Chemical analysis: modern instrumentation methods and techniques
"Chemical Analysis is an essential introduction to a wide range of analytical techniques and instruments. Assuming little in the way of prior knowledge, this text carefully guides the reader through more widely used and important techniques, whilst avoiding excessive technical detail. Covering...
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English French |
| Veröffentlicht: |
Chichester [u.a.]
Wiley
2007
|
| Ausgabe: | 2. ed., reprint. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Zusammenfassung: | "Chemical Analysis is an essential introduction to a wide range of analytical techniques and instruments. Assuming little in the way of prior knowledge, this text carefully guides the reader through more widely used and important techniques, whilst avoiding excessive technical detail. Covering both instrumentation techniques and the situations in which they will be used, the text always strives to maintain a balance between breadth and depth of coverage. Carefully structured, this book clearly differentiates between separation and spectroscopic methods, and includes a dedicated section on more specialized techniques." "The Second Edition of Chemical Analysis has been fully revised and updated throughout and includes some of the emerging techniques such as APXS, AMS, IMS or devices such as AGS. A new chapter on Elemental Analysis has been added, and additional problems and solutions have been introduced throughout the book."--BOOK JACKET. |
| Beschreibung: | XXIII, 574 S. Ill., graph. Darst. |
| ISBN: | 9780470859032 0470859032 9780470859025 |
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| 245 | 1 | 0 | |a Chemical analysis |b modern instrumentation methods and techniques |c Francis Rouessac and Annick Rouessac |
| 250 | |a 2. ed., reprint. | ||
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| 520 | 1 | |a "Chemical Analysis is an essential introduction to a wide range of analytical techniques and instruments. Assuming little in the way of prior knowledge, this text carefully guides the reader through more widely used and important techniques, whilst avoiding excessive technical detail. Covering both instrumentation techniques and the situations in which they will be used, the text always strives to maintain a balance between breadth and depth of coverage. Carefully structured, this book clearly differentiates between separation and spectroscopic methods, and includes a dedicated section on more specialized techniques." "The Second Edition of Chemical Analysis has been fully revised and updated throughout and includes some of the emerging techniques such as APXS, AMS, IMS or devices such as AGS. A new chapter on Elemental Analysis has been added, and additional problems and solutions have been introduced throughout the book."--BOOK JACKET. | |
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Datensatz im Suchindex
| _version_ | 1804137101317373952 |
|---|---|
| adam_text | FOREWORD TO THE FIRST ENGLISH EDITION XIII PREFACE TO THE FIRST ENGLISH
EDITION XV PREFACE TO SECOND EDITION XVII ACKNOWLEDGMENTS XIX
INTRODUCTION XXI PART 1 SEPARATION METHODS 1 1 GENERAL ASPECTS OF
CHROMATOGRAPHY 3 1.1 GENERAL CONCEPTS OF ANALYTICAL CHROMATOGRAPHY 3 1.2
THE CHROMATOGRAM 6 1.3 GAUSSIAN-SHAPED ELUTION PEAKS 7 1.4 THE PLATE
THEORY 9 1.5 NERNST PARTITION COEFFICIENT (K) 11 1.6 COLUMN EFFICIENCY
12 1.7 RETENTION PARAMETERS 14 1.8 SEPARATION (OR SELECTIVITY) FACTOR
