Noninvasive Assessment of the Role of Cyclooxygenases in
Cardiovascular Health: A Detailed HPLC/MS/MS Method
51
Wen-Liang Song, John A. Lawson,
Miao
Wang, Helen
Zou,
and Garret A. FitzGerald
1.
Introduction
52
2.
Background and History
53
vi
Contents
3.
Principles of Eicosanoid Analysis by Mass Spectrometry
54
4.
Urinary Markers of Systemic Eicosanoid Synthesis
63
5.
Date Analysis and Interpretation
69
6.
Concluding Remarks
69
References
71
4.
Lipidomics in Diabetes and the Metabolic Syndrome
73
Richard W. Gross and Xianlin Han
1.
Introduction
74
2.
Brief introduction of Multi-Dimensional MS-Based Shotgun Lipidomics
74
3.
Profiling
Human Plasma Triacylglycerol Molecular Species
77
4.
Analysis of Human Heart Lipidome
82
5.
High Mass Resolution-Based Shotgun Lipidomics for the Analysis of
Cardiolipin Molecular Species
86
Acknowledgment
88
References
89
5.
LC-MS-MS Analysis of Neutral Eicosanoids
91
Philip
).
Kingsley and Lawrence J. Marnett
1.
Introduction
92
2.
Purification of Analytes from Cell Culture Medium and Tissue
95
3.
Quantitation
103
4.
Linearity and Sensitivity
108
5.
Postmortem Changes in Analytes
109
6.
Summary
109
Acknowledgments
110
References
110
6.
Quantification of Fa-lsoprostanes in Biological Fluids and Tissues
as a Measure of
Oxidant
Stress
113
Ginger L. Milne, Huiyong Yin, Joshua D. Brooks, Stephanie Sanchez,
L. Jackson Roberts, II, and Jason D. Marrow
1.
Introduction
114
2.
Handling and Storage of Biological Fluids and Tissues for
Quantification of FHsoPs
115
3.
Extraction and Hydrolysis of F^lsoP-Containing Phospholipids in
Tissues and Biological Fluids u6
4.
Purification, Derivatization, and Quantification of Free F^lsoPs
117
5.
Application of the Assay to Quantify F^lsoPs in Biological
Tissues and Fluids Ug
Contents
vii
6. Alternative
Methods for Measuring F^IsoPs
121
7.
Fj-lsoprostanes as an Index of
Oxidant
Stress In Vivo
122
8.
Summary
123
Acknowledgments
124
References
124
7.
Measurement of Products of Docosahexaenoic Acid
Peroxidation,
Neuroprostanes, and Neurofurans
127
Kyle
0.
Arneson and
L
Jackson Roberts, II
1.
Introduction
128
2.
Handling and Storage of Biological Fluids and Tissues for
Quantification of F4-Neuroprostanes
132
3.
Extraction and Hydrolysis of F^-Neuroprostane-Containing
Phospholipids in Tissues and Biological Fluids
132
4.
Purification, Derivatization, and Quantification of
F4-Neuroprostanes
135
5.
Summary
141
Acknowledgments
141
References
141
8.
Enantiomeric Separation of Hydroxy and Hydroperoxy Eicosanoids
by Chiral Column Chromatography
145
Claus
Schneider, Zheyong Yu, William E. Boeglin, Yuxiang Zheng,
and Alan R. Brash
1.
Introduction
146
2.
Chiral Columns, Solvents, and Standards
147
3.
Chiral Analyses
151
4.
Application of Chiral Columns for Separation of Diastereomers
155
Acknowledgments
156
References
156
9.
Targeted Chiral Lipidomics Analysis by Liquid Chromatography
Electron Capture Atmospheric Pressure Chemical lonization
Mass Spectrometry (LC-ECAPCI/MS)
159
Seon Hwa Lee and Ian A. Blair
1.
Introduction
160
2.
Electron-Capture Atmospheric-Pressure Chemical lonization
161
3.
Dissociative Electron Capture
162
4.
Derivatization for LC-ECAPCI/MS
163
5.
Procedure
164
6.
Summary
171
Acknowledgments
172
References
172
viii Contents
10.
Shotgun Lipidomics by
Tandem
Mass Spectrometry
under
Data-Dependent Acquisition Control
175
Dominik Schwudke,
Gerhard
Liebisch, Ronny Herzog, Gerd Schmitz, and
Andrej Shevchenko
1.
Introduction
176
2.
Procedure
177
3. Automated Interpretation
of MS/MS Spectra Acquired
in DDA Experiments
181
4.
