Inorganic experiments:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH
2006
|
| Ausgabe: | 2., completely rev. and enl. ed., 1. reprint |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XXI, 377 S. graph. Darst. |
| ISBN: | 9783527305100 3527305106 |
Internformat
MARC
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| 245 | 1 | 0 | |a Inorganic experiments |c ed. by J. Derek Woollins |
| 250 | |a 2., completely rev. and enl. ed., 1. reprint | ||
| 264 | 1 | |a Weinheim |b Wiley-VCH |c 2006 | |
| 300 | |a XXI, 377 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 4 | |a Chemistry, Inorganic |x Experiments | |
| 650 | 0 | 7 | |a Anorganische Chemie |0 (DE-588)4002145-2 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Praktikum |0 (DE-588)4127380-1 |2 gnd |9 rswk-swf |
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| 689 | 0 | 1 | |a Praktikum |0 (DE-588)4127380-1 |D s |
| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a Woollins, J. Derek |e Sonstige |4 oth | |
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Datensatz im Suchindex
| _version_ | 1804136550712213504 |
|---|---|
| adam_text | CONTENTS
PREFACE
1 INTRODUCTION 1
1.1 INTRODUCTION 3
1.2 INTRODUCTION TO DISCOVERY ORIENTED/GROUP LEANING LABORATORY
EXPERIENCES 4
ALLEN
D. HUNTER
2 INTRODUCTORY EXPERIMENTS
7
2.1 PREPARATION AND INVESTIGATION OF SOME COORDINATION COMPOUNDS
9
RODERICK
D. CANNON AND MANFRED
BOCHMANN
2.2 GRAVIMETRIC ANALYSIS OF HEXAAMMINE NICKEL(II) TETRAFLUOROBORATE,
[NI(NH
3
)
6
](BF
4
)
2
12
RODERICK
D. CANNON AND MANFRED
BOCHMANN
2.3 ANALYSIS OF AN IRON(III) OXALATE COMPLEX
17
RODERICK
D. CANNON AND
MANFRED BOCHMANN
2.4 CHARACTERISATION OF A COPPER OXALATE COMPLEX K
FL
CU
FC
(C
2
0
4
)
C
* DH
2
0 22
ANDREW W. G.
PIATT
2.5 VANADIUM ALUM: AN EXPERIMENT IN
ELECTROSYNTHESIS
24
DAVID T.
RICHENS
2.6 AMMONIUM DICHROMATE, CHROMIUM(III) OXIDE,
POTASSIUM CHROMATE
AND POTASSIUM TETRAPEROXOCHROMATE (V)
27
ANTONIN
RUXICKA AND ZDIRAD
ZAK
2.7 LINKAGE ISOMERISM: AN INFRA-RED STUDY
31
DAVID T. RICHENS AND CHRISTOPHER
GLIDEWELL
2.8 PREPARATION AND COMPLEXATION OF
TRIS{3,5-DIMETHYLPYRAZOYL)HYDROBORATE
33
MANFRED
BOCHMANN
TETRAIODOTIN(IV) AND ITS TRIPHENYLPHOSPHINE COMPLEX
36
J. DEREK
WOOLUNS
SILICON OXYGEN COMPOUNDS AND
SILOXANE POLYMERS 38
PAUL D. LICKISS
PREPARATION AND NMR
IDENTIFICATION OF TWO
PHOSPHORUS ESTERS 42
CHRISTOPHER GLIDEWELL
THE PREPARATION OF POTASSIUM
PEROXODISULPHATE, K
2
S
2
0
8
44
ZDIRAD 2AK
AND ANTONIN
RUZICKA
K
2
ON (S0
3
)
2
(FREM/S SALT) AND [PH
3
PCH
2
C
6
H
4
CH
2
PPH
3
]ON (S0
3
)
2
47
DAVID
M. L.
GOODGAME
POLYIODIDES, ME
4
NI
X
49
ANDREW W. G.
PLATT
INTERHALOGEN COMPOUNDS 51
IVAN
P. PARKIN
SYNTHESIS AND INFRARED SPECTROSCOPIC CHARACTERISATION OF BORANES
AND GERMANES 56
IVAN
P. PARKIN
DEDUCTION OF THE COORDINATION MODE OF BH
4
IN BIS(TRIPHENYLPHOSPHINE)
COPPER(I) BOROHYDRIDE (PH
3
P)
2
CUBH
4
61
ANDREW W. G. PLATT
SYNTHESIS AND CHARACTERISATION OF A METAL HYDRIDE COMPLEX 64
ANDREW W. G. PLATT
PREPARATION AND IDENTIFICATION OF A COPPER(I) COMPLEX 66
ANDREW W.