BETWEEN TWO SOLUTES 17 1.9 RESOLUTION FACTOR BETWEEN TWO PEAKS 17 1.10
THE RATE THEORY OF CHROMATOGRAPHY 19 1.11 OPTIMIZATION OF A
CHROMATOGRAPHIE ANALYSIS 22 1.12 CLASSIFICATION OF CHROMATOGRAPHIE
TECHNIQUES 24 PROBLEMS 27 2 GAS CHROMATOGRAPHY 31 2.1 COMPONENTS OF A GC
INSTALLATION 31 2.2 CARRIER GAS AND FIOW REGULATION 33 2.3 SAMPLE
INTRODUCTION AND THE INJEETION CHAMBER 34 2.4 THERMOSTATICALLY CONTROUEED
OVEN 39 2.5 COLUMNS 39 2.6 STATIONARY PHASES 41 2.7 PRINCIPAL GAS
CHROMATOGRAPHIE DETECTORS 46 2.8 DETECTORS PROVIDING STRUCTURAL DATA 50
2.9 FAST CHROMATOGRAPHY 52 2.10 MULTI-DIMENSIONAL CHROMATOGRAPHY 53 2.11
RETENTION INDEXES AND STATIONARY PHASE CONSTANTS 54 PROBLEMS 58 VI
CONTENTS 3 HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY 63 3.1 THE BEGINNINGS
OF HPLC 63 3.2 GENERAL CONCEPT OF AN HPLC SYSTEM 64 3.3 PUMPS AND
GRADIENT ELUTION 65 3.4 INJECTORS 68 3.5 COLUMNS 68 3.6 STATIONARY
PHASES 70 3.7 CHIRAL CHROMATOGRAPHY 75 3.8 MOBILE PHASES 76 3.9
PAIRED-ION CHROMATOGRAPHY 78 3.10 HYDROPHOBIE INTERACTION CHROMATOGRAPHY
80 3.11 PRINCIPAL DETECTORS 80 3.12 EVOLUTION AND APPLICATIONS OF HPLC
87 PROBLEMS 89 4 ION CHROMATOGRAPHY 93 4.1 BASICS OF ION CHROMATOGRAPHY
93 4.2 STATIONARY PHASES 96 4.3 MOBILE PHASES 98 4.4 CONDUCTIVITY
DETECTORS 100 4.5 ION SUPPRESSORS 101 4.6 PRINCIPLE AND BASIC
RELATIONSHIP 104 4.7 AREAS OF THE PEAKS AND DATA TREATMENT SOFTWARE 105
4.8 EXTERNAL STANDARD METHOD 105 4.9 INTERNAL STANDARD METHOD 107 4.10
INTERNAL NORMALIZATION METHOD 110 PROBLEMS 112 5 THIN LAYER
CHROMATOGRAPHY 117 5.1 PRINCIPLE OF TLC 117 5.2 CHARACTERISTICS OF TLC
120 5.3 STATIONARY PHASES 121 5.4 SEPARATION AND RETENTION PARAMETERS
122 5.5 QUANTITATIVE TLC 123 PROBLEMS 125 6 SUPERCNTICAL FLUID
CHROMATOGRAPHY 127 6.1 SUPERCNTICAL FLUIDS: A REMINDER 127 6.2
SUPERCNTICAL FLUIDS AS MOBILE PHASES 129 6.3 INSTRUMENTATION IN SFC 130
6.4 COMPARISON OF SFC WITH HPLC AND GC 131 6.5 SFC IN CHROMATOGRAPHIE
TECHNIQUES 133 7 SIZE EXCLUSION CHROMATOGRAPHY 135 7.1 PRINCIPLE OF SEC
135 7.2 STATIONARY AND MOBILE PHASES 137 7.3 CALIBRATION CURVES 138 7.4
INSTRUMENTATION 139 7.5 APPLICATIONS OF SEC 140 PROBLEMS 143 CONTENTS
VII CAPIUARY ELECTROPHORESIS AND ELECTROCHROMATOGRAPHY 145 8.1 FROM ZONE
ELECTROPHORESIS TO CAPILLARY ELECTROPHORESIS 145 8.2 ELECTROPHORETK
MOBILITY AND ELECTRO-OSMOTIC FLOW 148 8.3 INSTRUMENTATION 152 8.4
ELECTROPHORETIC TECHNIQUES 155 8.5 PERFORMANCE OF CE 157 8.6 CAPHLARY
ELECTROCHROMATOGRAPHY 159 PROBLEMS 161 PART 2 SPECTROSCOPIC METHODS 165
ULTRAVIOLET AND VISIBLE ABSORPTION SPECTROSCOPY 167 9.1 THE UV/VIS
SPECTRAL REGION AND THE ONGIN OF THE ABSORPTIONS 167 9.2 THE UV/VIS
SPECTRUM 169 9.3 ELECTRONIC TRANSITIONS OF ORGANIC COMPOUNDS 171 9.4
CHROMOPHORE GROUPS 173 9.5 SOLVENT EFFECTS: SOLVATOCHROMISM 174 9.6
FIESER-WOODWARD RULES 176 9.7 INSTRUMENTATION IN THE UV/VISIBLE 178 9.8
UV/VIS SPECTROPHOTOMETERS 181 9.9 QUANTITATIVE ANALYSIS: LAWS OF
MOLECULAR ABSORPTION 186 9.10 METHODS IN QUANTITATIVE ANALYSIS 190 9.11
ANALYSIS OF A SINGLE ANALYTE AND PURITY CONTROL 192 9.12 MULTICOMPONENT
ANALYSIS (MCA) 193 9.13 METHODS OF BASELINE CORRECTION 196 9.14 RELATIVE
ERROR DISTRIBUTION DUE TO INSTRUMENTS 198 9.15 DERIVATIVE SPECTROMETRY
200 9.16 VISUAL COLORIMETRY BY TRANSMISSION OR REFLECTION 202 PROBLEMS
203 10 INFRARED SPECTROSCOPY 207 10.1 THE ORIGIN OF LIGHT ABSORPTION IN
THE INFRARED 207 10.2 ABSORPTIONS IN THE INFRARED 208 10.3
ROTATIONAL-VIBRATIONAL BANDS IN THE MID-IR 208 10.4 SIMPLIFIED MODEL FOR
