Neutron and x-ray spectroscopy:
Gespeichert in:
| Format: | Buch |
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| Sprache: | English |
| Veröffentlicht: |
Dordrecht
Springer
2006
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| Schriftenreihe: | Grenoble sciences
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XXIV, 566 S. Ill., graph. Darst. |
| ISBN: | 1402033370 9781402033377 9781402033360 1402033362 |
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| 650 | 4 | |a Spectroscopie des rayons X | |
| 650 | 4 | |a Neutrons |x Scattering | |
| 650 | 4 | |a Neutrons |x Spectra | |
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Datensatz im Suchindex
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| adam_text | NEUTRON AND X-RAY SPECTROSCOPY TU DARMSTADT TEILBIB!IOF H E E TABLE OF
CONTENTS CONTRIBUTORS XV FOREWORD XIX INTRODUCTION XXI X-RAY
SPECTROSCOPY 1 - FUNDAMENTALS OF X-RAY ABSORPTION AND DICHROISM: THE
MULTIPLET APPROACH F. DE GROOT-J. VOGEL 3 1. INTRODUCTION 4 1.1.
INTERACTION OF X-RAYS WITH MATTER 4 1.2. BASICS OF XAFS SPECTROSCOPY
...6 1.3. EXPERIMENTAL ASPECTS 9 2. MULTIPLET EFFECTS 11 2.1. ATOMIC
MULTIPLETS 14 2.1.1. TERM SYMBOLS 14 2.1.2. MATRIX ELEMENTS 18 2.2.
ATOMIC MULTIPLET GROUND STATES OF 3D SYSTEMS 20 2.3. J -J COUPLING 20
2.4. X-RAY ABSORPTION SPECTRA DESCRIBED WITH ATOMIC MULTIPLETS 21 2.4.1.
TRANSITION METAL //./// EDGE 21 2.4.2. M IV . V EDGES OF RARE EARTHS 28
3. CRYSTAL FIELD THEORY 31 3.1. THE CRYSTAL FIELD MULTIPLET HAMILTONIAN
32 3.2. CUBIC CRYSTAL FIELDS 33 3.3. THE ENERGIES OF THE 3D
CONFIGURATIONS 36 3.3.1. SYMMETRY EFFECTS IN D 4H SYMMETRY 40 3.3.2. THE
EFFECT OF THE 3D SPIN-ORBIT COUPLING. 40 3.3.3. THE EFFECTS ON THE X-RAY
ABSORPTION CALCULATIONS 42 3.3.4. 3D SYSTEMS IN OCTAHEDRAL SYMMETRY 42
3.3.5. 3D 0 SYSTEMS IN LOWER SYMMETRIES 45 3.3.6. X-RAY ABSORPTION
SPECTRA OF 3D SYSTEMS 46 4. CHARGE TRANSFER EFFECTS 47 4.1. INITIAL
STATE EFFECTS 47 4.2. FINAL STATE EFFECTS 52 4.3. THE X-RAY ABSORPTION
SPECTRUM WITH CHARGE TRANSFER EFFECTS 53 5. X-RAY LINEAR AND CIRCULAR
DICHROISM 59 REFERENCES 64 V VI NEUTRON AND X-RAY SPECTROSCOPY 2 -
MULTIPLE SCATTERING THEORY APPLIED TO X-RAY ABSORPTION NEAR-EDGE
STRUCTURE P. SAINCTAVIT - D. CABARET - V. BRIOIS 67 1. INTRODUCTION 67
2. MST FOR REAL SPACE CALCULATIONS 70 2.1. THE ABSORPTION CROSS-SECTION
; 71 2.2. CALCULATION OF THE CROSS-SECTION FOR THREE DIFFERENT
POTENTIALS 73 2.2.1. FREE PARTICLE 73 2.2.2. PARTICLE IN A SPHERICAL
POTENTIAL 75 2.2.3. PARTICLE IN A MUFFIN-TIN POTENTIAL 78 3.
CONSTRUCTION OF THE POTENTIAL 83 3.1. X-A EXCHANGE POTENTIAL 85 3.2.
DIRAC-HARA EXCHANGE POTENTIAL 85 3.3. COMPLEX HEDIN-LUNDQVIST EXCHANGE
AND CORRELATION POTENTIAL 87 4. APPLICATION OF THE MULTIPLE SCATTERING
THEORY 89 4.1. VANADIUM K EDGE CROSS-SECTION FOR VO 6 CLUSTER 90 4.2.
IRON K EDGE CROSS-SECTION FOR FEO^ CLUSTER 93 4.3. CROSS-SECTION
CALCULATIONS IN DISTORTED OCTAHEDRA 94 5. SPIN TRANSITION IN FE N
(O-PHENANTROLINE) 2 (NCS) 2 FOLLOWED AT THE IRON K EDGE 95 6. CONCLUSION
97 APPENDIX - EXPRESSION FOR THE PROPAGATORS J[[, AND H^J. 97
ACKNOWLEDGMENTS 99 REFERENCES 100 3 - X-RAY MAGNETIC CIRCULAR DICHROISM
F. BANDELET 103 1. INTRODUCTION 103 2. ORIGINS OF MAGNETIC CIRCULAR
DICHROISM 104 2.1. THEORETICAL ASPECTS: ROLE OF THE SPIN-ORBIT COUPLING
104 2.2. LIGHT POLARIZATION AND POLARIZATION-DEPENDENT SELECTION RULES
106 2.3. ORIGIN OF THE XMCD SIGNAL 108 2.3.1. HEURISTIC MODEL: LJ T - L
M EDGES OF TRANSITION METALS AND RARE EARTH ELEMENTS 108 2.3.2.
