Chemistry and technology of carbodiimides:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Chichester [u.a.]
Wiley
2007
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Includes bibliographical references |
| Beschreibung: | XIV, 294 S. graph. Darst. |
| ISBN: | 9780470065105 0470065109 |
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| 100 | 1 | |a Ulrich, Henri |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Chemistry and technology of carbodiimides |c Henri Ulrich |
| 264 | 1 | |a Chichester [u.a.] |b Wiley |c 2007 | |
| 300 | |a XIV, 294 S. |b graph. Darst. | ||
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Datensatz im Suchindex
| _version_ | 1804137139248562176 |
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| adam_text | Titel: Chemistry and technology of carbodiimides
Autor: Ulrich, Henri
Jahr: 2007
Contents
Preface xiü
Acknowledgements xv
1 General Introduction I
1.1 References 5
2 Alkyl- and Arylcarbodümides 9
2.1 Introduction 9
2.2 Synthesis of Alkyl- and Arylcarbodümides 10
2.2.1 From Thioureas, Isothioureas and Selenoureas 10
2.2.2 By Dehydration of Ureas 16
2.2.3 From Isocyanates or Isothiocyanates 17
2.2.4 From Cyanamides 25
2.2.5 By Nitrene Rearrangements 25
2.2.6 From Haloformamidines or Carbonimidoyl Dihalides 28
2.2.7 By Thermolysis Reactions 29
2.2.8 By Miscellaneous Other Methods 33
2.3 References I 36
2.4 Reactions of Alkyl- and Arylcarbodümides 41
vi Contents
2.4.1 Oligomerïzation and Polymerization 41
2.4.2 Cycloaddition Reactions 46
2.4.3 Reaction of Ylides with Carbodiimides 76
2.4.4 Insertion Reactions 78
2.4.5 Nucleophilic Reactions 83
2.4.6 Heterocycles from Carbodiimides 104
2.4.7 Use of Carbodiimides In Condensation Reactions 113
2.4.8 Miscellaneous Reactions 125
2.5 References II 130
3 Unsaturated Carbodiimides 147
3.1 Introduction 147
3.2 Synthesis of Unsaturated Carbodiimides 148
3.2.1 From Thioureas 148
3.2.2 From Unsaturated Isocyanates 148
3.2.3 From Unsaturated Iminophosphoranes and
Isocyanates or Isothiocyanates 148
3.2.4 By Other Methods 154
3.3 Reactions of Unsaturated Carbodiimides 154
3.3.1 Polymerization Reactions 154
3.3.2 Cycloaddition Reactions 154
3.3.3 Other Reactions 162
3.4 References 162
4 Halogenated Carbodiimides 165
4.1 Introduction 165
Contents vi i
4.2 Synthesis of Halogenated Carbodiimides 165
4.2.1 From a-Haloisocyanates 165
4.2.2 By Halogenation of Carbodiimides 166
4.2.3 From Carbonimidoyl Dichlorides or ImidoyI Chlorides 166
4.2.4 By Other Methods 167
4.3 Reactions of Halogenated Carbodiimides 168
4.3.1 Cycloaddition Reactions 168
4.3.2 Nucleophilic Reactions 169
4.3.3 Other Reactions 170
4.4 References 171
Acyl-, Thioacyl- and Imidoylcarbodiimides 173
5.1 Introduction 173
5.2 Synthesis of Acyl-, Thioacyl- and Imidoylcarbodiimides 174
5.2.1 From Thioureas 174
5.2.2 From Ureas 176
5.2.3 From Isocyanates 177
5.2.4 From Carbonimidoyl Dichlorides
or Chloroformamidines 178
5.2.5 From Cyanamides 179
5.2.6 From Other Carbodiimides 179
5.2.7 By Other Methods 179
5.3 Reactions of Acyl-, Thioacyl- and Imidoylcarbodiimides 180
5.3.1 Cycloaddition Reactions 180
5.3.2 Other Reaction 180
v¡¡¡ Contents
5.4 References 180
6 Silicon Substituted Carbodiimides 183
6.1 Introduction 183
6.2 Synthesis of Silicon Substituted Carbodiimides 183
6.2.1 From Cyanamides 183
6.2.2 From Ureas 184
6.2.3 From Isocyanates and Isothiocyanates 184
6.2.4 From Silylamines 185
6.2.5 From Other Carbodiimides 186
6.2.6 By Other Methods 186
6.3 Reactions of Silicon Substituted Carbodiimides 187