VIBRATIONAL INTERACTIONS 210 10.5 REAL COMPOUNDS 212 10.6 CHARACTERISTIC
BANDS FOR ORGANIC COMPOUNDS 212 10.7 INFRARED SPECTROMETERS AND
ANALYSERS 216 10.8 SOURCES AND DETECTORS USED IN THE MID-IR 221 10-9
SAMPLE ANALYSIS TECHNIQUES 225 10.10 CHEMICAL IMAGING SPECTROSCOPY IN
THE INFRARED 230 10.11 ARCHIVING SPECTRA 232 10.12 COMPARISON OF SPECTRA
233 10.13 QUANTITATIVE ANALYSIS 234 PROBLEMS 238 11 FLUORIMETRY AND
CHEMILUMINESCENCE 241 11.1 FLUORESCENCE AND PHOSPHORESCENCE 241 11.2 THE
ORIGIN OF FLUORESCENCE 243 11.3 RELATIONSHIP BETWEEN FLUORESCENCE AND
CONCENTRATION 245 11.4 RAYLEIGH SCATTERING AND RAMAN BANDS 247 11.5
INSTRUMENTATION 249 11.6 APPLICATIONS 253 11.7 TIME-RESOLVED FLUORIMETRY
255 11.8 CHEMILUMINESCENCE 256 PROBLEMS 259 12 X-RAY FLUORESCENCE
SPECTROMETRY 263 12.1 8ASIC PRINCIPLES 263 12.2 THE X-RAY FLUORESCENCE
SPECTRUM 264 12.3 EXCITATION MODES OF ELEMENTS IN X-RAY FLUORESCENCE 266
12.4 DETECTION OF X-RAYS 271 12.5 OIFFERENT TYPES OF INSTRUMENTS 273
12.6 SAMPLE PREPARATION 277 12.7 X-RAY ABSORPTION - X-RAY DENSIMETRY 278
12.8 QUANTITATIVE ANALYSIS BY X-RAY FLUORESCENCE 279 12.9 APPLICATIONS
OF X-RAY FTUORESCENCE 279 PROBLEMS 281 13 ATOMIC ABSORPTION AND FLAME
EMISSION SPECTROSCOPY 285 13.1 THE EFFECT OF TEMPERATURE UPON AN ELEMENT
285 13.2 APPLICATIONS TO MODERN INSTRUMENTS 288 13.3 ATOMIC ABSORPTION
VERSUS FLAME EMISSION 288 13.4 MEASUREMENTS BY AAS OR BY FES 290 13.5
BASIC INSTRUMENTATION FOR AAS 291 13.6 FLAME PHOTOMETERS 297 13.7
CORRECTION OF INTERFERING ABSORPTIONS 298 13.8 PHYSICAL AND CHEMICAL
INTERFERENCES 302 13.9 SENSITIVITY AND DETECTION LIMITS IN AAS 304
PROBLEMS 305 14 ATOMIC EMISSION SPECTROSCOPY 309 14.1 OPTICAL EMISSION
SPECTROSCOPY {OES} 309 14.2 PRINCIPLE OF ATOMIC EMISSION ANALYSIS 310
14.3 DISSOCIATION OF THE SAMPLE INTO ATOMS OR IONS 311 14.4 OISPERSIVE
SYSTEMS AND SPECTRAL LINES 315 14.5 SIMULTANEOUS AND SEQUENTIAL
INSTRUMENTS 317 14.6 PERFORMANCES 321 14.7 APPLICATIONS OF OES 323
PROBLEMS 324 15 NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY 327 15.1 GENERAL
INTRODUCTION 327 15.2 SPIN/MAGNETIC FIELD INTERACTION FOR A NUCLEUS 328
15.3 NUCLEI THAT CAN BE STUDIED BY NMR 331 CONTENTS IX 15.4 BLOCH THEORY
FOR A NUCLEUS OF SPIN NUMBER / *1/2 331 15.5 LARMOR FREQUENCY 333 15.6
PULSED NMR 335 15.7 THE PROCESSES OF NUCLEAR RELAXATION 339 15.8
CHEMICAL SHIFT 340 15.9 MEASURING THE CHEMICAL SHIFT 341 15.10 SHIELDING
AND DESHIELDING OF THE NUCLEI 342 15.11 FACTORS INFLUENCING CHEMICAL
SHIFTS 342 15.12 HYPERFINE STRUCTURE - SPIN-SPIN COUPLING 344 15.13
HETERONUCLEAR COUPLING 345 15.14 HOMONUCLEAR COUPLING 347 15.15 SPIN
DECOUPLING AND PARTICULAR PULSE SEQUENCES 352 15.16 HPLC-NMR COUPLING
354 15.17 FLUORINE AND PHOSPHORUS NMR 355 15.18 QUANTITATIVE NMR 356
15.19 ANALYSERS USING PULSED NMR 360 PROBLEMS 364 PART 3 OTHER METHODS
367 16 MASS SPECTROMETRY 369 16.1 BASIC PRINCIPLES 369 16.2 THE
MAGNETIC-SECTOR DESIGN 372 16.3 EB OR BE GEOMETRY MASS ANALYSERS 374
16.4 TIME OF FLIGHT ANALYSERS (TOF) 379 16.5 QUADRUPOLE ANALYSERS 381
16.6 QUADRUPOLE ION TRAP ANALYSERS 385 16.7 ION CYDOTRON RESONANCE
ANALYSERS (ICRMS) 387 16.8 MASS SPECTROMETER PERFORMANCES 389 16.9
SAMPLE INTRODUCTION 391 16.10 MAJOR VACUUM IONIZATION TECHNIQUES 392
16.11 ATMOSPHERIC PRESSURE IONIZATION (API) 397 16.12 TANDEM MASS
SPECTROMETRY (MS/MS) 401 16.13 ION DETECTION 402 16.14 IDENTIFICATION BY
MEANS OF A SPECTRAL LIBRARY 404 16.15 ANALYSIS OF THE ELEMENTARY
COMPOSITION OF IONS 405 16.16 DETERMINATION OF MOLECULAR MASSES FROM