CALCULATION OFP E FOR THE L N - L M EDGES: P E (L U ) AND P E (L M ) 109
2.3.3. CALCULATION OFPJOR THE K - L, EDGES: P E (K) AND P/L,) 112 2.4.
MAGNITUDE OF THE XMCD SIGNAL 113 3. THE SUM RULES 114 4. XMCD SIGNAL AT
THE K EDGES (IS * P) 117 5. XMCD AND LOCALIZED MAGNETISM (MULTIPLET
APPROACH) 118 6. Z-II-III EDGES OF RARE EARTHS 121 7. MAGNETIC EXAFS 125
8. APPLICATION TO MULTILAYERS WITH GMR 126 9. STUDY OF HIGHLY CORRELATED
[CE/LA/FE] AND [LA/CE/FEL MULTILAYERS 127 REFERENCES 128 TABLE OF
CONTENTS VII 4 - EXTENDED X-RAY ABSORPTION FINE STRUCTURE B. LENGELER
. . 131 1. INTRODUCTION 131 2. X-RAY ABSORPTION IN ISOLATED ATOMS 133 3.
X-RAY ABSORPTION FINE STRUCTURE (XAFS) 136 3.1. X-RAY ABSORPTION FINE
STRUCTURE: THE BASIC FORMULA 136 3.2. CORRECTIONS TO THE BASIC EXAFS
FORMULA 141 3.2.1. SPHERICAL PHOTOELECTRON WAVE 142 3.2.2. MULTIPLE
SCATTERING 142 3.3. SET-UP FOR MEASURING X-RAY ABSORPTION 143 3.4. XAFS
DATA ANALYSIS 145 3.5. POSITION AND STRUCTURE OF THE ABSORPTION EDGE 149
4. SOME APPLICATIONS OF XAS 153 4.1. LATTICE DISTORTION AROUND
IMPURITIES IN DILUTE ALLOYS 154 4.2. PRECIPITATION IN IMMISCIBLE GIANT
MAGNETORESISTANCE AG]_ X NI X ALLOYS 155 4.3. LATTICE SITE LOCATION OF
VERY LIGHT ELEMENTS IN METALS BY XAFS 158 4.4. VALENCE OF IRIDIUM IN
ANODICALLY OXIDIZED IRIDIUM FILMS 160 4.5. COPPER-BASED METHANOL
SYNTHESIS CATALYST 163 4.6. COMBINED X-RAY ABSORPTION AND X-RAY
CRYSTALLOGRAPHY 165 REFERENCES 167 5 - INELASTIC X-RAY SCATTERING FROM
COLLECTIVE ATOM DYNAMICS F. SETTE - M. KRISCH 169 1. INTRODUCTION 169 2.
SCATTERING KINEMATICS AND INELASTIC X-RAY SCATTERING CROSS-SECTION 17 0
3. EXPERIMENTAL APPARATUS 175 4. THE FAST SOUND PHENOMENON IN LIQUID
WATER 179 5. DETERMINATION OF THE LONGITUDINAL SOUND VELOCITY IN IRON TO
110 GPA 182 6. CONCLUSIONS AND OUTLOOK 186 REFERENCES! 187 6 -
PHOTOELECTRON SPECTROSCOPY M. GRIONI 189 1. INTRODUCTION 189 2. WHAT IS
PHOTOEMISSION? 190 3. PHOTOEMISSION IN THE SINGLE-PARTICLE LIMIT- BAND
MAPPING 193 4. BEYOND THE SINGLE-PARTICLE APPROXIMATION 201 5. CASE
STUDIES 209 5.1. FERMI LIQUID LINESHAPE IN A NORMAL METAL 209 5.2. GAP
SPECTROSCOPY 215 5.3. ELECTRONIC INSTABILITIES IN LOW DIMENSIONS 220
5.4. SOME RECENT DEVELOPMENTS 229 6. CONCLUSIONS 235 REFERENCES 236 VIII
NEUTRON AND X-RAY SPECTROSCOPY 7 - ANOMALOUS SCATTERING AND DIFFRACTION
ANOMALOUS FINE STRUCTURE J.L. HODEAU - H. RENEVIER 239 1. ANOMALOUS
SCATTERING, ABSORPTION AND REFRACTION 240 2. THEORETICAL VERSUS
EXPERIMENTAL DETERMINATION OF ANOMALOUS CONTRIBUTION 24 1 3.
APPLICATIONS OF ANOMALOUS DISPERSION 244 3.1. STRUCTURE FACTOR PHASE
SOLUTION (MAD METHOD) 245 3.2. ELEMENT-SELECTIVE DIFFRACTION (CONTRAST
METHOD) 247 4. DIFFRACTION ANOMALOUS FINE STRUCTURE DATA ANALYSIS 249
4.1. DAFS AND EDAFS FORMALISM 251 4.1.1. SINGLE ANOMALOUS SITE ANALYSIS
252 4.1.2. MULTIPLE ANOMALOUS SITE ANALYSIS 253 4.2. DAFS AND EDAFS
DETERMINATION 255 4.3. DAFS AND DANES VALENCE DETERMINATION 258 4.4.
ANISOTROPY OF ANOMALOUS SCATTERING 260 5. REQUIREMENTS FOR ANOMALOUS
DIFFRACTION EXPERIMENTS 262 6. CONCLUSION 263 REFERENCES 264 8 - SOFT
X-RAY PHOTOELECTRON EMISSION MICROSCOPY (X-PEEM) CM. SCHNEIDER 271 1. A
NANOSCALE INTRODUCTION 271 2. VISUALIZING MICRO- AND NANOSTRUCTURES
271 3. TECHNICAL ASPECTS OF AN ELECTRON EMISSION MICROSCOPE (EEM) 273
3.1. ELECTRON-OPTICAL CONSIDERATIONS 273 3.2. TRANSMISSION AND LATERAL
RESOLUTION 275 4. NON-MAGNETIC IMAGE CONTRAST IN X-PEEM 276 4.1. PRIMARY
CONTRAST MECHANISMS 276 4.1.1. WORK FUNCTION CONTRAST 276 4.1.2.
