Mass spectral and GC data of drugs, poisons, pesticides, pollutants and their metabolites: 1 Methods and tables
Gespeichert in:
| Hauptverfasser: | , , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH
2007
|
| Ausgabe: | 3., rev. and enl. ed. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XII, 199 S. |
| ISBN: | 9783527315383 |
Internformat
MARC
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| 245 | 1 | 0 | |a Mass spectral and GC data of drugs, poisons, pesticides, pollutants and their metabolites |n 1 |p Methods and tables |c Hans H. Maurer ; Karl Pfleger ; Armin A. Weber |
| 250 | |a 3., rev. and enl. ed. | ||
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| adam_text | HANS H. MAURER, KARL PFLEGER, ARMIN A. WEBER MASS SPECTRAL AND GC DATA
OF DRUGS, POISONS, PESTICIDES, POLLUTANTS AND THEIR METABOLITES VOLUME
1: METHODS AND TABLES THIRD, REVISED AND ENLARGED EDITION 1 8 O 7 WILEY
2 OO 7 WILEY-VCH VERLAG GMBH & CO. KGAA CONTENTS OF VOLUME 1 (METHODS,
TABLES) METHODS 1 INTRODUCTION 3 2 EXPERIMENTAL SECTION 4 2.1 ORIGIN AND
CHOICE OF SAMPLES 4 2.2 SAMPLE PREPARATION 4 2.2.1 STANDARD EXTRACTION
PROCEDURES 4 2.2.1.1 STANDARD LIQUID-LIQUID EXTRACTION (LLE) FOR PLASMA,
URINE OR GASTRIC CONTENTS (P, U, G) 4 2.2.1.2 STA PROCEDURE (HYDROLYSIS,
EXTRACTION AND MICROWAVE-ASSISTED ACETYLATION) FOR URINE (U+UHYAC) 5
2.2.1.3 EXTRACTION OF URINE AFTER CLEAVAGE OF CONJUGATES BY
GLUCURONIDASE AND ARYLSULFATASE (UGLUC) 5 2.2.1.4 EXTRACTIVE METHYLATION
PROCEDURE FOR URINE OR PLASMA (UME, PME) 5 2.2.1.5 SOLID-PHASE
EXTRACTION FOR PLASMA OR URINE (PSPE, USPE) 5 2.2.1.6 LLE OF PLASMA FOR
DETERMINATION OF DRUGS FOR BRAIN DEATH DIAGNOSIS 6 2.2.1.7 EXTRACTION OF
ETHYLENE GLYCOL AND OTHER GLYCOLS FROM PLASMA OR URINE FOLLOWED BY
MICROWAVE-ASSISTED PIVALYLATION (PEGPIV OR UEGPIV) 6 2.2.2
DERIVATIZATION PROCEDURES 6 2.2.2.1 ACETYLATION (AC) 7 2.2.2.2
METHYLATION (ME) 7 2.2.2.3 ETHYLATION (ET) 7 2.2.2.4
TERT.-BUTYLDIMETHYLSILYLATION (TBDMS) 7 2.2.2.5 TRIMETHYLSILYLATION
(TMS) 7 2.2.2.6 TRIMETHYLSILYLATION FOLLOWED BY TRIFLUOROACETYLATION
(TMSTFA) 7 2.2.2.7 TRIFLUOROACETYLATION (TFA) 7 2.2.2.8
PENTAFLUOROPROPIONYLATION (PFP) 7 2.2.2.9 PENTAFLUOROPROPYLATION (PFPOL)
7 2.2.2.10 HEPTAFLUOROBUTYRYLATION (HFB) 7 2.2.2.11 PIVALYLATION (PIV) 8
2.2.2.12 HEPTAFLUOROBUTYRYLPROLYLATION(HFBP) 8 2.3 GC-MS APPARATUS 8
2.3.1 APPARATUS AND OPERATION CONDITIONS 8 2.3.2 QUALITY ASSURANCE OF
THE APPARATUS PERFORMANCE 8 2.4 DETERMINATION OF RETENTION INDICES 10
2.5 SYSTEMATIC TOXICOLOGICAL ANALYSIS (STA) OF SEVERAL CLASSES OF DRUGS