MULTICHARGED IONS 407 16.17 DETERMINATION OF ISOTOPE RATIOS FOR AN
ELEMENT 408 16.18 FRAGMENTATION OF ORGANIC IONS 410 PROBLEMS 415 17
LABELLING METHODS 419 17.1 THE PRINCIPLE OF LABELLING METHODOLOGIES 419
17.2 DIRECT ISOTOPE DILUTION ANALYSIS WITH A RADIOACTIVE LABEL 420 17.3
SUBSTOICHIOMETRIC ISOTOPE DILUTION ANALYSIS 421 17.4 RADIO IMMUNO-ASSAYS
(RIA) 422 17.5 MEASURING RADIOISOTOPE ACTIVITY 423 17.6 ANTIGENS AND
ANTIBODIES 425 X CONTENTS 17.7 ENZYMATIC-IMMUNOASSAY (EIA) 426 17.8
OTHER IMMUNOENZYMATIC TECHNIQUES 429 17.9 ADVANTAGES AND LIMITATIONS OF
THE ELISA TEST IN CHEMISTRY 430 17.10 IMMUNOFLUORESCENCE ANALYSIS (IFA)
431 17.11 STAHLE ISOTOPE LABELLING 431 17.12 NEUTRON ACTIVATION ANALYSIS
(NAA) 432 PROBLEMS 437 18 ELEMENTAL ANALYSIS 441 18.1 PARTICULAR
ANALYSES 441 18.2 ELEMENTAL ORGANIC MICROANALYSIS 442 18.3 TOTAL
NITROGEN ANALYSERS (TN) 445 18.4 TOTAL SULFUR ANALYSERS 447 18.5 TOTAL
CARBON ANALYSERS (TC, TIC AND TOC) 447 18.6 MERCURY ANALYSERS 450
PROBLEMS 451 19 POTENTIOMETRIC METHODS 453 19.1 GENERAL PRINCIPLES 453
19.2 A PARTICULAR ISE: THE PH ELECTRODE 455 19.3 OTHER ION SELECTIVE
ELECTRODES 457 19.4 SLOPE AND CALCULATIONS 460 19.5 APPLICATIONS 463
PROBLEMS 463 20 VOLTAMMETRIC AND COULOMETRIC METHODS 465 20.1 GENERAL
PRINCIPLES 465 20.2 THE DROPPING-MERCURY ELECTRODE 467 20.3 DIRECT
CURRENT POLAROGRAPHY (DCP) 467 20.4 DIFFUSION CURRENT 468 20.5 PULSED
POLAROGRAPHY 470 20.6 AMPEROMETRIC DETECTION IN HPLC AND HPCE 472 20.7
AMPEROMETRIC SENSORS 472 20.8 STRIPPING VOLTAMMETRY (SV) 478 20.9
POTENTIOSTATIC COULOMETRY AND AMPEROMETRIC COULOMETRY 480 20.10
COULOMETRIC TITRATION OF WATER BY THE KARL FISCHER REACTION 481 PROBLEMS
484 21 SAMPLE PREPARATION 487 21.1 THE NEED FOR SAMPLE PRETREATMENT 487
21.2 SOLID PHASE EXTRACTION (SPE) 488 21.3 IMMUNOAFFINITY EXTRACTION 490
21.4 MICROEXTRACTION PROCEDURES 491 21.5 GAS EXTRACTION ON A CARTRIDGE
OR A DISC 493 21.6 HEADSPACE 494 21.7 SUPERCRITICAL PHASE EXTRACTION
(SPE) 496 21.8 MICROWAVE REACTORS 498 21.9 ON-LINE ANALYSERS 498
CONTENTS XI 22 BASIC STATISTICAL PARAMETERS 501 22.1 MEAN VALUE,
ACCURACY OF A COLLECTION OF MEASUREMENTS 501 22.2 VARIANCE AND STANDARD
DEVIATION 504 22.3 RANDOM OR INDETERMINATE ERRORS 504 22.4 CONFIDENCE
INTERVAL OF THE MEAN 506 22.5 COMPARISON OF RESULTS - PARAMETRIC TESTS
508 22.6 REJECTION CRITERIA G-TEST (OR DIXON TEST) 510 22.7 CALIBRATION
CURVE AND REGRESSION ANALYSIS 511 22.8 ROBUST METHODS OR NON-PARAMETRIC
TESTS 513 22.9 OPTIMIZATION THROUGH THE ONE-FACTOR-AT-A-TIME (OFAT)
EXPERIMENTATION 515 PROBLEMS 516 SOLUTIONS 519 APPENDIX - LIST OF
ACRONYMS 561 BIBLIOGRAPHY 565 TABLE OF SOME USEFUL CONSTANTS - 567 INDEX
569
|
| adam_txt |
FOREWORD TO THE FIRST ENGLISH EDITION XIII PREFACE TO THE FIRST ENGLISH
EDITION XV PREFACE TO SECOND EDITION XVII ACKNOWLEDGMENTS XIX
INTRODUCTION XXI PART 1 SEPARATION METHODS 1 1 GENERAL ASPECTS OF
CHROMATOGRAPHY 3 1.1 GENERAL CONCEPTS OF ANALYTICAL CHROMATOGRAPHY 3 1.2
THE CHROMATOGRAM 6 1.3 GAUSSIAN-SHAPED ELUTION PEAKS 7 1.4 THE PLATE
THEORY 9 1.5 NERNST PARTITION COEFFICIENT (K) 11 1.6 COLUMN EFFICIENCY
12 1.7 RETENTION PARAMETERS 14 1.8 SEPARATION (OR SELECTIVITY) FACTOR
BETWEEN TWO SOLUTES 17 1.9 RESOLUTION FACTOR BETWEEN TWO PEAKS 17 1.10
THE RATE THEORY OF CHROMATOGRAPHY 19 1.11 OPTIMIZATION OF A
CHROMATOGRAPHIE ANALYSIS 22 1.12 CLASSIFICATION OF CHROMATOGRAPHIE
TECHNIQUES 24 PROBLEMS 27 2 GAS CHROMATOGRAPHY 31 2.1 COMPONENTS OF A GC
INSTALLATION 31 2.2 CARRIER GAS AND FIOW REGULATION 33 2.3 SAMPLE