CHEMICAL CONTRAST 277 4.2. SECONDARY CONTRAST MECHANISMS 280 5. MAGNETIC
CONTRAST IN X-PEEM 281 5.1. MAGNETIC X-RAY CIRCULAR DICHROISM (XMCD) 282
5.1.1. PHYSICS OF THE MAGNETIC CONTRAST MECHANISM 282 5.1.2. CONTRAST
ENHANCEMENT 284 5.1.3. ANGULAR DEPENDENCE OF THE IMAGE CONTRAST 285
5.1.4. MAGNETIC DOMAIN WALLS 286 5.1.5. INFORMATION DEPTH 288 5.2. X-RAY
MAGNETIC LINEAR DICHROISM (XMLD) 290 5.2.1. PROPERTIES OF THE CONTRAST
MECHANISM 290 5.2.2. IMAGING DOMAINS IN ANTIFERROMAGNETS 291 6.
CONCLUDING REMARKS 292 REFERENCES 293 TABLE OF CONTENTS IX 9 - X-RAY
INTENSITY FLUCTUATION SPECTROSCOPY M.SUTTON 297 1. INTRODUCTION 297 2.
MUTUAL COHERENCE FUNCTIONS 301 3. DIFFRACTION BY PARTIALLY COHERENT
SOURCES 304 4. KINETICS OF MATERIALS 308 5. X-RAY INTENSITY FLUCTUATION
SPECTROSCOPY 310 6. CONCLUSIONS 316 REFERENCES 317 10 - VIBRATIONAL
SPECTROSCOPY AT SURFACES AND INTERFACES USING SYNCHROTRON SOURCES AND
FREE ELECTRON LASERS A. TADJEDDINE - P. DUMAS 319 1. INTRODUCTION 319 2.
INFRARED SYNCHROTRON SOURCE AND FREE ELECTRON LASERS 321 2.1. INFRARED
SYNCHROTRON SOURCES 321 2.1.1. PRINCIPLES 321 2.1.2. EXTRACTION OF THE
IR BEAM FROM THE SYNCHROTRON RING 324 2.1.3. FOURIER TRANSFORM
INTERFEROMETER 324 2.2. NON LINEAR SURFACE SPECTROSCOPY WITH
CONVENTIONAL AND FREE ELECTRON LASERS 325 2.2.1. PRINCIPLE OF SFG 326
2.2.2. EXPERIMENTAL SFG SET-UP 328 2.2.3. THE CLIO-FEL INFRARED LASER
328 3. EXAMPLES OF APPLICATIONS IN SURFACE SCIENCE 331 3.1. SYNCHROTRON
INFRARED SPECTROSCOPY AT SURFACES 331 3.1.1. LOW FREQUENCY MODES OF
ADSORBED MOLECULES AND ATOMS 333 3.1.2. VIBRATIONAL DYNAMICS OF LOW
FREQUENCY MODES 335 3.2. SUM FREQUENCY AND DIFFERENCE FREQUENCY
GENERATION AT INTERFACES 339 3.2.1. IDENTIFICATION OF ADSORBED
INTERMEDIATE OF ELECTROCHEMICAL REACTIONS BY SFG 340 3.2.2. VIBRATIONAL
SPECTROSCOPY OF CYANIDE AT METAL-ELECTROLYTE INTERFACE 342 3.2.3.
VIBRATIONAL SPECTROSCOPY OF SELF-ASSEMBLED MONOLAYERS ON METAL SUBSTRATE
346 3.2.4. VIBRATIONAL SPECTROSCOPY OFFULLERENES C(,Q, ADSORBED ON AG(L
11), IN UHV ENVIRONMENT 348 3.2.5. ADSORPTION OF 4-CYANOPYRIDINE ON
AU(LLL) MONITORED BY SFG 352 4. CONCLUSION AND OUTLOOK 356 REFERENCES
356 X , NEUTRON AND X-RAY SPECTROSCOPY NEUTRON SPECTROSCOPY 11 -
INELASTIC NEUTRON SCATTERING: INTRODUCTION R. SCHERM - B. FDK 361 1.
INTERACTION OF NEUTRONS WITH MATTER 361 2. KINEMATICS 362 2.1. ENERGY
AND MOMENTUM CONSERVATION 362 2.2. SCATTERING TRIANGLE 363 2.3.
PARABOLAS 364 3. MASTER EQUATION AND S(Q,U ) 364 4. CORRELATION FUNCTION
366 5. COHERENT AND INCOHERENT SCATTERING 367 6. GENERAL PROPERTIES OF
S(Q,O) 369 6.1. DETAILED BALANCE 369 6.2. MOMENTS 370 6.3. TOTAL VERSUS
ELASTIC SCATTERING 371 7. MAGNETIC SCATTERING 372 8. RESPONSE FROM
SIMPLE SYSTEMS 373 8.1. EXAMPLES 373 8.2. RESPONSE FUNCTIONS 375 9.