Boolean Scans: A Novel Scan Type Enabled by
Postacquisition
Data Processing
183
5.
Comprehensive Characterization of Total
Lipid
Extracts by
DDA-Driven Profiling
185
6.
Selected Reaction Monitoring in Quantification of Cholesterol and
Chotesteryl Esters
188
Acknowledgments
189
References
190
11.
Identification of Intact
Lipid
Peroxides by Ag+ Coordination
Ion-Spray Mass Spectrometry (CIS-MS)
193
Huiyong Yin and Ned A. Porter
1.
Introduction
194
2.
Analysis of
Lipid
Oxidation Products
196
3.
Ag+ Coordination Ion-Spray MS
196
4.
Identification of
Lipid
Oxidation Products of Cholestrol Esters by
LC^ CIS-MS
198
5.
Identification
of Intact
Lipid
Peroxides from Phospholipids
by Ag+ CIS-MS
204
6.
Precautions of Applying Ag+ CIS-MS to Study Lipids
207
7.
Conclusions
208
Acknowledgments
209
References
209
12.
Quantification of Cardiolipin by Liquid
Chromatography-Electrospray lonization Mass Spectrometry
213
Teresa A. Garrett,
Reza
Kordestani, and Christian R. H. Raetz
1.
Introduction
214
2.
Complexity of Cardiolipin Structure
217
3.
Analysis of Synthetic Cardiolipin Standards Using Liquid
Chromatography-Mass Spectrometry 2a8
Contents ix
4. Liquid Chromatography-Mass Spectrometry
of
Cardiolipins in
Total Lipid
Extracts
221
5.
Quantification of
Cardiolipin
226
Acknowledgments
228
References
228
Author Index
231
Subject Index
245 |
| adam_txt |
Contents
Contributors
xi
Preface
xv
Volumes in Series
xvii
1.
Liquid Chromatography Mass Spectrometry for Quantifying Plasma
Lysophospholipids: Potential Biomarkers for Cancer Diagnosis
ι
Mandi Murph,
Tamotsu Tanaka, Jihai Pang, Edward Felix, Shuying Liu,
Rosanne Trost,
Andrew K. Godwin, Robert Newman, and Gordon Mills
ι.
Introduction
2
2.
Procedure
6
3.
Liquid Chromatography/Mass Spectrometry/Mass Spectrometry
7
4.
Discussion
9
5.
Challenges to the Development of a Clinically Applicable
Screening Assay
19
Acknowledgments
21
References
21
г.
Measurement of Eicosanoids in Cancer Tissues
27
Dingzhi Wang and Raymond
N.
DuBois
1.
Introduction
28
2.
Quantitative Measurement of Eicosanoids
32
3.
Preparation of Samples
33
4.
Eicosanoids Extraction
35
5. Chromatographie
Separation of Eicosanoids
36
6.
Quantitative Analysis of Eicosanoids
39
Acknowledgments
45
References
45
3.
Noninvasive Assessment of the Role of Cyclooxygenases in
Cardiovascular Health: A Detailed HPLC/MS/MS Method
51
Wen-Liang Song, John A. Lawson,
Miao
Wang, Helen
Zou,
and Garret A. FitzGerald
1.
Introduction
52
2.
Background and History
53
vi
Contents
3.
Principles of Eicosanoid Analysis by Mass Spectrometry
54
4.
Urinary Markers of Systemic Eicosanoid Synthesis
63
5.
Date Analysis and Interpretation
69
6.
Concluding Remarks
69
References
71
4.
Lipidomics in Diabetes and the Metabolic Syndrome
73
Richard W. Gross and Xianlin Han
1.
Introduction
74
2.
Brief introduction of Multi-Dimensional MS-Based Shotgun Lipidomics
74
3.
Profiling
Human Plasma Triacylglycerol Molecular Species
77
4.
Analysis of Human Heart Lipidome
82
5.
High Mass Resolution-Based Shotgun Lipidomics for the Analysis of
Cardiolipin Molecular Species
86
Acknowledgment
88
References
89
5.
LC-MS-MS Analysis of Neutral Eicosanoids
91
Philip
).
Kingsley and Lawrence J. Marnett
1.
Introduction
92
2.
Purification of Analytes from Cell Culture Medium and Tissue
95
3.
Quantitation
103
4.
Linearity and Sensitivity
108
5.
Postmortem Changes in Analytes
109
6.
Summary
109
Acknowledgments
110
References
110
6.