INTRODUCTION AND THE INJEETION CHAMBER 34 2.4 THERMOSTATICALLY CONTROUEED
OVEN 39 2.5 COLUMNS 39 2.6 STATIONARY PHASES 41 2.7 PRINCIPAL GAS
CHROMATOGRAPHIE DETECTORS 46 2.8 DETECTORS PROVIDING STRUCTURAL DATA 50
2.9 FAST CHROMATOGRAPHY 52 2.10 MULTI-DIMENSIONAL CHROMATOGRAPHY 53 2.11
RETENTION INDEXES AND STATIONARY PHASE CONSTANTS 54 PROBLEMS 58 VI
CONTENTS 3 HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY 63 3.1 THE BEGINNINGS
OF HPLC 63 3.2 GENERAL CONCEPT OF AN HPLC SYSTEM 64 3.3 PUMPS AND
GRADIENT ELUTION 65 3.4 INJECTORS 68 3.5 COLUMNS 68 3.6 STATIONARY
PHASES 70 3.7 CHIRAL CHROMATOGRAPHY 75 3.8 MOBILE PHASES 76 3.9
PAIRED-ION CHROMATOGRAPHY 78 3.10 HYDROPHOBIE INTERACTION CHROMATOGRAPHY
80 3.11 PRINCIPAL DETECTORS 80 3.12 EVOLUTION AND APPLICATIONS OF HPLC
87 PROBLEMS 89 4 ION CHROMATOGRAPHY 93 4.1 BASICS OF ION CHROMATOGRAPHY
93 4.2 STATIONARY PHASES 96 4.3 MOBILE PHASES 98 4.4 CONDUCTIVITY
DETECTORS 100 4.5 ION SUPPRESSORS " 101 4.6 PRINCIPLE AND BASIC
RELATIONSHIP 104 4.7 AREAS OF THE PEAKS AND DATA TREATMENT SOFTWARE 105
4.8 EXTERNAL STANDARD METHOD 105 4.9 INTERNAL STANDARD METHOD 107 4.10
INTERNAL NORMALIZATION METHOD 110 PROBLEMS 112 5 THIN LAYER
CHROMATOGRAPHY 117 5.1 PRINCIPLE OF TLC 117 5.2 CHARACTERISTICS OF TLC
120 5.3 STATIONARY PHASES 121 5.4 SEPARATION AND RETENTION PARAMETERS
122 5.5 QUANTITATIVE TLC 123 PROBLEMS 125 6 SUPERCNTICAL FLUID
CHROMATOGRAPHY 127 6.1 SUPERCNTICAL FLUIDS: A REMINDER 127 6.2
SUPERCNTICAL FLUIDS AS MOBILE PHASES 129 6.3 INSTRUMENTATION IN SFC 130
6.4 COMPARISON OF SFC WITH HPLC AND GC 131 6.5 SFC IN CHROMATOGRAPHIE
TECHNIQUES 133 7 SIZE EXCLUSION CHROMATOGRAPHY 135 7.1 PRINCIPLE OF SEC
135 7.2 STATIONARY AND MOBILE PHASES 137 7.3 CALIBRATION CURVES 138 7.4
INSTRUMENTATION 139 7.5 APPLICATIONS OF SEC 140 PROBLEMS 143 CONTENTS
VII CAPIUARY ELECTROPHORESIS AND ELECTROCHROMATOGRAPHY 145 8.1 FROM ZONE
ELECTROPHORESIS TO CAPILLARY ELECTROPHORESIS 145 8.2 ELECTROPHORETK
MOBILITY AND ELECTRO-OSMOTIC FLOW 148 8.3 INSTRUMENTATION 152 8.4
ELECTROPHORETIC TECHNIQUES 155 8.5 PERFORMANCE OF CE 157 8.6 CAPHLARY
ELECTROCHROMATOGRAPHY 159 PROBLEMS 161 PART 2 SPECTROSCOPIC METHODS 165
ULTRAVIOLET AND VISIBLE ABSORPTION SPECTROSCOPY 167 9.1 THE UV/VIS
SPECTRAL REGION AND THE ONGIN OF THE ABSORPTIONS 167 9.2 THE UV/VIS
SPECTRUM 169 9.3 ELECTRONIC TRANSITIONS OF ORGANIC COMPOUNDS 171 9.4
CHROMOPHORE GROUPS 173 9.5 SOLVENT EFFECTS: SOLVATOCHROMISM 174 9.6
FIESER-WOODWARD RULES 176 9.7 INSTRUMENTATION IN THE UV/VISIBLE 178 9.8
UV/VIS SPECTROPHOTOMETERS 181 9.9 QUANTITATIVE ANALYSIS: LAWS OF
MOLECULAR ABSORPTION 186 9.10 METHODS IN QUANTITATIVE ANALYSIS 190 9.11
ANALYSIS OF A SINGLE ANALYTE AND PURITY CONTROL 192 9.12 MULTICOMPONENT
ANALYSIS (MCA) 193 9.13 METHODS OF BASELINE CORRECTION 196 9.14 RELATIVE
ERROR DISTRIBUTION DUE TO INSTRUMENTS 198 9.15 DERIVATIVE SPECTROMETRY
200 9.16 VISUAL COLORIMETRY BY TRANSMISSION OR REFLECTION 202 PROBLEMS
203 10 INFRARED SPECTROSCOPY 207 10.1 THE ORIGIN OF LIGHT ABSORPTION IN
THE INFRARED 207 10.2 ABSORPTIONS IN THE INFRARED 208 10.3
ROTATIONAL-VIBRATIONAL BANDS IN THE MID-IR 208 10.4 SIMPLIFIED MODEL FOR
VIBRATIONAL INTERACTIONS 210 10.5 REAL COMPOUNDS 212 10.6 CHARACTERISTIC
BANDS FOR ORGANIC COMPOUNDS 212 10.7 INFRARED SPECTROMETERS AND
ANALYSERS 216 10.8 SOURCES AND DETECTORS USED IN THE MID-IR 221 10-9
SAMPLE ANALYSIS TECHNIQUES 225 10.10 CHEMICAL IMAGING SPECTROSCOPY IN
THE INFRARED 230 10.11 ARCHIVING SPECTRA 232 10.12 COMPARISON OF SPECTRA