G. PLATT
SYNTHESIS OF [NH
4
][BF
4
] AND SYNTHESIS AND TITRIMETRIC ANALYSIS
OF
[ZN(NH
3
)
4
][BF
4
]
2
68
MICHAEL A. BECKETT
IRON(II) AND LEAD(LL)
FORMATES 71
FRANCISCO J. ARNAIZ,
MARIA R. PEDROSA AND
RAFAEL AGUADO
PREPARATION OF COPPER(I) IODIDE 75
F. J. ARNAIZ,
M. R. PEDROSA
AND S. ARNAIZ
DISCOVERY RESEARCH WITH
SILOXANE CHEMISTRY 77
ALLEN
D. HUNTER
CONTENTS |
XI
3 INTERMEDIATE EXPERIMENTS 83
3.1 FERROCENE, (^
5
-C5H
5
)
2
FE, AND ITS DERIVATIVES
85
J. DEREK
WOOLLINS
3.2 THE USE OF ORGANOLITHIUM REAGENTS IN THE PREPARATION OF FERROCENE
DERIVATIVES 88
IAN
R. BUTLER
3.3 COMPLEXES OF IR-BONDING ARENE LIGANDS
95
ANDREW W. G. PLATT
3.4 ORGANOTIN CHEMISTRY 98
KIERAN C.
MOLLOY AND TIMOTHY T. PAGET
3.5 NICKEL CATALYSED CROSS-COUPLING OF ALKYLMAGNESIUM WITH HALOARENE
105
G. BRENT YOUNG
3.6 TRANSITION METAL CATALYSIS
109
NEIL M. BOAG
3.7 TRANSITION METAL-CARBON BONDS
IN CHEMISTRY AND BIOLOGY 113
C. J. JONES
3.8 COBALT COMPLEXES OF DIOXYGEN
124
DAVID T.
RICHENS AND CHRISTOPHER GLIDEWELL
3.9 PREPARATION OF NITROSYL COMPLEXES OF IRON AND
NICKEL 127
ANDREW W. G. PLAIT AND JOHN
F. GIBSON
3.10 PREPARATION OF AN IRON DINITROGEN COMPLEX
130
ANDREW W. G. PLAIT
3.11 NICKEL DIHALIDE PHOSPHINE COMPLEXES
132
IVAN
P. PARKIN
3.12 INFLUENCE OF LIGAND FIELD TETRAGONALITY ON THE GROUND-STATE SPIN OF
NICKEL(II) COMPLEXES 136
DAVID M. L. GOODGAME
3.13 PREPARATION OFTRANS-PTHCL{PPH
3
)
2
AND MEASUREMENT OF ITS
1
H,
31
PAND
195
PTNMR SPECTRA 139
WILLIAM
P. GRIFFITH
3.14 IDENTIFICATION OF STEREOCHEMICAL (GEOMETRICAL) ISOMERS OF [MO(CO)
4
(L)
2
]
BY INFRA-RED SPECTROSCOPY
143
MICHAEL A. BECKETT
3.15 FIVE COORDINATE COMPLEXES: [VO(ACAC)
2
]
AND [CR(NH
3
)
6
][CUCL
5
]
146
CHRISTOPHER P.
MORLEY
3.16 METAL ACETYLACETONATE COMPLEXES: PREPARATION AND CHARACTERISATION
149
CHRISTOPHER GLIDEWELL
XII
J CONTENTS
3.17 NICKEL(II) COMPLEXES OF SOME SCHIFFBASE LIGANDS
160
C. J. JONES
3.18 THE SYNTHESIS AND COORDINATION CHEMISTRY OF MACROCYCLIC
COMPLEXES 167
MARTIN
SCHRODER
3.19 SYNTHESIS AND REACTIVITY OF TERTIARY PHOSPHINES
172
NEIL M. BOAG
3.20 INORGANIC HETEROCYCLES: CYCLOPHOSPHAZENES 176
JOSEF
NOVOSAD AND MILAN
ALBERTI
3.21 INORGANIC (CARBON-FREE) CHELATE RINGS: A DITHIOIMIDODIPHOSPHINATO
LIGAND AND SOME OF ITS METAL COMPLEXES
179
LONEL HAIDUC
3.22 AMIDOSULFURIC ACID.TRISILVERAMIDOSULFATE MONOHYDRATE AND S0
3
* N(CH
3
)
3
COMPLEXES 184
ANTONIN
RUIICKA AND ZDIRAD !ZAK
3.23 FOUR METHODS FOR ANALYSING FIRST ORDER
KINETICS 188
VERONIQUE
PIMIENTA,
DOMINIQUE LAVABRE,
JEAN-CLAUDE
MICHEAU
AND GASTON
LEVY
3.24 INORGANIC (CARBON-FREE) CHELATE RINGS
II: ASYMMETRICAL MIXED-DONOR
P-N-P LIGAND AND ITS
PALLADIUM COMPLEX 194
DAVID J. BIRDSALL
AND JOSEF
NOVOSAD
3.25 [MO0
2
BR2(H
2
0)2] *
(DIGLYME) AND [MO0
2
BR
2
(DMF)
2
]
199
FRANCISCO J. ARNAIZ,
MARIA
R. PEDROSA
AND RAFAEL
AGUADO
3.26 NITRATION OF COBALT(III)ACETYLACETONATE 203
DAVID J.