Quantification of Fa-lsoprostanes in Biological Fluids and Tissues
as a Measure of
Oxidant
Stress
113
Ginger L. Milne, Huiyong Yin, Joshua D. Brooks, Stephanie Sanchez,
L. Jackson Roberts, II, and Jason D. Marrow
1.
Introduction
114
2.
Handling and Storage of Biological Fluids and Tissues for
Quantification of FHsoPs
115
3.
Extraction and Hydrolysis of F^lsoP-Containing Phospholipids in
Tissues and Biological Fluids u6
4.
Purification, Derivatization, and Quantification of Free F^lsoPs
117
5.
Application of the Assay to Quantify F^lsoPs in Biological
Tissues and Fluids Ug
Contents
vii
6. Alternative
Methods for Measuring F^IsoPs
121
7.
Fj-lsoprostanes as an Index of
Oxidant
Stress In Vivo
122
8.
Summary
123
Acknowledgments
124
References
124
7.
Measurement of Products of Docosahexaenoic Acid
Peroxidation,
Neuroprostanes, and Neurofurans
127
Kyle
0.
Arneson and
L
Jackson Roberts, II
1.
Introduction
128
2.
Handling and Storage of Biological Fluids and Tissues for
Quantification of F4-Neuroprostanes
132
3.
Extraction and Hydrolysis of F^-Neuroprostane-Containing
Phospholipids in Tissues and Biological Fluids
132
4.
Purification, Derivatization, and Quantification of
F4-Neuroprostanes
135
5.
Summary
141
Acknowledgments
141
References
141
8.
Enantiomeric Separation of Hydroxy and Hydroperoxy Eicosanoids
by Chiral Column Chromatography
145
Claus
Schneider, Zheyong Yu, William E. Boeglin, Yuxiang Zheng,
and Alan R. Brash
1.
Introduction
146
2.
Chiral Columns, Solvents, and Standards
147
3.
Chiral Analyses
151
4.
Application of Chiral Columns for Separation of Diastereomers
155
Acknowledgments
156
References
156
9.
Targeted Chiral Lipidomics Analysis by Liquid Chromatography
Electron Capture Atmospheric Pressure Chemical lonization
Mass Spectrometry (LC-ECAPCI/MS)
159
Seon Hwa Lee and Ian A. Blair
1.
Introduction
160
2.
Electron-Capture Atmospheric-Pressure Chemical lonization
161
3.
Dissociative Electron Capture
162
4.
Derivatization for LC-ECAPCI/MS
163
5.
Procedure
164
6.
Summary
171
Acknowledgments
172
References
172
viii Contents
10.
Shotgun Lipidomics by
Tandem
Mass Spectrometry
under
Data-Dependent Acquisition Control
175
Dominik Schwudke,
Gerhard
Liebisch, Ronny Herzog, Gerd Schmitz, and
Andrej Shevchenko
1.
Introduction
176
2.
Procedure
177
3. Automated Interpretation
of MS/MS Spectra Acquired
in DDA Experiments
181
4.
Boolean Scans: A Novel Scan Type Enabled by
Postacquisition
Data Processing
183
5.
Comprehensive Characterization of Total
Lipid
Extracts by
DDA-Driven Profiling
185
6.
Selected Reaction Monitoring in Quantification of Cholesterol and
Chotesteryl Esters
188
Acknowledgments
189
References
190
11.
Identification of Intact
Lipid
Peroxides by Ag+ Coordination
Ion-Spray Mass Spectrometry (CIS-MS)
193
Huiyong Yin and Ned A. Porter
1.
Introduction
194
2.
Analysis of
Lipid
Oxidation Products
196
3.
Ag+ Coordination Ion-Spray MS
196
4.
Identification of
Lipid
Oxidation Products of Cholestrol Esters by
LC^ CIS-MS
198
5.
Identification
of Intact
Lipid
Peroxides from Phospholipids
by Ag+ CIS-MS
204
6.
Precautions of Applying Ag+ CIS-MS to Study Lipids
207
7.
Conclusions
208
Acknowledgments
209
References
209
12.
Quantification of Cardiolipin by Liquid
Chromatography-Electrospray lonization Mass Spectrometry
213
Teresa A. Garrett,
Reza
Kordestani, and Christian R. H. Raetz
1.
Introduction
214
2.
Complexity of Cardiolipin Structure
217
3.
Analysis of Synthetic Cardiolipin Standards Using Liquid
Chromatography-Mass Spectrometry 2a8
Contents ix
4. Liquid Chromatography-Mass Spectrometry
of
Cardiolipins in
Total Lipid
Extracts
221
5.
