Study of chemically reactive and non reactive mixtures with isocyanates: = Untersuchungen an chemisch reagierenden und nicht reagierenden Gemischen mit Isocyanaten
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Aachen
Shaker
2005
|
| Schriftenreihe: | Berichte aus der Thermodynamik
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | IX, 133 S. Ill., graph. Darst. 21 cm, 213 gr. |
| ISBN: | 3832243585 |
Internformat
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Datensatz im Suchindex
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| adam_text | STUDY OF CHEMICALLY REACTIVE AND NON REACTIVE MIXTURES WITH ISOCYANATES
UNTERSUCHUNGEN AN CHEMISCH REAGIERENDEN UND NICHT REAGIERENDEN GEMISCHEN
MIT ISOCYANATEN VON DER FAKULTAT DER MASCHINENWESEN DER RHEINISCH
-VVESTFALISCHEN TECHNISCHEN HOCHSCHULE AACHEN ZUR ERLANGUNG DES
AKADEMISCHEN GRADES EINES DOKTORS DER INGENIEURWISSENSCHAFTEN GENEHMIGTE
DISSERTATION VORGELEGT VON SUHEL AHMAD AUS BAHRAICH, INDIEN BERICHTER:
UNIVERSITATSPROFESSOR DR. -ING. KLAUS LUCAS UNIVERSITATSPROFESSOR DR.
-ING. KARL FRIEDRICH KNOCHE TAG DER MUNDLICHEN PRUFUNG: 22.02.2005
CONTENTS NOMENCLATURE VI KURZFASSUNG VTII ABSTRACT |X_ 1 INTRODUCTION L
2 EXPERIMENTAL SECTION 3 2.1 VAPOR PRESSURE MEASUREMENT AND SPECTROSCOPY
OF THE LIQUID PHASE 3 2.1.1 APPARATUS 3 2.1.2 VALIDATION OF VAPOR
PRESSURE MEASUREMENT 5 2.1.3 IR-SPECTROSCOPY 6 2.1.4 CALIBRATION OF THE
SPECTROMETER 7 2.1.5 PREPARATION OF SAMPLES 9 2.1.6 PROCEDURE OF THE
VAPOR PRESSURE AND SPECTROSCOPIC MEASUREMENTS 12 2.1.7 ERROR ANALYSIS OF
VAPOR PRESSURE AND SPECTROSCOPIC MEASUREMENTS 13 2.2 CALORIMETRIC
MEASUREMENTS 13 2.2.1 PRINCIPLE OF THELSOTHERMAL FLOW CALORIMETER 13
2.2.2 PROCEDURE FOR OBTAINING CALORIMETRIC DATA 15 2.2.3 EVALUATION OF
THE CALORIMETRIC DATA 18 2.2.4 VALIDATION OF CALORIMETRIC MEASUREMENTS
20 2.2.5 ERROR ANALYSIS OF CALORIMETRIC MEASUREMENTS 21 3 EXPERIMENTAL
RESULTS 22 3.1 P-T RESULTS FOR PURE SUBSTANCES 22 3.2 P-T-X RESULTS FOR
THE NON REACTIVE MIXTURES 25 3.2.1 N-BUTYLISOCYANATE + N-NONANE 25 3.2.2
N-BUTANOL + N-NONANE 25 3.2.3 BUTYL-CARBAMIC ACID BUTYL ESTER + N-NONANE
26 3.2.4 BUTYL-CARBAMIC ACID BUTYL ESTER + N-BUTANOL 26 3.2.5
BUTYL-CARBAMIC ACID BUTYL ESTER + N-BUTYLISOCYANATE 27 3.2.6
CYCLOHEXYLISOCYANATE + N-NONANE 27 3.2.7 CYCLOHEXYL-CARBAMIC ACID BUTYL