6.3.1 Oligomerization Reactions 187
6.3.2 Cycloaddition Reactions 188
6.3.3 Other Reactions 190
6.4 References 191
7 Nitrogen Substituted Carbodiimides 195
7.1 Introduction 195
7.2 Synthesis of Nitrogen Substituted Carbodiimides 195
7.3 Reactions of Nitrogen Substituted Carbodiimides 198
7.4 References 198
8 Phosphorous Substituted Carbodiimides 199
8.1 Introduction 199
8.2 Synthesis of Phosphorous Substituted Carbodiimides 199
Contents ix
8.2.1 From Thioureas 199
8.2.2 From Iminophosphoranes 200
8.2.3 From Carbonimidoyl Dichlorides 200
8.2.4 From Cyanamides 201
8.2.5 From Other Carbodiimides 202
8.2.6 By Other Method 203
8.3 Reactions of Phosphorous Substituted Carbodiimides 203
8.4 References 204
9 Sulfur Substituted Carbodiimides 205
9.1 Introduction 205
9.2 Synthesis of Sulfur Substituted Carbodiimides 205
9.2.1 From Thioureas or Ureas 205
9.2.2 From Carbonimidoyl Dichlorides or ImidoyI Chlorides 206
9.2.3 By Fragmentation Reactions 207
9.2.4 From Other Carbodiimides 208
9.2.5 By Other Methods 208
9.3 Reactions of Sulfur Substituted Carbodiimides 209
9.4 References 210
10 Metal Substituted Carbodiimides 213
10.1 Introduction 213
10.2 Synthesis of Metal Substituted Carbodiimides 214
10.2.1 From Cyanamides 214
10.2.2 From Isocyanates 215
÷ Contents
10.2.3 From Other Carbodiimides 216
10.2.4 By Other Methods 217
10.2.5 Synthesis of Metal Carbodiimide Adducts 218
10.3 Reactions of Metal Substituted Carbodiimides 222
10.4 References 223
11 Cyclic Carbodiimides 227
11.1 Introduction 227
11.2 Synthesis of Cyclic Carbodiimides 229
11.2.1 From Cyclic Thioureas 229
11.2.2 By Nitrene Rearrangement 230
11.2.3 From Bisaryliminophosphoranes and Isocyanates
or Isothiocyanates 231
11.3 Reactions of Cyclic Carbodiimides 236
11.3.1 Nucleophilic Reactions 236
11.3.2 Oligomerization Reactions 237
11.3.3 Cycloaddition Reactions 238
11.3.4 Other Reactions 240
11.4 References 241
12 Polymeric Carbodiimides 243
12.1 Introduction 243
12.2 Isocyanate Terminated Polycarbodiimides 243
12.3 Oligomeric Carbodiimides 247
12.4 Linear Homopolymers via Addition Across the C=N Bonds 248
Contents xi
12.5 Polymers Derived from Unsaturated Carbodiimides 250
12.6 Linear Polymers 251
12.7 Crosslinked Homo- and Copolymers 252
12.8 Modification of Linear Polymers with Carbodiimides 253
12.8.1 Crosslinking of Polymers 253
12.8.2 Modification of Linear Polymers 254
12.8.3 Modification of Crosslinked Polymers 254
12.9 References 255
13 Applications of Carbodiimides 259
13.1 Introduction 259
13.2 Applications in Organic Synthesis 260
13.3 Biological Applications 261
13.3.1 Antibiotic Synthesis 261
13.3.2 Protein and DNA Synthesis 261
13.3.3 Modification of Proteins 264
13.3.4 Crosslinking of Proteins 266
13.3.5 Carbodiimides in Pharmaceuticals, Herbicides
and Pesticides 267
13.4 Polymer and Industrial Applications 268
13.4.1 Use in Polymer Synthesis 268
13.4.2 Use in Polymer Applications 269
13.4.3 Polymer Modifications 271
13.4.4 Carbodiimides as Stabilizers 271
x¡¡ Contents
13.4.5 Carbodümides in Dye Applications 272
13.4.6 Other Applications 273
13.5 References 274
Index 283
|
| adam_txt |
Titel: Chemistry and technology of carbodiimides
Autor: Ulrich, Henri
Jahr: 2007
Contents
Preface xiü
Acknowledgements xv
1 General Introduction I
1.1 References 5
2 Alkyl- and Arylcarbodümides 9
2.1 Introduction 9
2.2 Synthesis of Alkyl- and Arylcarbodümides 10
2.2.1 From Thioureas, Isothioureas and Selenoureas 10
2.2.2 By Dehydration of Ureas 16
2.2.3 From Isocyanates or Isothiocyanates 17