OTWAY
3.27 [CO(DINOSAR)]CL
3
: AN ENCAPSULATION COMPLEX
PREPARED BY A TEMPLATE
REACTION 205
DAVID J. OTWAY
3.28 ANOMALOUS PARAMAGNETISM IN SOME IRON(III) CHELATES STUDIED BY THE
EVANS NMR
METHOD 208
DAVID J
OTWAY
3.29 SOLID SODIUM AMALGAM 211
ALLEN
D. HUNTER
3.30 DISCOVERY RESEARCH WITH CYCLOPENTADIENYL
IRON CARBONYL CHEMISTRY 214
ALLEN
D. HUNTER
3.31 DISCOVERY RESEARCH
WITH MODEL ONE-DIMENSIONAL ORGANOMETALLIC
MATERIALS OF NI, PD, ANDPT 222
ALLEN
D. HUNTER
CONTENTS |
XIII
4 ADVANCED
EXPERIMENTS 227
4.1 CHLOROTRIS(TERT-BUTYLIMIDO)MANGANESE(VII)
229
ANDREAS A. DANOPOULOS AND GEOFFREY
WILKINSON
4.2 2,2 :
6 ,2 -TERPYRIDINE COMPLEXES AND METAL DIRECTED
REACTIVITY 232
EDWIN C. CONSTABLE
4.3 ELECTRONIC CHARACTERISATION OF A TRANSITION-METAL COMPLEX USING
ELECTROCHEMICAL UV/VIS AND EPR TECHNIQUES
235
LESLEY J. YELLOWLEES
4.4 THE SYNTHESIS OF ^-ARENETRICARBONYL CHROMIUM(O) COMPLEXES
238
DAVID A. WIDDOWSON
4.5 MIGRATORY INSERTION
REACTIONS IN ORGANO TRANSITION-METAL CHEMISTRY
241
MARK
J. WINTER
4.6 ORGANOMETALLIC MOLYBDENUM COMPOUNDS
246
MANFRED BOCHMANN
AND PAUL
HAMMERTON
4.7 THE PREPARATION OF RAC-ETHYLENE-L,2-BIS(L-INDENYL)ZIRCONIUM
DICHLORIDE
AND DIBENZYL COMPLEXES 252
MANFRED BOCHMANN
AND SIMON
J. LANCASTER
4.8 HALFSANDWICH CARBONYL VANADIUM COMPLEXES
257
MAX
HERBERHOLD AND MATTHIAS
SCHREPFERMANN
4.9 COVALENT AND IONIC METALLOCENE HEXAFLUOROARSENATE COMPLEXES
263
INIS C. TORNIEPORTH-OETTING AND THOMAS
M. KLAPOTKE
4.10 PREPARATION OF THE IRON TRICARBONYL COMPLEX OF
METHYL-2-ACETAMIDOACRYLATE
266
SIMON
R. DRAKE,
M. ELENA
LASTERRA-SANCHEZ AND SUSAN
E. THOMAS
4.11 A TRANSITION-METAL ALKYLIDYNE COMPLEX
268
STEPHEN ANDERSON,
DARREN COOK
AND ANTHONY F.
HILL
4.12 PREPARATION OF IBU
4
NJ[B
3
H
8
] AND THE FORMATION OF
RUH[B
3
H
8
](CO)(PPH
3
)2
271
ANTHONY F.
HILL AND J. DEREK
WOOLLINS
4.13 VACUUM LINE TECHNIQUES: PREPARATION OF SIF
4
AND SIF
4
{C
5
H
5
N)
2
275
DENNIS F. EVANS AND J.