INSTRUMENTATION 376 9.1. TAS 378 9.2. TOF 379 10. HOW TO BEAT STATISTICS
379 REFERENCES 380 12 - THREE-AXIS INELASTIC NEUTRON SCATTERING R.
CURRAT 383 1. PRINCIPLE OF THE TECHNIQUE 383 2. THE THREE-AXIS
SPECTROMETER 386 3. THE TOF VERSUS TAS CHOICE 391 4. WHAT DETERMINES THE
TAS COUNT RATE? 394 5. WHAT DETERMINES THE SIZE AND SHAPE OF THE
RESOLUTION FUNCTION? 396 6. DECOUPLING ENERGY AND MOMENTUM RESOLUTIONS:
DIRECT SPACE FOCUSING 400 7. TAS MULTIPLEXING 403 8. PHONON STUDIES WITH
TAS 408 9. THE INS VERSUS IXS CHOICE 412 10. MAGNETIC EXCITATION STUDIES
WITH TAS 415 11. PRACTICAL ASPECTS 420 12. SUMMARY AND OUTLOOK 422
REFERENCES 423 TABLE OF CONTENTS _ XI 13 - NEUTRON SPIN ECHO
SPECTROSCOPY R. CYWINSKI : 427 1. INTRODUCTION 427 2. POLARIZED NEUTRON
BEAMS, LARMOR PRECESSION AND SPIN FLIPPERS 428 3. GENERALIZED NEUTRON
SPIN ECHO 432 4. POLARIZATION DEPENDENT SCATTERING PROCESSES 436 5.
PRACTICALITIES: MEASUREMENT OF THE SPIN ECHO SIGNAL 440 6. APPLICATIONS
OF NEUTRON SPIN ECHO SPECTROSCOPY 444 6.1. SOFT CONDENSED MATTER 444
6.2. GLASSY DYNAMICS 447 6.3. SPIN RELAXATION IN MAGNETIC SYSTEMS 449 7.
CONCLUSIONS 453 BIBLIOGRAPHY 453 REFERENCES 454 14 - TIME-OF-FLIGHT
INELASTIC SCATTERING R.ECCLESTON 457 1. INTRODUCTION 457 2. CLASSES OF
TOF SPECTROMETERS 458 2.1. DISTANCE-TIME PLOTS 458 2.2. KINEMATIC RANGE
460 3. BEAMLINE COMPONENTS 461 3.1. CHOPPERS 461 3.1.1. FERMI CHOPPERS
462 3.1.2. DISK CHOPPERS 462 3.1.4. T=0CHOPPERS 462 3.2. MONOCHROMATING
AND ANALYZING CRYSTALS 463 3.3. FILTERS 463 3.4. DETECTORS 464 3.5.
NEUTRON GUIDES 464 3.6. POLARIZERS AND POLARIZATION ANALYSIS 465 4.
DIRECT GEOMETRY SPECTROMETERS 465 4.1. CHOPPER SPECTROMETER ON A PULSED
SOURCE 465 4.2! CHOPPER SPECTROMETERS ON A STEADY STATE SOURCE 466 4.3.
MULTI-CHOPPER TOF SPECTROMETERS 467 5. RESOLUTION AND SPECTROMETER
OPTIMIZATION 469 6. FLUX 470 7. RESOLUTION AS A FUNCTION OF ENERGY
TRANSFER AND EXPERIMENTAL CONSIDERATIONS 471 SINGLE CRYSTAL EXPERIMENTS
ON A CHOPPER SPECTROMETER 472 8. INDIRECT GEOMETRY SPECTROMETERS 474
8.1. THE RESOLUTION OF INDIRECT GEOMETRY SPECTROMETERS 475 8.2.
BACKSCATTERING SPECTROMETER 475 8.3. CRYSTAL ANALYZER SPECTROMETERS 477
XII NEUTRON AND X-RAY SPECTROSCOPY 8.4. DEEP INELASTIC NEUTRON
SCATTERING 478 8.5. COHERENT EXCITATIONS 479 9. CONCLUSIONS 480 FURTHER
INFORMATION 481 REFERENCES 481 15 - NEUTRON BACKSCATTERING SPECTROSCOPY
B. FRICK 483 1. INTRODUCTION 483 2. REFLECTION FROM PERFECT CRYSTALS AND
ITS ENERGY RESOLUTION 485 3. GENERIC BACKSCATTERING SPECTROMETER
CONCEPTS 488 3.1. NEUTRON OPTICS OF THE PRIMARY SPECTROMETERS OF
REACTOR-BS INSTRUMENTS 489 3.2. NEUTRON OPTICS OF THE PRIMARY
SPECTROMETER OF SPALLATION SOURCE-BS INSTRUMENTS ...493 3.3. SECONDARY
SPECTROMETER 493 4. TOTAL ENERGY RESOLUTION OF THE SPECTROMETERS 49 4 5.
HOW TO DO SPECTROSCOPY? 494 5.1. SPECTROSCOPY ON REACTOR BASED
INSTRUMENTS 494 5.2. SPECTROSCOPY ON SPALLATION SOURCE-BS INSTRUMENTS
497 6. MORE DETAILS ON OPTICAL COMPONENTS 498 6.1. BS MONOCHROMATORS AND
ANALYZERS 498 6.2. HOW TO OBTAIN THE BEST ENERGY RESOLUTION IN
BACKSCATTERING? 499 6.3. MOSAIC CRYSTAL DEFLECTORS AND PHASE SPACE
TRANSFORMER 500 6.4. NEUTRON GUIDES 503 6.5. HIGHER ORDER SUPPRESSION
503 6.6. G-RESOLUTION 504 6.7. A SECOND TIME THROUGH THE SAMPLE? 504 7.
EXAMPLES FOR BACKSCATTERING INSTRUMENTS 505 7.1. REACTOR INSTRUMENTS 505
7.2. SPALLATION SOURCE INSTRUMENTS 509 8. DATA TREATMENT 511 9. TYPICAL
MEASURING METHODS AND EXAMPLES 513 9.1. FIXED WINDOW SCANS 513 9.2.
SPECTROSCOPY 516 REFERENCES 525 16 - NEUTRON INELASTIC SCATTERING AND
MOLECULAR MODELLING M.R. JOHNSON - G.J. KEARLEY-H.P. TROMMSDORFF. 529 1.