ESTER + N-NONANE 28 3.2.8 CYCLOHEXYL-CARBAMIC ACID BUTYL ESTER +
N-BUTANOL 28 3.2.9 CYCLOHEXYL-CARBAMIC ACID BUTYL ESTER +
CYCLOHEXYLISOCYANATE 29 3.3 P-T-X RESULTS FOR THE REACTIVE MIXTURES 30
3.3.1 N-BUTYLISOCYANATE + N-BUTANOL 30 3.3.2 CYCLOHEXYLISOCYANATE +
N-BUTANOL 30 3.4 RESULTS FOR THE ENTHALPY OF MIXING AND THE ENTHALPY OF
REACTION 31 3.4.1 N-BUTYLISOCYANATE + N-NONANE 31 3.4.2 N-BUTANOL +
N-NONANE 32 3.4.3 BUTYL-CARBAMIC ACID BUTYL ESTER + N-NONANE 32 3.4.4
BUTYL-CARBAMIC ACID BUTYL ESTER + N-BUTANOL 33 3.4.5 BUTYL-CARBAMIC ACID
BUTYL ESTER + N-BUTYLISOCYANATE 34 3.4.6 CYCLOHEXYLISOCYANATE + N-NONANE
34 3.4.7 CYCLOHEXYL-CARBAMIC ACID BUTYL ESTER + N-NONANE 35 3.4.8
CYCLOHEXYL-CARBAMIC ACID BUTYL ESTER + N-BUTANOL 36 3.4.9
CYCLOHEXYL-CARBAMIC ACID BUTYL ESTER + CYCLOHEXYLISOCYANATE 36 3.4.10
N-BUTYLISOCYANATE + N-BUTANOL 37 3.4.11 CYCLOHEXYLISOCYANATE + N-BUTANOL
38 4 THERMODYNAMIC MODELING 40 4.1 BASICS OF THERMODYNAMICS IN
MULTICOMPONENT SYSTEMS 40 4.2 NRTL MODEL 41 4.3 UNIQUAC MODEL 42 4.4
REDLICH-KISTER MODEL 44 5 EVALUATION OF VLE AND H E DATA USING
THERMODYNAMIC MODELS 45 5.1 SIMULTANEOUS FITTING OF THE VLE-AND H E DATA
USING THE NRTL MODEL 46 5.2 SIMULTANEOUS FITTING OF THE VLE-AND H E DATA
USING THE UNIQUAC MODEL 57 5.3 REACTIVE SYSTEMS 68 5.4 PREDICTION OF THE
VLE DATA OF TERNARY SYSTEMS 83 5.4.1 BUTYL-CARBAMIC ACID BUTYL ESTER +
N-BUTANOL + N-NONANE 83 5.4.2 CYCLOHEXYL-CARBAMIC ACID BUTYL ESTER +
N-BUTANOL + N-NONANE 83 5.5 DISCUSSION OF THE EXPERIMENTAL RESULTS 84 6
SUMMARY 86 APPENDIX 88 AL VAPOR PRESSURES OF PURE SUBSTANCES 87 A2
DESCRIPTION OF THE PLS MODEL AND DETERMINATION OF THE CONCENTRATION 90
A3 EXCESS ENTHALPY DATA FITTED WITH REDLICH-KISTER EQUATION 100 A4 VLE
AND H E DATA FITTED WITH NRTL AND UNIQUAC MODELS SIMULTANEOUSLY 108 A5
VLE DATA FOR TERNARY SYSTEMS 128 REFERENCES 130
|
| adam_txt |
STUDY OF CHEMICALLY REACTIVE AND NON REACTIVE MIXTURES WITH ISOCYANATES
UNTERSUCHUNGEN AN CHEMISCH REAGIERENDEN UND NICHT REAGIERENDEN GEMISCHEN
MIT ISOCYANATEN VON DER FAKULTAT DER MASCHINENWESEN DER RHEINISCH
-VVESTFALISCHEN TECHNISCHEN HOCHSCHULE AACHEN ZUR ERLANGUNG DES
AKADEMISCHEN GRADES EINES DOKTORS DER INGENIEURWISSENSCHAFTEN GENEHMIGTE
DISSERTATION VORGELEGT VON SUHEL AHMAD AUS BAHRAICH, INDIEN BERICHTER:
UNIVERSITATSPROFESSOR DR. -ING. KLAUS LUCAS UNIVERSITATSPROFESSOR DR.