233 10.13 QUANTITATIVE ANALYSIS 234 PROBLEMS 238 11 FLUORIMETRY AND
CHEMILUMINESCENCE 241 11.1 FLUORESCENCE AND PHOSPHORESCENCE 241 11.2 THE
ORIGIN OF FLUORESCENCE 243 11.3 RELATIONSHIP BETWEEN FLUORESCENCE AND
CONCENTRATION 245 11.4 RAYLEIGH SCATTERING AND RAMAN BANDS 247 11.5
INSTRUMENTATION 249 11.6 APPLICATIONS 253 11.7 TIME-RESOLVED FLUORIMETRY
255 11.8 CHEMILUMINESCENCE 256 PROBLEMS 259 12 X-RAY FLUORESCENCE
SPECTROMETRY 263 12.1 8ASIC PRINCIPLES 263 12.2 THE X-RAY FLUORESCENCE
SPECTRUM 264 12.3 EXCITATION MODES OF ELEMENTS IN X-RAY FLUORESCENCE 266
12.4 DETECTION OF X-RAYS 271 12.5 OIFFERENT TYPES OF INSTRUMENTS 273
12.6 SAMPLE PREPARATION 277 12.7 X-RAY ABSORPTION - X-RAY DENSIMETRY 278
12.8 QUANTITATIVE ANALYSIS BY X-RAY FLUORESCENCE 279 12.9 APPLICATIONS
OF X-RAY FTUORESCENCE 279 PROBLEMS 281 13 ATOMIC ABSORPTION AND FLAME
EMISSION SPECTROSCOPY 285 13.1 THE EFFECT OF TEMPERATURE UPON AN ELEMENT
285 13.2 APPLICATIONS TO MODERN INSTRUMENTS 288 13.3 ATOMIC ABSORPTION
VERSUS FLAME EMISSION 288 13.4 MEASUREMENTS BY AAS OR BY FES 290 13.5
BASIC INSTRUMENTATION FOR AAS 291 13.6 FLAME PHOTOMETERS 297 13.7
CORRECTION OF INTERFERING ABSORPTIONS 298 13.8 PHYSICAL AND CHEMICAL
INTERFERENCES 302 13.9 SENSITIVITY AND DETECTION LIMITS IN AAS 304
PROBLEMS 305 14 ATOMIC EMISSION SPECTROSCOPY 309 14.1 OPTICAL EMISSION
SPECTROSCOPY {OES} 309 14.2 PRINCIPLE OF ATOMIC EMISSION ANALYSIS 310
14.3 DISSOCIATION OF THE SAMPLE INTO ATOMS OR IONS 311 14.4 OISPERSIVE
SYSTEMS AND SPECTRAL LINES 315 14.5 SIMULTANEOUS AND SEQUENTIAL
INSTRUMENTS 317 14.6 PERFORMANCES 321 14.7 APPLICATIONS OF OES 323
PROBLEMS 324 15 NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY 327 15.1 GENERAL
INTRODUCTION 327 15.2 SPIN/MAGNETIC FIELD INTERACTION FOR A NUCLEUS 328
15.3 NUCLEI THAT CAN BE STUDIED BY NMR 331 CONTENTS IX 15.4 BLOCH THEORY
FOR A NUCLEUS OF SPIN NUMBER / *1/2 331 15.5 LARMOR FREQUENCY 333 15.6
PULSED NMR 335 15.7 THE PROCESSES OF NUCLEAR RELAXATION 339 15.8
CHEMICAL SHIFT 340 15.9 MEASURING THE CHEMICAL SHIFT 341 15.10 SHIELDING
AND DESHIELDING OF THE NUCLEI 342 15.11 FACTORS INFLUENCING CHEMICAL
SHIFTS 342 15.12 HYPERFINE STRUCTURE - SPIN-SPIN COUPLING 344 15.13
HETERONUCLEAR COUPLING 345 15.14 HOMONUCLEAR COUPLING 347 15.15 SPIN
DECOUPLING AND PARTICULAR PULSE SEQUENCES 352 15.16 HPLC-NMR COUPLING
354 15.17 FLUORINE AND PHOSPHORUS NMR 355 15.18 QUANTITATIVE NMR 356
15.19 ANALYSERS USING PULSED NMR 360 PROBLEMS 364 PART 3 OTHER METHODS
367 16 MASS SPECTROMETRY 369 16.1 BASIC PRINCIPLES 369 16.2 THE
MAGNETIC-SECTOR DESIGN 372 16.3 'EB' OR 'BE' GEOMETRY MASS ANALYSERS 374
16.4 TIME OF FLIGHT ANALYSERS (TOF) 379 16.5 QUADRUPOLE ANALYSERS 381
16.6 QUADRUPOLE ION TRAP ANALYSERS 385 16.7 ION CYDOTRON RESONANCE
ANALYSERS (ICRMS) 387 16.8 MASS SPECTROMETER PERFORMANCES 389 16.9
SAMPLE INTRODUCTION 391 16.10 MAJOR VACUUM IONIZATION TECHNIQUES 392
16.11 ATMOSPHERIC PRESSURE IONIZATION (API) 397 16.12 TANDEM MASS
SPECTROMETRY (MS/MS) 401 16.13 ION DETECTION 402 16.14 IDENTIFICATION BY
MEANS OF A SPECTRAL LIBRARY 404 16.15 ANALYSIS OF THE ELEMENTARY
COMPOSITION OF IONS 405 16.16 DETERMINATION OF MOLECULAR MASSES FROM
MULTICHARGED IONS 407 16.17 DETERMINATION OF ISOTOPE RATIOS FOR AN
ELEMENT 408 16.18 FRAGMENTATION OF ORGANIC IONS 410 PROBLEMS 415 17
LABELLING METHODS 419 17.1 THE PRINCIPLE OF LABELLING METHODOLOGIES 419
17.2 DIRECT ISOTOPE DILUTION ANALYSIS WITH A RADIOACTIVE LABEL 420 17.3
SUBSTOICHIOMETRIC ISOTOPE DILUTION ANALYSIS 421 17.4 RADIO IMMUNO-ASSAYS