INTRODUCTION 529 2. THEORY FRAMEWORK FOR TUNNELLING, VIBRATIONS AND
TOTAL ENERGY CALCULATIONS 532 2.1. HAMILTONIANS FOR QUANTUM TUNNELLING
532 2.2. THE DYNAMICAL MATRIX FOR MOLECULAR VIBRATIONS 536 2.3. TOTAL
ENERGY CALCULATIONS FOR DETERMINING PES AND FORCE CONSTANTS 538 3.
EXPERIMENTAL TECHNIQUES FOR MEASURING ROTATIONAL TUNNELLING AND
MOLECULAR VIBRATIONS 540 TABLE OF CONTENTS XIII 4. NUMERICAL SIMULATIONS
FOR UNDERSTANDING INS SPECTRA 544 4.1. SPM METHYL GROUP TUNNELLING 544
4.2. MULTI-DIMENSIONAL TUNNELLING DYNAMICS OF METHYL GROUPS 546 4.3.
VIBRATIONAL SPECTROSCOPY OF MOLECULAR CRYSTALS 547 5. DISCUSSION 551
REFERENCES 553 INDEX 557
|
| adam_txt |
NEUTRON AND X-RAY SPECTROSCOPY TU DARMSTADT TEILBIB!IOF H E E' TABLE OF
CONTENTS CONTRIBUTORS XV FOREWORD XIX INTRODUCTION XXI X-RAY
SPECTROSCOPY 1 - FUNDAMENTALS OF X-RAY ABSORPTION AND DICHROISM: THE
MULTIPLET APPROACH F. DE GROOT-J. VOGEL 3 1. INTRODUCTION 4 1.1.
INTERACTION OF X-RAYS WITH MATTER 4 1.2. BASICS OF XAFS SPECTROSCOPY
.6 1.3. EXPERIMENTAL ASPECTS 9 2. MULTIPLET EFFECTS 11 2.1. ATOMIC
MULTIPLETS 14 2.1.1. TERM SYMBOLS 14 2.1.2. MATRIX ELEMENTS 18 2.2.
ATOMIC MULTIPLET GROUND STATES OF 3D" SYSTEMS 20 2.3. J -J COUPLING 20
2.4. X-RAY ABSORPTION SPECTRA DESCRIBED WITH ATOMIC MULTIPLETS 21 2.4.1.
TRANSITION METAL //./// EDGE 21 2.4.2. M IV . V EDGES OF RARE EARTHS 28
3. CRYSTAL FIELD THEORY 31 3.1. THE CRYSTAL FIELD MULTIPLET HAMILTONIAN
32 3.2. CUBIC CRYSTAL FIELDS 33 3.3. THE ENERGIES OF THE 3D"
CONFIGURATIONS 36 3.3.1. SYMMETRY EFFECTS IN D 4H SYMMETRY 40 3.3.2. THE
EFFECT OF THE 3D SPIN-ORBIT COUPLING. 40 3.3.3. THE EFFECTS ON THE X-RAY
ABSORPTION CALCULATIONS 42 3.3.4. 3D SYSTEMS IN OCTAHEDRAL SYMMETRY 42
3.3.5. 3D 0 SYSTEMS IN LOWER SYMMETRIES 45 3.3.6. X-RAY ABSORPTION
SPECTRA OF 3D" SYSTEMS 46 4. CHARGE TRANSFER EFFECTS 47 4.1. INITIAL
STATE EFFECTS 47 4.2. FINAL STATE EFFECTS 52 4.3. THE X-RAY ABSORPTION
SPECTRUM WITH CHARGE TRANSFER EFFECTS 53 5. X-RAY LINEAR AND CIRCULAR
DICHROISM 59 REFERENCES 64 V VI NEUTRON AND X-RAY SPECTROSCOPY 2 -
MULTIPLE SCATTERING THEORY APPLIED TO X-RAY ABSORPTION NEAR-EDGE
STRUCTURE P. SAINCTAVIT - D. CABARET - V. BRIOIS 67 1. INTRODUCTION 67
2. MST FOR REAL SPACE CALCULATIONS 70 2.1. THE ABSORPTION CROSS-SECTION
; 71 2.2. CALCULATION OF THE CROSS-SECTION FOR THREE DIFFERENT
POTENTIALS 73 2.2.1. FREE PARTICLE 73 2.2.2. PARTICLE IN A SPHERICAL
POTENTIAL 75 2.2.3. PARTICLE IN A "MUFFIN-TIN"POTENTIAL 78 3.
CONSTRUCTION OF THE POTENTIAL 83 3.1. X-A EXCHANGE POTENTIAL 85 3.2.
DIRAC-HARA EXCHANGE POTENTIAL 85 3.3. COMPLEX HEDIN-LUNDQVIST EXCHANGE
AND CORRELATION POTENTIAL 87 4. APPLICATION OF THE MULTIPLE SCATTERING
THEORY 89 4.1. VANADIUM K EDGE CROSS-SECTION FOR VO 6 CLUSTER 90 4.2.
IRON K EDGE CROSS-SECTION FOR FEO^ CLUSTER 93 4.3. CROSS-SECTION
CALCULATIONS IN DISTORTED OCTAHEDRA 94 5. SPIN TRANSITION IN FE N
(O-PHENANTROLINE) 2 (NCS) 2 FOLLOWED AT THE IRON K EDGE 95 6. CONCLUSION
97 APPENDIX - EXPRESSION FOR THE PROPAGATORS J[[, AND H^J. 97
ACKNOWLEDGMENTS 99 REFERENCES 100 3 - X-RAY MAGNETIC CIRCULAR DICHROISM
F. BANDELET 103 1. INTRODUCTION 103 2. ORIGINS OF MAGNETIC CIRCULAR
DICHROISM 104 2.1. THEORETICAL ASPECTS: ROLE OF THE SPIN-ORBIT COUPLING
104 2.2. LIGHT POLARIZATION AND POLARIZATION-DEPENDENT SELECTION RULES
106 2.3. ORIGIN OF THE XMCD SIGNAL 108 2.3.1. HEURISTIC MODEL: LJ T - L
M EDGES OF TRANSITION METALS AND RARE EARTH ELEMENTS 108 2.3.2.