DEREK WOOLLINS
4.14 PREPARATION AND STRUCTURE OF THE ACETYL CHLORIDE-ANTIMONY
PENTACHLORIDE
COMPLEX 279
PETER
N. GATES
4.15 ARSENIUM CATIONS: CARBENE ANALOGUES 282
NEIL BURFORD AND TRENTON
M. PARKS
PREPARATION AND SOME REACTIONS OF THE FOLDED
P
2
N
4
S
2
RING 287
TRISTRAM
CHIVERS,
DANIEL D. DOXSEE AND ROBERT
W. HILTS
SULFUR-RICH HOMOCYCLES AND
HETEROCYCLES: TITANOCENE PENTASULFIDE,
CYC/O-HEPTASULFUR AND 1,2,3,4,5,6,7-HEPTATHIONANE
291
JORG ALBERTSEN
AND RALF
STEUDEL
REACTION OF ALKALI METAL POLYSELENIDES AND POLYTELLURIDES WITH GROUP 6
METAL CARBONYLS 295
JOSEPH W. KOLIS
SULPHUR-NITROGEN HETEROCYCLES AND [SNBR
0
.4]X POLYMER
300
}. DEREK
WOOLLINS
CHLOROTHIONITRENE AND CYDOTHIAZENO COMPLEXES OF TUNGSTEN 304
KURT DEHNICKE
SELENIUM-NITROGEN AND TELLURIUM-NITROGEN COMPOUNDS 307
HERBERT W.
ROESKY AND
JUDITH GINDL
NITRIDE CHLORIDES OF SELENIUM(III) AND SELENIUM(IV): SE
2
NCL
3
AND
SE
2
NCL
S
311
KURT DEHNICKE
STRUCTURAL, ELECTRICAL AND MAGNETIC PROPERTIES OF PEROVSKITE CERAMICS
315
COLIN
GREAVES
METAL-CONTAINING LIQUID
CRYSTALS. THE SYNTHESIS OF TRANS-BIS(4-ALKYL-4 -
CYANO-L.R-BIPHENYL)DICHLOROPLATINUM(II) AND RELATED
SPECIES-
THE USE OF MELT SYNTHESES 321
DUNCAN W. BRUCE
MAGNETOCHEMISTRY EXPERIMENTS: EXCHANGE COUPLING IN COPPER(II)-
NICKEL(II) BIMETALLIC COMPLEXES AND SPIN TRANSITION IN
IRON COMPLEXES
329
E. CORONADO AND J. J.
BORRAS-ALMENAR
N-FERROCENYL AMINE AND SOME REACTIVE DERIVATIVES
333
MAX HERBERHOLD,
HEIDI
E. MAISEL
AND BERND
WRACKMEYER
POLYOXOMOLYBDATE CLUSTERS: NANOSCOPIC WHEELS
AND BALLS 340
LEROY CRONIN,
EKKEHARD
DIEMANN AND ACHIM
MULLER
ONE-POT PREPARATION OF RU
3
(CO)
12
FROM RUCL
3
* 3 H
Z
O 347
GUY LAVIGNE,
CATHERINE
SACCAVINI AND
REMI
CHAUVIN
LOW TEMPERATURE SYNTHESIS OF BARIUM AMIDES AND PHENOXIDES
352
SIMON
R. DRAKE,
PHILIP HALL
AND DAVID
J. OTWAY
ALUMAZENE
- INORGANIC BENZENE ANALOG 357
JIRI
PINKAS
CONTENTS |
XV
4.31 COORDINATION CHEMISTRY OF ORGANIC FREE RADICALS: SYNTHESIS AND
MAGNETIC
PROPERTIES 360
A. ALBEROLA,
E. CORONADO AND
F. M. ROMERO
4.32 DISCOVERY RESEARCH WITH ARENE CHROMIUM TRICARBONYL CHEMISTRY
364
ALLEN
D. HUNTER
4.33 DISCOVERY RESEARCH WITH CR,
MO, AND W NITROSYL COMPLEXES: A MULTI-STEP
ORGANOMETALLIC SYNTHESIS 368
ALLEN
D. HUNTER
AND J.
D. WOOLLINS
SUBJECT INDEX 373
|
| adam_txt |
CONTENTS
PREFACE
1 INTRODUCTION 1
1.1 INTRODUCTION 3
1.2 INTRODUCTION TO DISCOVERY ORIENTED/GROUP LEANING LABORATORY
EXPERIENCES 4
ALLEN
D. HUNTER
2 INTRODUCTORY EXPERIMENTS
7
2.1 PREPARATION AND INVESTIGATION OF SOME COORDINATION COMPOUNDS
9
RODERICK
D. CANNON AND MANFRED
BOCHMANN
2.2 GRAVIMETRIC ANALYSIS OF HEXAAMMINE NICKEL(II) TETRAFLUOROBORATE,
[NI(NH
3
)
6
](BF
4
)
2
12
RODERICK
D. CANNON AND MANFRED
BOCHMANN
2.3 ANALYSIS OF AN IRON(III) OXALATE COMPLEX
17
RODERICK
D. CANNON AND
MANFRED BOCHMANN
2.4 CHARACTERISATION OF A COPPER OXALATE COMPLEX K
FL
CU
FC
(C
2
0
4
)
C
* DH
2
0 22
ANDREW W. G.