2.2.4 From Cyanamides 25
2.2.5 By Nitrene Rearrangements 25
2.2.6 From Haloformamidines or Carbonimidoyl Dihalides 28
2.2.7 By Thermolysis Reactions 29
2.2.8 By Miscellaneous Other Methods 33
2.3 References I 36
2.4 Reactions of Alkyl- and Arylcarbodümides 41
vi Contents
2.4.1 Oligomerïzation and Polymerization 41
2.4.2 Cycloaddition Reactions 46
2.4.3 Reaction of Ylides with Carbodiimides 76
2.4.4 Insertion Reactions 78
2.4.5 Nucleophilic Reactions 83
2.4.6 Heterocycles from Carbodiimides 104
2.4.7 Use of Carbodiimides In Condensation Reactions 113
2.4.8 Miscellaneous Reactions 125
2.5 References II 130
3 Unsaturated Carbodiimides 147
3.1 Introduction 147
3.2 Synthesis of Unsaturated Carbodiimides 148
3.2.1 From Thioureas 148
3.2.2 From Unsaturated Isocyanates 148
3.2.3 From Unsaturated Iminophosphoranes and
Isocyanates or Isothiocyanates 148
3.2.4 By Other Methods 154
3.3 Reactions of Unsaturated Carbodiimides 154
3.3.1 Polymerization Reactions 154
3.3.2 Cycloaddition Reactions 154
3.3.3 Other Reactions 162
3.4 References 162
4 Halogenated Carbodiimides 165
4.1 Introduction 165
Contents vi i
4.2 Synthesis of Halogenated Carbodiimides 165
4.2.1 From a-Haloisocyanates 165
4.2.2 By Halogenation of Carbodiimides 166
4.2.3 From Carbonimidoyl Dichlorides or ImidoyI Chlorides 166
4.2.4 By Other Methods 167
4.3 Reactions of Halogenated Carbodiimides 168
4.3.1 Cycloaddition Reactions 168
4.3.2 Nucleophilic Reactions 169
4.3.3 Other Reactions 170
4.4 References 171
Acyl-, Thioacyl- and Imidoylcarbodiimides 173
5.1 Introduction 173
5.2 Synthesis of Acyl-, Thioacyl- and Imidoylcarbodiimides 174
5.2.1 From Thioureas 174
5.2.2 From Ureas 176
5.2.3 From Isocyanates 177
5.2.4 From Carbonimidoyl Dichlorides
or Chloroformamidines 178
5.2.5 From Cyanamides 179
5.2.6 From Other Carbodiimides 179
5.2.7 By Other Methods 179
5.3 Reactions of Acyl-, Thioacyl- and Imidoylcarbodiimides 180
5.3.1 Cycloaddition Reactions 180
5.3.2 Other Reaction 180
v¡¡¡ Contents
5.4 References 180
6 Silicon Substituted Carbodiimides 183
6.1 Introduction 183
6.2 Synthesis of Silicon Substituted Carbodiimides 183
6.2.1 From Cyanamides 183
6.2.2 From Ureas 184
6.2.3 From Isocyanates and Isothiocyanates 184
6.2.4 From Silylamines 185
6.2.5 From Other Carbodiimides 186
6.2.6 By Other Methods 186
6.3 Reactions of Silicon Substituted Carbodiimides 187
6.3.1 Oligomerization Reactions 187
6.3.2 Cycloaddition Reactions 188
6.3.3 Other Reactions 190
6.4 References 191
7 Nitrogen Substituted Carbodiimides 195
7.1 Introduction 195
7.2 Synthesis of Nitrogen Substituted Carbodiimides 195
7.3 Reactions of Nitrogen Substituted Carbodiimides 198
7.4 References 198
8 Phosphorous Substituted Carbodiimides 199
8.1 Introduction 199
8.2 Synthesis of Phosphorous Substituted Carbodiimides 199
Contents ix
8.2.1 From Thioureas 199
8.2.2 From Iminophosphoranes 200
8.2.3 From Carbonimidoyl Dichlorides 200
8.2.4 From Cyanamides 201
8.2.5 From Other Carbodiimides 202
8.2.6 By Other Method 203
8.3 Reactions of Phosphorous Substituted Carbodiimides 203
8.4 References 204
9 Sulfur Substituted Carbodiimides 205
9.1 Introduction 205
9.2 Synthesis of Sulfur Substituted Carbodiimides 205
9.2.1 From Thioureas or Ureas 205
9.2.2 From Carbonimidoyl Dichlorides or ImidoyI Chlorides 206
9.2.3 By Fragmentation Reactions 207
9.2.4 From Other Carbodiimides 208
9.2.5 By Other Methods 208
9.3 Reactions of Sulfur Substituted Carbodiimides 209
9.4 References 210
10 Metal Substituted Carbodiimides 213
10.1 Introduction 213