CALCULATION OFP E FOR THE L N - L M EDGES: P E (L U ) AND P E (L M ) 109
2.3.3. CALCULATION OFPJOR THE K - L, EDGES: P E (K) AND P/L,) 112 2.4.
MAGNITUDE OF THE XMCD SIGNAL 113 3. THE SUM RULES 114 4. XMCD SIGNAL AT
THE K EDGES (IS * P) 117 5. XMCD AND LOCALIZED MAGNETISM (MULTIPLET
APPROACH) 118 6. Z-II-III EDGES OF RARE EARTHS 121 7. MAGNETIC EXAFS 125
8. APPLICATION TO MULTILAYERS WITH GMR 126 9. STUDY OF HIGHLY CORRELATED
[CE/LA/FE] AND [LA/CE/FEL MULTILAYERS 127 REFERENCES 128 TABLE OF
CONTENTS VII 4 - EXTENDED X-RAY ABSORPTION FINE STRUCTURE B. LENGELER
.'. 131 1. INTRODUCTION 131 2. X-RAY ABSORPTION IN ISOLATED ATOMS 133 3.
X-RAY ABSORPTION FINE STRUCTURE (XAFS) 136 3.1. X-RAY ABSORPTION FINE
STRUCTURE: THE BASIC FORMULA 136 3.2. CORRECTIONS TO THE BASIC EXAFS
FORMULA 141 3.2.1. SPHERICAL PHOTOELECTRON WAVE 142 3.2.2. MULTIPLE
SCATTERING 142 3.3. SET-UP FOR MEASURING X-RAY ABSORPTION 143 3.4. XAFS
DATA ANALYSIS 145 3.5. POSITION AND STRUCTURE OF THE ABSORPTION EDGE 149
4. SOME APPLICATIONS OF XAS 153 4.1. LATTICE DISTORTION AROUND
IMPURITIES IN DILUTE ALLOYS 154 4.2. PRECIPITATION IN IMMISCIBLE GIANT
MAGNETORESISTANCE AG]_ X NI X ALLOYS 155 4.3. LATTICE SITE LOCATION OF
VERY LIGHT ELEMENTS IN METALS BY XAFS 158 4.4. VALENCE OF IRIDIUM IN
ANODICALLY OXIDIZED IRIDIUM FILMS 160 4.5. COPPER-BASED METHANOL
SYNTHESIS CATALYST 163 4.6. COMBINED X-RAY ABSORPTION AND X-RAY
CRYSTALLOGRAPHY 165 REFERENCES 167 5 - INELASTIC X-RAY SCATTERING FROM
COLLECTIVE ATOM DYNAMICS F. SETTE - M. KRISCH 169 1. INTRODUCTION 169 2.
SCATTERING KINEMATICS AND INELASTIC X-RAY SCATTERING CROSS-SECTION 17 0
3. EXPERIMENTAL APPARATUS 175 4. THE "FAST SOUND" PHENOMENON IN LIQUID
WATER 179 5. DETERMINATION OF THE LONGITUDINAL SOUND VELOCITY IN IRON TO
110 GPA 182 6. CONCLUSIONS AND OUTLOOK 186 REFERENCES! 187 6 -
PHOTOELECTRON SPECTROSCOPY M. GRIONI 189 1. INTRODUCTION 189 2. WHAT IS
PHOTOEMISSION? 190 3. PHOTOEMISSION IN THE SINGLE-PARTICLE LIMIT- BAND
MAPPING 193 4. BEYOND THE SINGLE-PARTICLE APPROXIMATION 201 5. CASE
STUDIES 209 5.1. FERMI LIQUID LINESHAPE IN A NORMAL METAL 209 5.2. GAP
SPECTROSCOPY 215 5.3. ELECTRONIC INSTABILITIES IN LOW DIMENSIONS 220
5.4. SOME RECENT DEVELOPMENTS 229 6. CONCLUSIONS 235 REFERENCES 236 VIII
NEUTRON AND X-RAY SPECTROSCOPY 7 - ANOMALOUS SCATTERING AND DIFFRACTION
ANOMALOUS FINE STRUCTURE J.L. HODEAU - H. RENEVIER 239 1. ANOMALOUS
SCATTERING, ABSORPTION AND REFRACTION 240 2. THEORETICAL VERSUS
EXPERIMENTAL DETERMINATION OF ANOMALOUS CONTRIBUTION 24 1 3.
APPLICATIONS OF ANOMALOUS DISPERSION 244 3.1. STRUCTURE FACTOR PHASE
SOLUTION (MAD METHOD) 245 3.2. ELEMENT-SELECTIVE DIFFRACTION (CONTRAST
METHOD) 247 4. DIFFRACTION ANOMALOUS FINE STRUCTURE DATA ANALYSIS 249
4.1. DAFS AND EDAFS FORMALISM 251 4.1.1. SINGLE ANOMALOUS SITE ANALYSIS
252 4.1.2. MULTIPLE ANOMALOUS SITE ANALYSIS 253 4.2. DAFS AND EDAFS
DETERMINATION 255 4.3. DAFS AND DANES VALENCE DETERMINATION 258 4.4.