PIATT
2.5 VANADIUM ALUM: AN EXPERIMENT IN
ELECTROSYNTHESIS
24
DAVID T.
RICHENS
2.6 AMMONIUM DICHROMATE, CHROMIUM(III) OXIDE,
POTASSIUM CHROMATE
AND POTASSIUM TETRAPEROXOCHROMATE (V)
27
ANTONIN
RUXICKA AND ZDIRAD
ZAK
2.7 LINKAGE ISOMERISM: AN INFRA-RED STUDY
31
DAVID T. RICHENS AND CHRISTOPHER
GLIDEWELL
2.8 PREPARATION AND COMPLEXATION OF
TRIS{3,5-DIMETHYLPYRAZOYL)HYDROBORATE
33
MANFRED
BOCHMANN
TETRAIODOTIN(IV) AND ITS TRIPHENYLPHOSPHINE COMPLEX
36
J. DEREK
WOOLUNS
SILICON OXYGEN COMPOUNDS AND
SILOXANE POLYMERS 38
PAUL D. LICKISS
PREPARATION AND NMR
IDENTIFICATION OF TWO
PHOSPHORUS ESTERS 42
CHRISTOPHER GLIDEWELL
THE PREPARATION OF POTASSIUM
PEROXODISULPHATE, K
2
S
2
0
8
44
ZDIRAD 2AK
AND ANTONIN
RUZICKA
K
2
ON (S0
3
)
2
(FREM/S SALT) AND [PH
3
PCH
2
C
6
H
4
CH
2
PPH
3
]ON (S0
3
)
2
47
DAVID
M. L.
GOODGAME
POLYIODIDES, ME
4
NI
X
49
ANDREW W. G.
PLATT
INTERHALOGEN COMPOUNDS 51
IVAN
P. PARKIN
SYNTHESIS AND INFRARED SPECTROSCOPIC CHARACTERISATION OF BORANES
AND GERMANES 56
IVAN
P. PARKIN
DEDUCTION OF THE COORDINATION MODE OF BH
4
IN BIS(TRIPHENYLPHOSPHINE)
COPPER(I) BOROHYDRIDE (PH
3
P)
2
CUBH
4
61
ANDREW W. G. PLATT
SYNTHESIS AND CHARACTERISATION OF A METAL HYDRIDE COMPLEX 64
ANDREW W. G. PLATT
PREPARATION AND IDENTIFICATION OF A COPPER(I) COMPLEX 66
ANDREW W.
G. PLATT
SYNTHESIS OF [NH
4
][BF
4
] AND SYNTHESIS AND TITRIMETRIC ANALYSIS
OF
[ZN(NH
3
)
4
][BF
4
]
2
68
MICHAEL A. BECKETT
IRON(II) AND LEAD(LL)
FORMATES 71
FRANCISCO J. ARNAIZ,
MARIA R. PEDROSA AND
RAFAEL AGUADO
PREPARATION OF COPPER(I) IODIDE 75
F. J. ARNAIZ,
M. R. PEDROSA
AND S. ARNAIZ
DISCOVERY RESEARCH WITH
SILOXANE CHEMISTRY 77
ALLEN
D. HUNTER
CONTENTS |
XI
3 INTERMEDIATE EXPERIMENTS 83
3.1 FERROCENE, (^
5
-C5H
5
)
2
FE, AND ITS DERIVATIVES
85
J. DEREK
WOOLLINS
3.2 THE USE OF ORGANOLITHIUM REAGENTS IN THE PREPARATION OF FERROCENE
DERIVATIVES 88
IAN
R. BUTLER
3.3 COMPLEXES OF IR-BONDING ARENE LIGANDS
95
ANDREW W. G. PLATT
3.4 ORGANOTIN CHEMISTRY 98
KIERAN C.