AND THEIR METABOLITES BY GC-MS 10 2.5.1 SCREENING FOR 200 DRUGS IN BLOOD
PLASMA AFTER LLE 10 2.5.2 SCREENING FOR MOST OF THE BASIC AND NEUTRAL
DRUGS IN URINE AFTER ACID HYDROLYSIS, LLE AND ACETYLATION 10 2.5.3
SYSTEMATIC TOXICOLOGICAL ANALYSIS PROCEDURES FOR THE DETECTION OF ACIDIC
DRUGS AND/OR THEIR METABOLITES 14 2.5.4 GENERAL SCREENING PROCEDURE FOR
ZWITTERIONIC COMPOUNDS AFTER SPE AND SILYLATION 14 2.6 APPLICATION OF
THE ELECTRONIC VERSION OF THIS HANDBOOK 15 2.7 QUANTITATIVE
DETERMINATION 15 3 CORRELATION BETWEEN STRUCTURE AND FRAGMENTATION 16
3.1 PRINCIPLE OF ELECTRON-IONIZATION MASS SPECTROMETRY (EI-MS) 16 3.2
CORRELATION BETWEEN FUNDAMENTAL STRUCTURES OR SIDE CHAINS AND FRAGMENT
IONS 16 4 FORMATION OF ARTIFACTS 17 4.1 ARTIFACTS FORMED BY OXIDATION
DURING EXTRACTION WITH DIETHYL ETHER 17 4.1.1 N-OXIDATION OF TERTIARY
AMINES 17 4.1.2 S-OXIDATION OF PHENOTHIAZINES 1 7 4.2 ARTIFACTS FORMED
BY THERMOLYSIS DURING GC (GC ARTIFACT) 17 4.2.1 DECARBOXYLATION OF
CARBOXYLIC ACIDS 17 4.2.2 COPE ELIMINATION OF N-OXIDES (-(CH 3 ) 2 NOH,
-(C 2 H 5 ) 2 NOH, -C 6 H I4 N 2 O 2 ) 17 4.2.3 REARRANGEMENT OF
BIS-DEETHYL FLURAZEPAM (-H 2 O) 17 4.2.4 ELIMINATION OF VARIOUS RESIDUES
17 4.2.5 METHYLATION OF CARBOXYLIC ACIDS IN METHANOL ((ME), ME IN
METHANOL) 18 4.2.6 FORMATION OF FORMALDEHYDE ADDUCTS USING METHANOL AS
SOLVENT (GC ARTIFACT IN METHANOL) 18 4.3 ARTIFACTS FORMED BY THERMOLYSIS
DURING GC AND DURING ACID HYDROLYSIS (GC ARTIFACT, HY ARTIFACT) 18 4.3.1
DEHYDRATION OF ALCOHOLS (-H 2 O) 18 4.3.2 DECARBAMOYLATION OF CARBAMATES
18 4.3.3 CLEAVAGE OF MORAZONE TO PHENMETRAZINE 18 4.4 ARTIFACTS FORMED
DURING ACID HYDROLYSIS 18 4.4.1 CLEAVAGE OF THE ETHER BRIDGE IN
BETA-BLOCKERS AND ALKANOLAMINE ANTIHISTAMINES (H Y) 18 4.4.2 CLEAVAGE OF
1,4-BENZODIAZEPINES TO AMINOBENZOYL DERIVATIVES (HY) 18 4.4.3 CLEAVAGE
AND REARRANGEMENT OF N-DEMETHYL METABOLITES OF CLOBAZAM TO BENZIMIDAZOLE
DERIVATIVES (HY) 19 4.4.4 CLEAVAGE AND REARRANGEMENT OF BIS-DEETHYL
FLURAZEPAM (HY-H 2 O) 19 4.4.5 CLEAVAGE AND REARRANGEMENT OF TETRAZEPAM
AND ITS METABOLITES 19 4.4.6 DEALKYLATIONOF ETHYLENEDIAMINE
ANTIHISTAMINES (HY) 19 4.4.7 HYDRATIONOFA DOUBLE BOND (+H 2 O) 19 5
TABLE OF ATOMIC MASSES 20 6 ABBREVIATIONS 21 7 REFERENCES 24 TABLES 8
TABLE OF COMPOUNDS IN ORDER OF NAMES 35 8.1 EXPLANATORY NOTES 35 8.2
TABLE OF COMPOUNDS IN ORDER OF NAMES 37 9 TABLE OF COMPOUNDS IN ORDER OF
CATEGORIES 189 9.1 EXPLANATORY NOTES 189 9.2 TABLE OF COMPOUNDS IN ORDER
OF CATEGORIES 189
|
| adam_txt |
HANS H. MAURER, KARL PFLEGER, ARMIN A. WEBER MASS SPECTRAL AND GC DATA
OF DRUGS, POISONS, PESTICIDES, POLLUTANTS AND THEIR METABOLITES VOLUME