10.2 Synthesis of Metal Substituted Carbodiimides 214
10.2.1 From Cyanamides 214
10.2.2 From Isocyanates 215
÷ Contents
10.2.3 From Other Carbodiimides 216
10.2.4 By Other Methods 217
10.2.5 Synthesis of Metal Carbodiimide Adducts 218
10.3 Reactions of Metal Substituted Carbodiimides 222
10.4 References 223
11 Cyclic Carbodiimides 227
11.1 Introduction 227
11.2 Synthesis of Cyclic Carbodiimides 229
11.2.1 From Cyclic Thioureas 229
11.2.2 By Nitrene Rearrangement 230
11.2.3 From Bisaryliminophosphoranes and Isocyanates
or Isothiocyanates 231
11.3 Reactions of Cyclic Carbodiimides 236
11.3.1 Nucleophilic Reactions 236
11.3.2 Oligomerization Reactions 237
11.3.3 Cycloaddition Reactions 238
11.3.4 Other Reactions 240
11.4 References 241
12 Polymeric Carbodiimides 243
12.1 Introduction 243
12.2 Isocyanate Terminated Polycarbodiimides 243
12.3 Oligomeric Carbodiimides 247
12.4 Linear Homopolymers via Addition Across the C=N Bonds 248
Contents xi
12.5 Polymers Derived from Unsaturated Carbodiimides 250
12.6 Linear Polymers 251
12.7 Crosslinked Homo- and Copolymers 252
12.8 Modification of Linear Polymers with Carbodiimides 253
12.8.1 Crosslinking of Polymers 253
12.8.2 Modification of Linear Polymers 254
12.8.3 Modification of Crosslinked Polymers 254
12.9 References 255
13 Applications of Carbodiimides 259
13.1 Introduction 259
13.2 Applications in Organic Synthesis 260
13.3 Biological Applications 261
13.3.1 Antibiotic Synthesis 261
13.3.2 Protein and DNA Synthesis 261
13.3.3 Modification of Proteins 264
13.3.4 Crosslinking of Proteins 266
13.3.5 Carbodiimides in Pharmaceuticals, Herbicides
and Pesticides 267
13.4 Polymer and Industrial Applications 268
13.4.1 Use in Polymer Synthesis 268
13.4.2 Use in Polymer Applications 269
13.4.3 Polymer Modifications 271
13.4.4 Carbodiimides as Stabilizers 271
x¡¡ Contents
13.4.5 Carbodümides in Dye Applications 272
13.4.6 Other Applications 273
13.5 References 274
Index 283 |
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| index_date | 2024-07-02T18:49:19Z |
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| language | English |
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| spelling | Ulrich, Henri Verfasser aut Chemistry and technology of carbodiimides Henri Ulrich Chichester [u.a.] Wiley 2007 XIV, 294 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Includes bibliographical references Carbodiimides Carbodiimide (DE-588)4147293-7 gnd rswk-swf Carbodiimide (DE-588)4147293-7 s DE-604 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016082342&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Ulrich, Henri Chemistry and technology of carbodiimides Carbodiimides Carbodiimide (DE-588)4147293-7 gnd |
| subject_GND | (DE-588)4147293-7 |
| title | Chemistry and technology of carbodiimides |
| title_auth | Chemistry and technology of carbodiimides |
| title_exact_search | Chemistry and technology of carbodiimides |
| title_exact_search_txtP | Chemistry and technology of carbodiimides |
| title_full | Chemistry and technology of carbodiimides Henri Ulrich |
| title_fullStr | Chemistry and technology of carbodiimides Henri Ulrich |
| title_full_unstemmed | Chemistry and technology of carbodiimides Henri Ulrich |
| title_short | Chemistry and technology of carbodiimides |
| title_sort | chemistry and technology of carbodiimides |
| topic | Carbodiimides Carbodiimide (DE-588)4147293-7 gnd |
| topic_facet | Carbodiimides Carbodiimide |
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