MOLLOY AND TIMOTHY T. PAGET
3.5 NICKEL CATALYSED CROSS-COUPLING OF ALKYLMAGNESIUM WITH HALOARENE
105
G. BRENT YOUNG
3.6 TRANSITION METAL CATALYSIS
109
NEIL M. BOAG
3.7 TRANSITION METAL-CARBON BONDS
IN CHEMISTRY AND BIOLOGY 113
C. J. JONES
3.8 COBALT COMPLEXES OF DIOXYGEN
124
DAVID T.
RICHENS AND CHRISTOPHER GLIDEWELL
3.9 PREPARATION OF NITROSYL COMPLEXES OF IRON AND
NICKEL 127
ANDREW W. G. PLAIT AND JOHN
F. GIBSON
3.10 PREPARATION OF AN IRON DINITROGEN COMPLEX
130
ANDREW W. G. PLAIT
3.11 NICKEL DIHALIDE PHOSPHINE COMPLEXES
132
IVAN
P. PARKIN
3.12 INFLUENCE OF LIGAND FIELD TETRAGONALITY ON THE GROUND-STATE SPIN OF
NICKEL(II) COMPLEXES 136
DAVID M. L. GOODGAME
3.13 PREPARATION OFTRANS-PTHCL{PPH
3
)
2
AND MEASUREMENT OF ITS
1
H,
31
PAND
195
PTNMR SPECTRA 139
WILLIAM
P. GRIFFITH
3.14 IDENTIFICATION OF STEREOCHEMICAL (GEOMETRICAL) ISOMERS OF [MO(CO)
4
(L)
2
]
BY INFRA-RED SPECTROSCOPY
143
MICHAEL A. BECKETT
3.15 FIVE COORDINATE COMPLEXES: [VO(ACAC)
2
]
AND [CR(NH
3
)
6
][CUCL
5
]
146
CHRISTOPHER P.
MORLEY
3.16 METAL ACETYLACETONATE COMPLEXES: PREPARATION AND CHARACTERISATION
149
CHRISTOPHER GLIDEWELL
XII
J CONTENTS
3.17 NICKEL(II) COMPLEXES OF SOME SCHIFFBASE LIGANDS
160
C. J. JONES
3.18 THE SYNTHESIS AND COORDINATION CHEMISTRY OF MACROCYCLIC
COMPLEXES 167
MARTIN
SCHRODER
3.19 SYNTHESIS AND REACTIVITY OF TERTIARY PHOSPHINES
172
NEIL M. BOAG
3.20 INORGANIC HETEROCYCLES: CYCLOPHOSPHAZENES 176
JOSEF
NOVOSAD AND MILAN
ALBERTI
3.21 INORGANIC (CARBON-FREE) CHELATE RINGS: A DITHIOIMIDODIPHOSPHINATO
LIGAND AND SOME OF ITS METAL COMPLEXES
179
LONEL HAIDUC
3.22 AMIDOSULFURIC ACID.TRISILVERAMIDOSULFATE MONOHYDRATE AND S0
3
* N(CH
3
)
3
COMPLEXES 184
ANTONIN
RUIICKA AND ZDIRAD !ZAK
3.23 FOUR METHODS FOR ANALYSING FIRST ORDER
KINETICS 188
VERONIQUE
PIMIENTA,
DOMINIQUE LAVABRE,
JEAN-CLAUDE
MICHEAU
AND GASTON
LEVY
3.24 INORGANIC (CARBON-FREE) CHELATE RINGS
II: ASYMMETRICAL MIXED-DONOR
P-N-P LIGAND AND ITS
PALLADIUM COMPLEX 194
DAVID J. BIRDSALL
AND JOSEF
NOVOSAD
3.25 [MO0
2
BR2(H
2
0)2] *
(DIGLYME) AND [MO0
2
BR
2
(DMF)
2
]
199
FRANCISCO J. ARNAIZ,
MARIA
R. PEDROSA
AND RAFAEL
AGUADO
3.26 NITRATION OF COBALT(III)ACETYLACETONATE 203
DAVID J.