-ING. KARL FRIEDRICH KNOCHE TAG DER MUNDLICHEN PRUFUNG: 22.02.2005
CONTENTS NOMENCLATURE VI KURZFASSUNG VTII ABSTRACT |X_ 1 INTRODUCTION L
2 EXPERIMENTAL SECTION 3 2.1 VAPOR PRESSURE MEASUREMENT AND SPECTROSCOPY
OF THE LIQUID PHASE 3 2.1.1 APPARATUS 3 2.1.2 VALIDATION OF VAPOR
PRESSURE MEASUREMENT 5 2.1.3 IR-SPECTROSCOPY 6 2.1.4 CALIBRATION OF THE
SPECTROMETER 7 2.1.5 PREPARATION OF SAMPLES 9 2.1.6 PROCEDURE OF THE
VAPOR PRESSURE AND SPECTROSCOPIC MEASUREMENTS 12 2.1.7 ERROR ANALYSIS OF
VAPOR PRESSURE AND SPECTROSCOPIC MEASUREMENTS 13 2.2 CALORIMETRIC
MEASUREMENTS 13 2.2.1 PRINCIPLE OF THELSOTHERMAL FLOW CALORIMETER 13
2.2.2 PROCEDURE FOR OBTAINING CALORIMETRIC DATA 15 2.2.3 EVALUATION OF
THE CALORIMETRIC DATA 18 2.2.4 VALIDATION OF CALORIMETRIC MEASUREMENTS
20 2.2.5 ERROR ANALYSIS OF CALORIMETRIC MEASUREMENTS 21 3 EXPERIMENTAL
RESULTS 22 3.1 P-T RESULTS FOR PURE SUBSTANCES 22 3.2 P-T-X RESULTS FOR
THE NON REACTIVE MIXTURES 25 3.2.1 N-BUTYLISOCYANATE + N-NONANE 25 3.2.2
N-BUTANOL + N-NONANE 25 3.2.3 BUTYL-CARBAMIC ACID BUTYL ESTER + N-NONANE
26 3.2.4 BUTYL-CARBAMIC ACID BUTYL ESTER + N-BUTANOL 26 3.2.5
BUTYL-CARBAMIC ACID BUTYL ESTER + N-BUTYLISOCYANATE 27 3.2.6
CYCLOHEXYLISOCYANATE + N-NONANE 27 3.2.7 CYCLOHEXYL-CARBAMIC ACID BUTYL
ESTER + N-NONANE 28 3.2.8 CYCLOHEXYL-CARBAMIC ACID BUTYL ESTER +
N-BUTANOL 28 3.2.9 CYCLOHEXYL-CARBAMIC ACID BUTYL ESTER +
CYCLOHEXYLISOCYANATE 29 3.3 P-T-X RESULTS FOR THE REACTIVE MIXTURES 30
3.3.1 N-BUTYLISOCYANATE + N-BUTANOL 30 3.3.2 CYCLOHEXYLISOCYANATE +
N-BUTANOL 30 3.4 RESULTS FOR THE ENTHALPY OF MIXING AND THE ENTHALPY OF
REACTION 31 3.4.1 N-BUTYLISOCYANATE + N-NONANE 31 3.4.2 N-BUTANOL +
N-NONANE 32 3.4.3 BUTYL-CARBAMIC ACID BUTYL ESTER + N-NONANE 32 3.4.4
BUTYL-CARBAMIC ACID BUTYL ESTER + N-BUTANOL 33 3.4.5 BUTYL-CARBAMIC ACID
BUTYL ESTER + N-BUTYLISOCYANATE 34 3.4.6 CYCLOHEXYLISOCYANATE + N-NONANE
34 3.4.7 CYCLOHEXYL-CARBAMIC ACID BUTYL ESTER + N-NONANE 35 3.4.8
CYCLOHEXYL-CARBAMIC ACID BUTYL ESTER + N-BUTANOL 36 3.4.9
CYCLOHEXYL-CARBAMIC ACID BUTYL ESTER + CYCLOHEXYLISOCYANATE 36 3.4.10
N-BUTYLISOCYANATE + N-BUTANOL 37 3.4.11 CYCLOHEXYLISOCYANATE + N-BUTANOL
38 4 THERMODYNAMIC MODELING 40 4.1 BASICS OF THERMODYNAMICS IN
MULTICOMPONENT SYSTEMS 40 4.2 NRTL MODEL 41 4.3 UNIQUAC MODEL 42 4.4
REDLICH-KISTER MODEL 44 5 EVALUATION OF VLE AND H E DATA USING
THERMODYNAMIC MODELS 45 5.1 SIMULTANEOUS FITTING OF THE VLE-AND H E DATA
USING THE NRTL MODEL 46 5.2 SIMULTANEOUS FITTING OF THE VLE-AND H E DATA
USING THE UNIQUAC MODEL 57 5.3 REACTIVE SYSTEMS 68 5.4 PREDICTION OF THE
VLE DATA OF TERNARY SYSTEMS 83 5.4.1 BUTYL-CARBAMIC ACID BUTYL ESTER +
N-BUTANOL + N-NONANE 83 5.4.2 CYCLOHEXYL-CARBAMIC ACID BUTYL ESTER +
N-BUTANOL + N-NONANE 83 5.5 DISCUSSION OF THE EXPERIMENTAL RESULTS 84 6
SUMMARY 86 APPENDIX 88 AL VAPOR PRESSURES OF PURE SUBSTANCES 87 A2
DESCRIPTION OF THE PLS MODEL AND DETERMINATION OF THE CONCENTRATION 90