ANISOTROPY OF ANOMALOUS SCATTERING 260 5. REQUIREMENTS FOR ANOMALOUS
DIFFRACTION EXPERIMENTS 262 6. CONCLUSION 263 REFERENCES 264 8 - SOFT
X-RAY PHOTOELECTRON EMISSION MICROSCOPY (X-PEEM) CM. SCHNEIDER 271 1. A
"NANOSCALE" INTRODUCTION 271 2. VISUALIZING MICRO- AND NANOSTRUCTURES
271 3. TECHNICAL ASPECTS OF AN ELECTRON EMISSION MICROSCOPE (EEM) 273
3.1. ELECTRON-OPTICAL CONSIDERATIONS 273 3.2. TRANSMISSION AND LATERAL
RESOLUTION 275 4. NON-MAGNETIC IMAGE CONTRAST IN X-PEEM 276 4.1. PRIMARY
CONTRAST MECHANISMS 276 4.1.1. WORK FUNCTION CONTRAST 276 4.1.2.
CHEMICAL CONTRAST 277 4.2. SECONDARY CONTRAST MECHANISMS 280 5. MAGNETIC
CONTRAST IN X-PEEM 281 5.1. MAGNETIC X-RAY CIRCULAR DICHROISM (XMCD) 282
5.1.1. PHYSICS OF THE MAGNETIC CONTRAST MECHANISM 282 5.1.2. CONTRAST
ENHANCEMENT 284 5.1.3. ANGULAR DEPENDENCE OF THE IMAGE CONTRAST 285
5.1.4. MAGNETIC DOMAIN WALLS 286 5.1.5. INFORMATION DEPTH 288 5.2. X-RAY
MAGNETIC LINEAR DICHROISM (XMLD) 290 5.2.1. PROPERTIES OF THE CONTRAST
MECHANISM 290 5.2.2. IMAGING DOMAINS IN ANTIFERROMAGNETS 291 6.
CONCLUDING REMARKS 292 REFERENCES 293 TABLE OF CONTENTS IX 9 - X-RAY
INTENSITY FLUCTUATION SPECTROSCOPY M.SUTTON 297 1. INTRODUCTION 297 2.
MUTUAL COHERENCE FUNCTIONS 301 3. DIFFRACTION BY PARTIALLY COHERENT
SOURCES 304 4. KINETICS OF MATERIALS 308 5. X-RAY INTENSITY FLUCTUATION
SPECTROSCOPY 310 6. CONCLUSIONS 316 REFERENCES 317 10 - VIBRATIONAL
SPECTROSCOPY AT SURFACES AND INTERFACES USING SYNCHROTRON SOURCES AND
FREE ELECTRON LASERS A. TADJEDDINE - P. DUMAS 319 1. INTRODUCTION 319 2.
INFRARED SYNCHROTRON SOURCE AND FREE ELECTRON LASERS 321 2.1. INFRARED
SYNCHROTRON SOURCES 321 2.1.1. PRINCIPLES 321 2.1.2. EXTRACTION OF THE
IR BEAM FROM THE SYNCHROTRON RING 324 2.1.3. FOURIER TRANSFORM
INTERFEROMETER 324 2.2. NON LINEAR SURFACE SPECTROSCOPY WITH
CONVENTIONAL AND FREE ELECTRON LASERS 325 2.2.1. PRINCIPLE OF SFG 326
2.2.2. EXPERIMENTAL SFG SET-UP 328 2.2.3. THE CLIO-FEL INFRARED LASER
328 3. EXAMPLES OF APPLICATIONS IN SURFACE SCIENCE 331 3.1. SYNCHROTRON
INFRARED SPECTROSCOPY AT SURFACES 331 3.1.1. LOW FREQUENCY MODES OF
ADSORBED MOLECULES AND ATOMS 333 3.1.2. VIBRATIONAL DYNAMICS OF LOW
FREQUENCY MODES 335 3.2. SUM FREQUENCY AND DIFFERENCE FREQUENCY
GENERATION AT INTERFACES 339 3.2.1. IDENTIFICATION OF ADSORBED
INTERMEDIATE OF ELECTROCHEMICAL REACTIONS BY SFG 340 3.2.2. VIBRATIONAL
SPECTROSCOPY OF CYANIDE AT METAL-ELECTROLYTE INTERFACE 342 3.2.3.
VIBRATIONAL SPECTROSCOPY OF SELF-ASSEMBLED MONOLAYERS ON METAL SUBSTRATE
346 3.2.4. VIBRATIONAL SPECTROSCOPY OFFULLERENES C(,Q, ADSORBED ON AG(L
11), IN UHV ENVIRONMENT 348 3.2.5. ADSORPTION OF 4-CYANOPYRIDINE ON
AU(LLL) MONITORED BY SFG 352 4. CONCLUSION AND OUTLOOK 356 REFERENCES
356 X , NEUTRON AND X-RAY SPECTROSCOPY NEUTRON SPECTROSCOPY 11 -
INELASTIC NEUTRON SCATTERING: INTRODUCTION R. SCHERM - B. FDK 361 1.
INTERACTION OF NEUTRONS WITH MATTER 361 2. KINEMATICS 362 2.1. ENERGY
AND MOMENTUM CONSERVATION 362 2.2. SCATTERING TRIANGLE 363 2.3.
PARABOLAS 364 3. MASTER EQUATION AND S(Q,U ) 364 4. CORRELATION FUNCTION
366 5. COHERENT AND INCOHERENT SCATTERING 367 6. GENERAL PROPERTIES OF
S(Q,O) 369 6.1. DETAILED BALANCE 369 6.2. MOMENTS 370 6.3. TOTAL VERSUS
ELASTIC SCATTERING 371 7. MAGNETIC SCATTERING 372 8. RESPONSE FROM
SIMPLE SYSTEMS 373 8.1. EXAMPLES 373 8.2. RESPONSE FUNCTIONS 375 9.