1: METHODS AND TABLES THIRD, REVISED AND ENLARGED EDITION 1 8 O 7 WILEY
2 OO 7 WILEY-VCH VERLAG GMBH & CO. KGAA CONTENTS OF VOLUME 1 (METHODS,
TABLES) METHODS 1 INTRODUCTION 3 2 EXPERIMENTAL SECTION 4 2.1 ORIGIN AND
CHOICE OF SAMPLES 4 2.2 SAMPLE PREPARATION 4 2.2.1 STANDARD EXTRACTION
PROCEDURES 4 2.2.1.1 STANDARD LIQUID-LIQUID EXTRACTION (LLE) FOR PLASMA,
URINE OR GASTRIC CONTENTS (P, U, G) 4 2.2.1.2 STA PROCEDURE (HYDROLYSIS,
EXTRACTION AND MICROWAVE-ASSISTED ACETYLATION) FOR URINE (U+UHYAC) 5
2.2.1.3 EXTRACTION OF URINE AFTER CLEAVAGE OF CONJUGATES BY
GLUCURONIDASE AND ARYLSULFATASE (UGLUC) 5 2.2.1.4 EXTRACTIVE METHYLATION
PROCEDURE FOR URINE OR PLASMA (UME, PME) 5 2.2.1.5 SOLID-PHASE
EXTRACTION FOR PLASMA OR URINE (PSPE, USPE) 5 2.2.1.6 LLE OF PLASMA FOR
DETERMINATION OF DRUGS FOR BRAIN DEATH DIAGNOSIS 6 2.2.1.7 EXTRACTION OF
ETHYLENE GLYCOL AND OTHER GLYCOLS FROM PLASMA OR URINE FOLLOWED BY
MICROWAVE-ASSISTED PIVALYLATION (PEGPIV OR UEGPIV) 6 2.2.2
DERIVATIZATION PROCEDURES 6 2.2.2.1 ACETYLATION (AC) 7 2.2.2.2
METHYLATION (ME) 7 2.2.2.3 ETHYLATION (ET) 7 2.2.2.4
TERT.-BUTYLDIMETHYLSILYLATION (TBDMS) 7 2.2.2.5 TRIMETHYLSILYLATION
(TMS) 7 2.2.2.6 TRIMETHYLSILYLATION FOLLOWED BY TRIFLUOROACETYLATION
(TMSTFA) 7 2.2.2.7 TRIFLUOROACETYLATION (TFA) 7 2.2.2.8
PENTAFLUOROPROPIONYLATION (PFP) 7 2.2.2.9 PENTAFLUOROPROPYLATION (PFPOL)
7 2.2.2.10 HEPTAFLUOROBUTYRYLATION (HFB) 7 2.2.2.11 PIVALYLATION (PIV) 8
2.2.2.12 HEPTAFLUOROBUTYRYLPROLYLATION(HFBP) 8 2.3 GC-MS APPARATUS 8
2.3.1 APPARATUS AND OPERATION CONDITIONS 8 2.3.2 QUALITY ASSURANCE OF
THE APPARATUS PERFORMANCE 8 2.4 DETERMINATION OF RETENTION INDICES 10
2.5 SYSTEMATIC TOXICOLOGICAL ANALYSIS (STA) OF SEVERAL CLASSES OF DRUGS
AND THEIR METABOLITES BY GC-MS 10 2.5.1 SCREENING FOR 200 DRUGS IN BLOOD
PLASMA AFTER LLE 10 2.5.2 SCREENING FOR MOST OF THE BASIC AND NEUTRAL
DRUGS IN URINE AFTER ACID HYDROLYSIS, LLE AND ACETYLATION 10 2.5.3
SYSTEMATIC TOXICOLOGICAL ANALYSIS PROCEDURES FOR THE DETECTION OF ACIDIC
DRUGS AND/OR THEIR METABOLITES 14 2.5.4 GENERAL SCREENING PROCEDURE FOR
ZWITTERIONIC COMPOUNDS AFTER SPE AND SILYLATION 14 2.6 APPLICATION OF
THE ELECTRONIC VERSION OF THIS HANDBOOK 15 2.7 QUANTITATIVE
DETERMINATION 15 3 CORRELATION BETWEEN STRUCTURE AND FRAGMENTATION 16
3.1 PRINCIPLE OF ELECTRON-IONIZATION MASS SPECTROMETRY (EI-MS) 16 3.2
CORRELATION BETWEEN FUNDAMENTAL STRUCTURES OR SIDE CHAINS AND FRAGMENT
IONS 16 4 FORMATION OF ARTIFACTS 17 4.1 ARTIFACTS FORMED BY OXIDATION
DURING EXTRACTION WITH DIETHYL ETHER 17 4.1.1 N-OXIDATION OF TERTIARY
AMINES 17 4.1.2 S-OXIDATION OF PHENOTHIAZINES 1 7 4.2 ARTIFACTS FORMED