OTWAY
3.27 [CO(DINOSAR)]CL
3
: AN ENCAPSULATION COMPLEX
PREPARED BY A TEMPLATE
REACTION 205
DAVID J. OTWAY
3.28 ANOMALOUS PARAMAGNETISM IN SOME IRON(III) CHELATES STUDIED BY THE
EVANS NMR
METHOD 208
DAVID J
OTWAY
3.29 SOLID SODIUM AMALGAM 211
ALLEN
D. HUNTER
3.30 DISCOVERY RESEARCH WITH CYCLOPENTADIENYL
IRON CARBONYL CHEMISTRY 214
ALLEN
D. HUNTER
3.31 DISCOVERY RESEARCH
WITH MODEL ONE-DIMENSIONAL ORGANOMETALLIC
MATERIALS OF NI, PD, ANDPT 222
ALLEN
D. HUNTER
CONTENTS |
XIII
4 ADVANCED
EXPERIMENTS 227
4.1 CHLOROTRIS(TERT-BUTYLIMIDO)MANGANESE(VII)
229
ANDREAS A. DANOPOULOS AND GEOFFREY
WILKINSON
4.2 2,2':
6',2"-TERPYRIDINE COMPLEXES AND METAL DIRECTED
REACTIVITY 232
EDWIN C. CONSTABLE
4.3 ELECTRONIC CHARACTERISATION OF A TRANSITION-METAL COMPLEX USING
ELECTROCHEMICAL UV/VIS AND EPR TECHNIQUES
235
LESLEY J. YELLOWLEES
4.4 THE SYNTHESIS OF ^-ARENETRICARBONYL CHROMIUM(O) COMPLEXES
238
DAVID A. WIDDOWSON
4.5 MIGRATORY INSERTION
REACTIONS IN ORGANO TRANSITION-METAL CHEMISTRY
241
MARK
J. WINTER
4.6 ORGANOMETALLIC MOLYBDENUM COMPOUNDS
246
MANFRED BOCHMANN
AND PAUL
HAMMERTON
4.7 THE PREPARATION OF RAC-ETHYLENE-L,2-BIS(L-INDENYL)ZIRCONIUM
DICHLORIDE
AND DIBENZYL COMPLEXES 252
MANFRED BOCHMANN
AND SIMON
J. LANCASTER
4.8 HALFSANDWICH CARBONYL VANADIUM COMPLEXES
257
MAX
HERBERHOLD AND MATTHIAS
SCHREPFERMANN
4.9 COVALENT AND IONIC METALLOCENE HEXAFLUOROARSENATE COMPLEXES
263
INIS C. TORNIEPORTH-OETTING AND THOMAS
M. KLAPOTKE
4.10 PREPARATION OF THE IRON TRICARBONYL COMPLEX OF
METHYL-2-ACETAMIDOACRYLATE
266
SIMON
R. DRAKE,
M. ELENA
LASTERRA-SANCHEZ AND SUSAN
E. THOMAS
4.11 A TRANSITION-METAL ALKYLIDYNE COMPLEX
268
STEPHEN ANDERSON,
DARREN COOK
AND ANTHONY F.
HILL
4.12 PREPARATION OF IBU
4
NJ[B
3
H
8
] AND THE FORMATION OF
RUH[B
3
H
8
](CO)(PPH
3
)2
271
ANTHONY F.
HILL AND J. DEREK
WOOLLINS
4.13 VACUUM LINE TECHNIQUES: PREPARATION OF SIF
4
AND SIF
4
{C
5
H
5
N)
2
275
DENNIS F. EVANS AND J.
DEREK WOOLLINS
4.14 PREPARATION AND STRUCTURE OF THE ACETYL CHLORIDE-ANTIMONY
PENTACHLORIDE
COMPLEX 279
PETER
N. GATES
4.15 ARSENIUM CATIONS: CARBENE ANALOGUES 282
NEIL BURFORD AND TRENTON
M. PARKS
PREPARATION AND SOME REACTIONS OF THE FOLDED
P
2
N
4
S
2
RING 287
TRISTRAM
CHIVERS,
DANIEL D. DOXSEE AND ROBERT
W. HILTS
SULFUR-RICH HOMOCYCLES AND
HETEROCYCLES: TITANOCENE PENTASULFIDE,
CYC/O-HEPTASULFUR AND 1,2,3,4,5,6,7-HEPTATHIONANE
291
JORG ALBERTSEN
AND RALF
STEUDEL
REACTION OF ALKALI METAL POLYSELENIDES AND POLYTELLURIDES WITH GROUP 6
METAL CARBONYLS 295
JOSEPH W. KOLIS
SULPHUR-NITROGEN HETEROCYCLES AND [SNBR
0
.4]X POLYMER
300
}. DEREK
WOOLLINS
CHLOROTHIONITRENE AND CYDOTHIAZENO COMPLEXES OF TUNGSTEN 304
KURT DEHNICKE
SELENIUM-NITROGEN AND TELLURIUM-NITROGEN COMPOUNDS 307
HERBERT W.