A3 EXCESS ENTHALPY DATA FITTED WITH REDLICH-KISTER EQUATION 100 A4 VLE
AND H E DATA FITTED WITH NRTL AND UNIQUAC MODELS SIMULTANEOUSLY 108 A5
VLE DATA FOR TERNARY SYSTEMS 128 REFERENCES 130 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Ahmad, Suhel 1966- |
| author_GND | (DE-588)130360511 |
| author_facet | Ahmad, Suhel 1966- |
| author_role | aut |
| author_sort | Ahmad, Suhel 1966- |
| author_variant | s a sa |
| building | Verbundindex |
| bvnumber | BV021686915 |
| ctrlnum | (OCoLC)76121294 (DE-599)BVBBV021686915 |
| dewey-full | 660 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering |
| dewey-raw | 660 |
| dewey-search | 660 |
| dewey-sort | 3660 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie |
| discipline_str_mv | Chemie / Pharmazie |
| format | Thesis Book |
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| id | DE-604.BV021686915 |
| illustrated | Illustrated |
| index_date | 2024-07-02T15:13:12Z |
| indexdate | 2024-07-09T20:41:40Z |
| institution | BVB |
| isbn | 3832243585 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-014901032 |
| oclc_num | 76121294 |
| open_access_boolean | |
| owner | DE-91 DE-BY-TUM |
| owner_facet | DE-91 DE-BY-TUM |
| physical | IX, 133 S. Ill., graph. Darst. 21 cm, 213 gr. |
| publishDate | 2005 |
| publishDateSearch | 2005 |
| publishDateSort | 2005 |
| publisher | Shaker |
| record_format | marc |
| series2 | Berichte aus der Thermodynamik |
| spelling | Ahmad, Suhel 1966- Verfasser (DE-588)130360511 aut Study of chemically reactive and non reactive mixtures with isocyanates = Untersuchungen an chemisch reagierenden und nicht reagierenden Gemischen mit Isocyanaten Suhel Ahmad Untersuchungen an chemisch reagierenden und nicht reagierenden Gemischen mit Isocyanaten Aachen Shaker 2005 IX, 133 S. Ill., graph. Darst. 21 cm, 213 gr. txt rdacontent n rdamedia nc rdacarrier Berichte aus der Thermodynamik Zugl.: Aachen, Techn. Hochsch., Diss., 2005 Phasengleichgewicht (DE-588)4132145-5 gnd rswk-swf Isocyanate (DE-588)4162492-0 gnd rswk-swf Mehrstoffsystem (DE-588)4132152-2 gnd rswk-swf Mischungsenthalpie (DE-588)4253990-0 gnd rswk-swf Dampf-Flüssigkeit-Gemisch (DE-588)4264519-0 gnd rswk-swf Messung (DE-588)4038852-9 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Isocyanate (DE-588)4162492-0 s Mehrstoffsystem (DE-588)4132152-2 s Dampf-Flüssigkeit-Gemisch (DE-588)4264519-0 s Phasengleichgewicht (DE-588)4132145-5 s Messung (DE-588)4038852-9 s DE-604 Mischungsenthalpie (DE-588)4253990-0 s HEBIS Datenaustausch Darmstadt application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=014901032&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Ahmad, Suhel 1966- Study of chemically reactive and non reactive mixtures with isocyanates = Untersuchungen an chemisch reagierenden und nicht reagierenden Gemischen mit Isocyanaten Phasengleichgewicht (DE-588)4132145-5 gnd Isocyanate (DE-588)4162492-0 gnd Mehrstoffsystem (DE-588)4132152-2 gnd Mischungsenthalpie (DE-588)4253990-0 gnd Dampf-Flüssigkeit-Gemisch (DE-588)4264519-0 gnd Messung (DE-588)4038852-9 gnd |