BY THERMOLYSIS DURING GC (GC ARTIFACT) 17 4.2.1 DECARBOXYLATION OF
CARBOXYLIC ACIDS 17 4.2.2 COPE ELIMINATION OF N-OXIDES (-(CH 3 ) 2 NOH,
-(C 2 H 5 ) 2 NOH, -C 6 H I4 N 2 O 2 ) 17 4.2.3 REARRANGEMENT OF
BIS-DEETHYL FLURAZEPAM (-H 2 O) 17 4.2.4 ELIMINATION OF VARIOUS RESIDUES
17 4.2.5 METHYLATION OF CARBOXYLIC ACIDS IN METHANOL ((ME), ME IN
METHANOL) 18 4.2.6 FORMATION OF FORMALDEHYDE ADDUCTS USING METHANOL AS
SOLVENT (GC ARTIFACT IN METHANOL) 18 4.3 ARTIFACTS FORMED BY THERMOLYSIS
DURING GC AND DURING ACID HYDROLYSIS (GC ARTIFACT, HY ARTIFACT) 18 4.3.1
DEHYDRATION OF ALCOHOLS (-H 2 O) 18 4.3.2 DECARBAMOYLATION OF CARBAMATES
18 4.3.3 CLEAVAGE OF MORAZONE TO PHENMETRAZINE 18 4.4 ARTIFACTS FORMED
DURING ACID HYDROLYSIS 18 4.4.1 CLEAVAGE OF THE ETHER BRIDGE IN
BETA-BLOCKERS AND ALKANOLAMINE ANTIHISTAMINES (H Y) 18 4.4.2 CLEAVAGE OF
1,4-BENZODIAZEPINES TO AMINOBENZOYL DERIVATIVES (HY) 18 4.4.3 CLEAVAGE
AND REARRANGEMENT OF N-DEMETHYL METABOLITES OF CLOBAZAM TO BENZIMIDAZOLE
DERIVATIVES (HY) 19 4.4.4 CLEAVAGE AND REARRANGEMENT OF BIS-DEETHYL
FLURAZEPAM (HY-H 2 O) 19 4.4.5 CLEAVAGE AND REARRANGEMENT OF TETRAZEPAM
AND ITS METABOLITES 19 4.4.6 DEALKYLATIONOF ETHYLENEDIAMINE
ANTIHISTAMINES (HY) 19 4.4.7 HYDRATIONOFA DOUBLE BOND (+H 2 O) 19 5
TABLE OF ATOMIC MASSES 20 6 ABBREVIATIONS 21 7 REFERENCES 24 TABLES 8
TABLE OF COMPOUNDS IN ORDER OF NAMES 35 8.1 EXPLANATORY NOTES 35 8.2
TABLE OF COMPOUNDS IN ORDER OF NAMES 37 9 TABLE OF COMPOUNDS IN ORDER OF
CATEGORIES 189 9.1 EXPLANATORY NOTES 189 9.2 TABLE OF COMPOUNDS IN ORDER
OF CATEGORIES 189 |
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| id | DE-604.BV022550342 |
| illustrated | Not Illustrated |
| index_date | 2024-07-02T18:13:18Z |
| indexdate | 2024-07-09T21:00:03Z |
| institution | BVB |
| isbn | 9783527315383 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-015756669 |
| oclc_num | 315410234 |
| open_access_boolean | |
| owner | DE-703 DE-11 |
| owner_facet | DE-703 DE-11 |
| physical | XII, 199 S. |
| publishDate | 2007 |
| publishDateSearch | 2007 |
| publishDateSort | 2007 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Maurer, Hans H. 1950- Verfasser (DE-588)1051482097 aut Mass spectral and GC data of drugs, poisons, pesticides, pollutants and their metabolites 1 Methods and tables Hans H. Maurer ; Karl Pfleger ; Armin A. Weber 3., rev. and enl. ed. Weinheim Wiley-VCH 2007 XII, 199 S. txt rdacontent n rdamedia nc rdacarrier Gift (DE-588)4021007-8 gnd rswk-swf Metabolit (DE-588)4138579-2 gnd rswk-swf Arzneimittel (DE-588)4003115-9 gnd rswk-swf