Quantification of
Cardiolipin
226
Acknowledgments
228
References
228
Author Index
231
Subject Index
245 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| building | Verbundindex |
| bvnumber | BV022964637 |
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| classification_tum | CHE 840f |
| ctrlnum | (OCoLC)181101160 (DE-599)BVBBV022964637 |
| dewey-full | 547.77046 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 547 - Organic chemistry |
| dewey-raw | 547.77046 |
| dewey-search | 547.77046 |
| dewey-sort | 3547.77046 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Biologie Chemie |
| discipline_str_mv | Chemie / Pharmazie Biologie Chemie |
| format | Book |
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| genre | (DE-588)4143413-4 Aufsatzsammlung gnd-content |
| genre_facet | Aufsatzsammlung |
| id | DE-604.BV022964637 |
| illustrated | Illustrated |
| index_date | 2024-07-02T19:06:07Z |
| indexdate | 2024-08-14T00:52:03Z |
| institution | BVB |
| isbn | 9780123739667 0123739667 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-016168966 |
| oclc_num | 181101160 |
| open_access_boolean | |
| owner | DE-355 DE-BY-UBR DE-12 DE-91G DE-BY-TUM DE-20 DE-19 DE-BY-UBM |
| owner_facet | DE-355 DE-BY-UBR DE-12 DE-91G DE-BY-TUM DE-20 DE-19 DE-BY-UBM |
| physical | XLII, 249 S. Ill., graph. Darst. |
| publishDate | 2007 |
| publishDateSearch | 2007 |
| publishDateSort | 2007 |
| publisher | Elsevier, Acad. Press |
| record_format | marc |
| series | Methods in enzymology |
| series2 | Methods in enzymology |
| spelling | Lipidomics and bioactive lipids: Specialized analytical methods and lipids in disease ed. by H. Alex Brown Amsterdam [u.a.] Elsevier, Acad. Press 2007 XLII, 249 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Methods in enzymology 433 Lipids Analysis Lipids Spectra Lipids analysis Mass Spectrometry methods Mass spectrometry Lipide (DE-588)4035873-2 gnd rswk-swf Labortechnik (DE-588)4123602-6 gnd rswk-swf Krankheit (DE-588)4032844-2 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Lipide (DE-588)4035873-2 s Krankheit (DE-588)4032844-2 s Labortechnik (DE-588)4123602-6 s b DE-604 Brown, H. Alex Sonstige oth Methods in enzymology 433 (DE-604)BV000000938 433 Digitalisierung UB Regensburg application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016168966&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Lipidomics and bioactive lipids: Specialized analytical methods and lipids in disease Methods in enzymology Lipids Analysis Lipids Spectra Lipids analysis Mass Spectrometry methods Mass spectrometry Lipide (DE-588)4035873-2 gnd Labortechnik (DE-588)4123602-6 gnd Krankheit (DE-588)4032844-2 gnd |
| subject_GND | (DE-588)4035873-2 (DE-588)4123602-6 (DE-588)4032844-2 (DE-588)4143413-4 |
| title | Lipidomics and bioactive lipids: Specialized analytical methods and lipids in disease |
| title_auth | Lipidomics and bioactive lipids: Specialized analytical methods and lipids in disease |
| title_exact_search | Lipidomics and bioactive lipids: Specialized analytical methods and lipids in disease |
| title_exact_search_txtP | Lipidomics and bioactive lipids: Specialized analytical methods and lipids in disease |
| title_full | Lipidomics and bioactive lipids: Specialized analytical methods and lipids in disease ed. by H. Alex Brown |
| title_fullStr | Lipidomics and bioactive lipids: Specialized analytical methods and lipids in disease ed. by H. Alex Brown |
| title_full_unstemmed | Lipidomics and bioactive lipids: Specialized analytical methods and lipids in disease ed. by H. Alex Brown |
| title_short | Lipidomics and bioactive lipids: Specialized analytical methods and lipids in disease |
| title_sort | lipidomics and bioactive lipids specialized analytical methods and lipids in disease |
| topic | Lipids Analysis Lipids Spectra Lipids analysis Mass Spectrometry methods Mass spectrometry Lipide (DE-588)4035873-2 gnd Labortechnik (DE-588)4123602-6 gnd Krankheit (DE-588)4032844-2 gnd |
| topic_facet | Lipids Analysis Lipids Spectra Lipids analysis Mass Spectrometry methods Mass spectrometry Lipide Labortechnik Krankheit Aufsatzsammlung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016168966&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV000000938 |
| work_keys_str_mv | AT brownhalex lipidomicsandbioactivelipidsspecializedanalyticalmethodsandlipidsindisease |