(RIA) 422 17.5 MEASURING RADIOISOTOPE ACTIVITY 423 17.6 ANTIGENS AND
ANTIBODIES 425 X CONTENTS 17.7 ENZYMATIC-IMMUNOASSAY (EIA) 426 17.8
OTHER IMMUNOENZYMATIC TECHNIQUES 429 17.9 ADVANTAGES AND LIMITATIONS OF
THE ELISA TEST IN CHEMISTRY 430 17.10 IMMUNOFLUORESCENCE ANALYSIS (IFA)
431 17.11 STAHLE ISOTOPE LABELLING 431 17.12 NEUTRON ACTIVATION ANALYSIS
(NAA) 432 PROBLEMS 437 18 ELEMENTAL ANALYSIS 441 18.1 PARTICULAR
ANALYSES 441 18.2 ELEMENTAL ORGANIC MICROANALYSIS 442 18.3 TOTAL
NITROGEN ANALYSERS (TN) 445 18.4 TOTAL SULFUR ANALYSERS 447 18.5 TOTAL
CARBON ANALYSERS (TC, TIC AND TOC) 447 18.6 MERCURY ANALYSERS 450
PROBLEMS 451 19 POTENTIOMETRIC METHODS 453 19.1 GENERAL PRINCIPLES 453
19.2 A PARTICULAR ISE: THE PH ELECTRODE 455 19.3 OTHER ION SELECTIVE
ELECTRODES 457 19.4 SLOPE AND CALCULATIONS 460 19.5 APPLICATIONS 463
PROBLEMS 463 20 VOLTAMMETRIC AND COULOMETRIC METHODS 465 20.1 GENERAL
PRINCIPLES 465 20.2 THE DROPPING-MERCURY ELECTRODE 467 20.3 DIRECT
CURRENT POLAROGRAPHY (DCP) 467 20.4 DIFFUSION CURRENT 468 20.5 PULSED
POLAROGRAPHY 470 20.6 AMPEROMETRIC DETECTION IN HPLC AND HPCE 472 20.7
AMPEROMETRIC SENSORS 472 20.8 STRIPPING VOLTAMMETRY (SV) 478 20.9
POTENTIOSTATIC COULOMETRY AND AMPEROMETRIC COULOMETRY 480 20.10
COULOMETRIC TITRATION OF WATER BY THE KARL FISCHER REACTION 481 PROBLEMS
484 21 SAMPLE PREPARATION 487 21.1 THE NEED FOR SAMPLE PRETREATMENT 487
21.2 SOLID PHASE EXTRACTION (SPE) 488 21.3 IMMUNOAFFINITY EXTRACTION 490
21.4 MICROEXTRACTION PROCEDURES 491 21.5 GAS EXTRACTION ON A CARTRIDGE
OR A DISC 493 21.6 HEADSPACE 494 21.7 SUPERCRITICAL PHASE EXTRACTION
(SPE) 496 21.8 MICROWAVE REACTORS 498 21.9 ON-LINE ANALYSERS 498
CONTENTS XI 22 BASIC STATISTICAL PARAMETERS 501 22.1 MEAN VALUE,
ACCURACY OF A COLLECTION OF MEASUREMENTS 501 22.2 VARIANCE AND STANDARD
DEVIATION 504 22.3 RANDOM OR INDETERMINATE ERRORS 504 22.4 CONFIDENCE
INTERVAL OF THE MEAN 506 22.5 COMPARISON OF RESULTS - PARAMETRIC TESTS
508 22.6 REJECTION CRITERIA G-TEST (OR DIXON TEST) 510 22.7 CALIBRATION
CURVE AND REGRESSION ANALYSIS 511 22.8 ROBUST METHODS OR NON-PARAMETRIC
TESTS 513 22.9 OPTIMIZATION THROUGH THE ONE-FACTOR-AT-A-TIME (OFAT)
EXPERIMENTATION 515 PROBLEMS 516 SOLUTIONS 519 APPENDIX - LIST OF
ACRONYMS 561 BIBLIOGRAPHY 565 TABLE OF SOME USEFUL CONSTANTS - 567 INDEX
569 |
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| author | Rouessac, Francis Rouessac, Annick |
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| bvnumber | BV022822523 |
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| dewey-full | 543 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543 |
| dewey-search | 543 |
| dewey-sort | 3543 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| discipline_str_mv | Chemie / Pharmazie |
| edition | 2. ed., reprint. |
| format | Book |
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| id | DE-604.BV022822523 |
| illustrated | Illustrated |
| index_date | 2024-07-02T18:40:37Z |
| indexdate | 2024-07-09T21:06:56Z |
| institution | BVB |
| isbn | 9780470859032 0470859032 9780470859025 |
| language | English French |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-016027858 |
| oclc_num | 74916103 |
| open_access_boolean | |
| owner | DE-20 DE-19 DE-BY-UBM DE-634 DE-11 DE-858 |
| owner_facet | DE-20 DE-19 DE-BY-UBM DE-634 DE-11 DE-858 |
| physical | XXIII, 574 S. Ill., graph. Darst. |
| publishDate | 2007 |
| publishDateSearch | 2007 |
| publishDateSort | 2007 |
| publisher | Wiley |