Massenspektrometrie (DE-588)4037882-2 gnd rswk-swf Massenspektrum (DE-588)4169044-8 gnd rswk-swf Massenspektrometrie (DE-588)4037882-2 s Arzneimittel (DE-588)4003115-9 s DE-604 Gift (DE-588)4021007-8 s Metabolit (DE-588)4138579-2 s Massenspektrum (DE-588)4169044-8 s Pfleger, Karl 1924-2013 Verfasser (DE-588)112566634X aut Weber, Armin Verfasser aut (DE-604)BV022550341 1 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=015756669&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Maurer, Hans H. 1950- Pfleger, Karl 1924-2013 Weber, Armin Mass spectral and GC data of drugs, poisons, pesticides, pollutants and their metabolites Gift (DE-588)4021007-8 gnd Metabolit (DE-588)4138579-2 gnd Arzneimittel (DE-588)4003115-9 gnd Massenspektrometrie (DE-588)4037882-2 gnd Massenspektrum (DE-588)4169044-8 gnd |
| subject_GND | (DE-588)4021007-8 (DE-588)4138579-2 (DE-588)4003115-9 (DE-588)4037882-2 (DE-588)4169044-8 |
| title | Mass spectral and GC data of drugs, poisons, pesticides, pollutants and their metabolites |
| title_auth | Mass spectral and GC data of drugs, poisons, pesticides, pollutants and their metabolites |
| title_exact_search | Mass spectral and GC data of drugs, poisons, pesticides, pollutants and their metabolites |
| title_exact_search_txtP | Mass spectral and GC data of drugs, poisons, pesticides, pollutants and their metabolites |
| title_full | Mass spectral and GC data of drugs, poisons, pesticides, pollutants and their metabolites 1 Methods and tables Hans H. Maurer ; Karl Pfleger ; Armin A. Weber |
| title_fullStr | Mass spectral and GC data of drugs, poisons, pesticides, pollutants and their metabolites 1 Methods and tables Hans H. Maurer ; Karl Pfleger ; Armin A. Weber |
| title_full_unstemmed | Mass spectral and GC data of drugs, poisons, pesticides, pollutants and their metabolites 1 Methods and tables Hans H. Maurer ; Karl Pfleger ; Armin A. Weber |
| title_short | Mass spectral and GC data of drugs, poisons, pesticides, pollutants and their metabolites |
| title_sort | mass spectral and gc data of drugs poisons pesticides pollutants and their metabolites methods and tables |
| topic | Gift (DE-588)4021007-8 gnd Metabolit (DE-588)4138579-2 gnd Arzneimittel (DE-588)4003115-9 gnd Massenspektrometrie (DE-588)4037882-2 gnd Massenspektrum (DE-588)4169044-8 gnd |
| topic_facet | Gift Metabolit Arzneimittel Massenspektrometrie Massenspektrum |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=015756669&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV022550341 |
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