| subject_GND | (DE-588)4132145-5 (DE-588)4162492-0 (DE-588)4132152-2 (DE-588)4253990-0 (DE-588)4264519-0 (DE-588)4038852-9 (DE-588)4113937-9 |
| title | Study of chemically reactive and non reactive mixtures with isocyanates = Untersuchungen an chemisch reagierenden und nicht reagierenden Gemischen mit Isocyanaten |
| title_alt | Untersuchungen an chemisch reagierenden und nicht reagierenden Gemischen mit Isocyanaten |
| title_auth | Study of chemically reactive and non reactive mixtures with isocyanates = Untersuchungen an chemisch reagierenden und nicht reagierenden Gemischen mit Isocyanaten |
| title_exact_search | Study of chemically reactive and non reactive mixtures with isocyanates = Untersuchungen an chemisch reagierenden und nicht reagierenden Gemischen mit Isocyanaten |
| title_exact_search_txtP | Study of chemically reactive and non reactive mixtures with isocyanates = Untersuchungen an chemisch reagierenden und nicht reagierenden Gemischen mit Isocyanaten |
| title_full | Study of chemically reactive and non reactive mixtures with isocyanates = Untersuchungen an chemisch reagierenden und nicht reagierenden Gemischen mit Isocyanaten Suhel Ahmad |
| title_fullStr | Study of chemically reactive and non reactive mixtures with isocyanates = Untersuchungen an chemisch reagierenden und nicht reagierenden Gemischen mit Isocyanaten Suhel Ahmad |
| title_full_unstemmed | Study of chemically reactive and non reactive mixtures with isocyanates = Untersuchungen an chemisch reagierenden und nicht reagierenden Gemischen mit Isocyanaten Suhel Ahmad |
| title_short | Study of chemically reactive and non reactive mixtures with isocyanates |
| title_sort | study of chemically reactive and non reactive mixtures with isocyanates untersuchungen an chemisch reagierenden und nicht reagierenden gemischen mit isocyanaten |
| title_sub | = Untersuchungen an chemisch reagierenden und nicht reagierenden Gemischen mit Isocyanaten |
| topic | Phasengleichgewicht (DE-588)4132145-5 gnd Isocyanate (DE-588)4162492-0 gnd Mehrstoffsystem (DE-588)4132152-2 gnd Mischungsenthalpie (DE-588)4253990-0 gnd Dampf-Flüssigkeit-Gemisch (DE-588)4264519-0 gnd Messung (DE-588)4038852-9 gnd |
| topic_facet | Phasengleichgewicht Isocyanate Mehrstoffsystem Mischungsenthalpie Dampf-Flüssigkeit-Gemisch Messung Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=014901032&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT ahmadsuhel studyofchemicallyreactiveandnonreactivemixtureswithisocyanatesuntersuchungenanchemischreagierendenundnichtreagierendengemischenmitisocyanaten AT ahmadsuhel untersuchungenanchemischreagierendenundnichtreagierendengemischenmitisocyanaten |