ROESKY AND
JUDITH GINDL
NITRIDE CHLORIDES OF SELENIUM(III) AND SELENIUM(IV): SE
2
NCL
3
AND
SE
2
NCL
S
311
KURT DEHNICKE
STRUCTURAL, ELECTRICAL AND MAGNETIC PROPERTIES OF PEROVSKITE CERAMICS
315
COLIN
GREAVES
METAL-CONTAINING LIQUID
CRYSTALS. THE SYNTHESIS OF TRANS-BIS(4-ALKYL-4'-
CYANO-L.R-BIPHENYL)DICHLOROPLATINUM(II) AND RELATED
SPECIES-
THE USE OF MELT SYNTHESES 321
DUNCAN W. BRUCE
MAGNETOCHEMISTRY EXPERIMENTS: EXCHANGE COUPLING IN COPPER(II)-
NICKEL(II) BIMETALLIC COMPLEXES AND SPIN TRANSITION IN
IRON COMPLEXES
329
E. CORONADO AND J. J.
BORRAS-ALMENAR
N-FERROCENYL AMINE AND SOME REACTIVE DERIVATIVES
333
MAX HERBERHOLD,
HEIDI
E. MAISEL
AND BERND
WRACKMEYER
POLYOXOMOLYBDATE CLUSTERS: NANOSCOPIC WHEELS
AND BALLS 340
LEROY CRONIN,
EKKEHARD
DIEMANN AND ACHIM
MULLER
ONE-POT PREPARATION OF RU
3
(CO)
12
FROM RUCL
3
* 3 H
Z
O 347
GUY LAVIGNE,
CATHERINE
SACCAVINI AND
REMI
CHAUVIN
LOW TEMPERATURE SYNTHESIS OF BARIUM AMIDES AND PHENOXIDES
352
SIMON
R. DRAKE,
PHILIP HALL
AND DAVID
J. OTWAY
ALUMAZENE
- INORGANIC BENZENE ANALOG 357
JIRI
PINKAS
CONTENTS |
XV
4.31 COORDINATION CHEMISTRY OF ORGANIC FREE RADICALS: SYNTHESIS AND
MAGNETIC
PROPERTIES 360
A. ALBEROLA,
E. CORONADO AND
F. M. ROMERO
4.32 DISCOVERY RESEARCH WITH ARENE CHROMIUM TRICARBONYL CHEMISTRY
364
ALLEN
D. HUNTER
4.33 DISCOVERY RESEARCH WITH CR,
MO, AND W NITROSYL COMPLEXES: A MULTI-STEP
ORGANOMETALLIC SYNTHESIS 368
ALLEN
D. HUNTER
AND J.
D. WOOLLINS
SUBJECT INDEX 373 |
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| discipline_str_mv | Chemie / Pharmazie Chemie |
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| format | Book |
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| id | DE-604.BV022465708 |
| illustrated | Illustrated |
| index_date | 2024-07-02T17:42:17Z |
| indexdate | 2024-07-09T20:58:11Z |
| institution | BVB |
| isbn | 9783527305100 3527305106 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-015673301 |
| oclc_num | 254393534 |
| open_access_boolean | |
| owner | DE-703 DE-29T |
| owner_facet | DE-703 DE-29T |
| physical | XXI, 377 S. graph. Darst. |
| publishDate | 2006 |
| publishDateSearch | 2006 |
| publishDateSort | 2006 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Inorganic experiments ed. by J. Derek Woollins 2., completely rev. and enl. ed., 1. reprint Weinheim Wiley-VCH 2006 XXI, 377 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chemistry, Inorganic Experiments Anorganische Chemie (DE-588)4002145-2 gnd rswk-swf Praktikum (DE-588)4127380-1 gnd rswk-swf Anorganische Chemie (DE-588)4002145-2 s Praktikum (DE-588)4127380-1 s DE-604 Woollins, J. Derek Sonstige oth DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=015673301&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Inorganic experiments Chemistry, Inorganic Experiments Anorganische Chemie (DE-588)4002145-2 gnd Praktikum (DE-588)4127380-1 gnd |
| subject_GND | (DE-588)4002145-2 (DE-588)4127380-1 |
| title | Inorganic experiments |
| title_auth | Inorganic experiments |
| title_exact_search | Inorganic experiments |
| title_exact_search_txtP | Inorganic experiments |
| title_full | Inorganic experiments ed. by J. Derek Woollins |
| title_fullStr | Inorganic experiments ed. by J. Derek Woollins |
| title_full_unstemmed | Inorganic experiments ed. by J. Derek Woollins |
| title_short | Inorganic experiments |
| title_sort | inorganic experiments |
| topic | Chemistry, Inorganic Experiments Anorganische Chemie (DE-588)4002145-2 gnd Praktikum (DE-588)4127380-1 gnd |
| topic_facet | Chemistry, Inorganic Experiments Anorganische Chemie Praktikum |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=015673301&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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