| record_format | marc |
| spelling | Rouessac, Francis Verfasser aut Analyse chimique Chemical analysis modern instrumentation methods and techniques Francis Rouessac and Annick Rouessac 2. ed., reprint. Chichester [u.a.] Wiley 2007 XXIII, 574 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier "Chemical Analysis is an essential introduction to a wide range of analytical techniques and instruments. Assuming little in the way of prior knowledge, this text carefully guides the reader through more widely used and important techniques, whilst avoiding excessive technical detail. Covering both instrumentation techniques and the situations in which they will be used, the text always strives to maintain a balance between breadth and depth of coverage. Carefully structured, this book clearly differentiates between separation and spectroscopic methods, and includes a dedicated section on more specialized techniques." "The Second Edition of Chemical Analysis has been fully revised and updated throughout and includes some of the emerging techniques such as APXS, AMS, IMS or devices such as AGS. A new chapter on Elemental Analysis has been added, and additional problems and solutions have been introduced throughout the book."--BOOK JACKET. Química analítica instrumental larpcal Instrumental analysis Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Instrumentelle Analytik (DE-588)4222592-9 gnd rswk-swf Methode (DE-588)4038971-6 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 s Methode (DE-588)4038971-6 s DE-604 Instrumentelle Analytik (DE-588)4222592-9 s Rouessac, Annick Verfasser aut OEBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016027858&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Rouessac, Francis Rouessac, Annick Chemical analysis modern instrumentation methods and techniques Química analítica instrumental larpcal Instrumental analysis Analytische Chemie (DE-588)4129906-1 gnd Instrumentelle Analytik (DE-588)4222592-9 gnd Methode (DE-588)4038971-6 gnd |
| subject_GND | (DE-588)4129906-1 (DE-588)4222592-9 (DE-588)4038971-6 |
| title | Chemical analysis modern instrumentation methods and techniques |
| title_alt | Analyse chimique |
| title_auth | Chemical analysis modern instrumentation methods and techniques |
| title_exact_search | Chemical analysis modern instrumentation methods and techniques |
| title_exact_search_txtP | Chemical analysis modern instrumentation methods and techniques |
| title_full | Chemical analysis modern instrumentation methods and techniques Francis Rouessac and Annick Rouessac |
| title_fullStr | Chemical analysis modern instrumentation methods and techniques Francis Rouessac and Annick Rouessac |
| title_full_unstemmed | Chemical analysis modern instrumentation methods and techniques Francis Rouessac and Annick Rouessac |
| title_short | Chemical analysis |
| title_sort | chemical analysis modern instrumentation methods and techniques |
| title_sub | modern instrumentation methods and techniques |
| topic | Química analítica instrumental larpcal Instrumental analysis Analytische Chemie (DE-588)4129906-1 gnd Instrumentelle Analytik (DE-588)4222592-9 gnd Methode (DE-588)4038971-6 gnd |
| topic_facet | Química analítica instrumental Instrumental analysis Analytische Chemie Instrumentelle Analytik Methode |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016027858&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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