INSTRUMENTATION 376 9.1. TAS 378 9.2. TOF 379 10. HOW TO BEAT STATISTICS
379 REFERENCES 380 12 - THREE-AXIS INELASTIC NEUTRON SCATTERING R.
CURRAT 383 1. PRINCIPLE OF THE TECHNIQUE 383 2. THE THREE-AXIS
SPECTROMETER 386 3. THE TOF VERSUS TAS CHOICE 391 4. WHAT DETERMINES THE
TAS COUNT RATE? 394 5. WHAT DETERMINES THE SIZE AND SHAPE OF THE
RESOLUTION FUNCTION? 396 6. DECOUPLING ENERGY AND MOMENTUM RESOLUTIONS:
DIRECT SPACE FOCUSING 400 7. TAS MULTIPLEXING 403 8. PHONON STUDIES WITH
TAS 408 9. THE INS VERSUS IXS CHOICE 412 10. MAGNETIC EXCITATION STUDIES
WITH TAS 415 11. PRACTICAL ASPECTS 420 12. SUMMARY AND OUTLOOK 422
REFERENCES 423 TABLE OF CONTENTS _ XI 13 - NEUTRON SPIN ECHO
SPECTROSCOPY R. CYWINSKI : 427 1. INTRODUCTION 427 2. POLARIZED NEUTRON
BEAMS, LARMOR PRECESSION AND SPIN FLIPPERS 428 3. GENERALIZED NEUTRON
SPIN ECHO 432 4. POLARIZATION DEPENDENT SCATTERING PROCESSES 436 5.
PRACTICALITIES: MEASUREMENT OF THE SPIN ECHO SIGNAL 440 6. APPLICATIONS
OF NEUTRON SPIN ECHO SPECTROSCOPY 444 6.1. SOFT CONDENSED MATTER 444
6.2. GLASSY DYNAMICS 447 6.3. SPIN RELAXATION IN MAGNETIC SYSTEMS 449 7.
CONCLUSIONS 453 BIBLIOGRAPHY 453 REFERENCES 454 14 - TIME-OF-FLIGHT
INELASTIC SCATTERING R.ECCLESTON 457 1. INTRODUCTION 457 2. CLASSES OF
TOF SPECTROMETERS 458 2.1. DISTANCE-TIME PLOTS 458 2.2. KINEMATIC RANGE
460 3. BEAMLINE COMPONENTS 461 3.1. CHOPPERS 461 3.1.1. FERMI CHOPPERS
462 3.1.2. DISK CHOPPERS 462 3.1.4. T=0CHOPPERS 462 3.2. MONOCHROMATING
AND ANALYZING CRYSTALS 463 3.3. FILTERS 463 3.4. DETECTORS 464 3.5.
NEUTRON GUIDES 464 3.6. POLARIZERS AND POLARIZATION ANALYSIS 465 4.
DIRECT GEOMETRY SPECTROMETERS 465 4.1. CHOPPER SPECTROMETER ON A PULSED
SOURCE 465 4.2!"CHOPPER SPECTROMETERS ON A STEADY STATE SOURCE 466 4.3.
MULTI-CHOPPER TOF SPECTROMETERS 467 5. RESOLUTION AND SPECTROMETER
OPTIMIZATION 469 6. FLUX 470 7. RESOLUTION AS A FUNCTION OF ENERGY
TRANSFER AND EXPERIMENTAL CONSIDERATIONS 471 SINGLE CRYSTAL EXPERIMENTS
ON A CHOPPER SPECTROMETER 472 8. INDIRECT GEOMETRY SPECTROMETERS 474
8.1. THE RESOLUTION OF INDIRECT GEOMETRY SPECTROMETERS 475 8.2.
BACKSCATTERING SPECTROMETER 475 8.3. CRYSTAL ANALYZER SPECTROMETERS 477
XII NEUTRON AND X-RAY SPECTROSCOPY 8.4. DEEP INELASTIC NEUTRON
SCATTERING 478 8.5. COHERENT EXCITATIONS 479 9. CONCLUSIONS 480 FURTHER
INFORMATION 481 REFERENCES 481 15 - NEUTRON BACKSCATTERING SPECTROSCOPY
B. FRICK 483 1. INTRODUCTION 483 2. REFLECTION FROM PERFECT CRYSTALS AND
ITS ENERGY RESOLUTION 485 3. GENERIC BACKSCATTERING SPECTROMETER
CONCEPTS 488 3.1. NEUTRON OPTICS OF THE PRIMARY SPECTROMETERS OF
REACTOR-BS INSTRUMENTS 489 3.2. NEUTRON OPTICS OF THE PRIMARY
SPECTROMETER OF SPALLATION SOURCE-BS INSTRUMENTS .493 3.3. SECONDARY
SPECTROMETER 493 4. TOTAL ENERGY RESOLUTION OF THE SPECTROMETERS 49 4 5.
HOW TO DO SPECTROSCOPY? 494 5.1. SPECTROSCOPY ON REACTOR BASED
INSTRUMENTS 494 5.2. SPECTROSCOPY ON SPALLATION SOURCE-BS INSTRUMENTS
497 6. MORE DETAILS ON OPTICAL COMPONENTS 498 6.1. BS MONOCHROMATORS AND
ANALYZERS 498 6.2. HOW TO OBTAIN THE BEST ENERGY RESOLUTION IN
BACKSCATTERING? 499 6.3. MOSAIC CRYSTAL DEFLECTORS AND PHASE SPACE
TRANSFORMER 500 6.4. NEUTRON GUIDES 503 6.5. HIGHER ORDER SUPPRESSION
503 6.6. G-RESOLUTION 504 6.7. A SECOND TIME THROUGH THE SAMPLE? 504 7.
EXAMPLES FOR BACKSCATTERING INSTRUMENTS 505 7.1. REACTOR INSTRUMENTS 505
7.2. SPALLATION SOURCE INSTRUMENTS 509 8. DATA TREATMENT 511 9. TYPICAL
MEASURING METHODS AND EXAMPLES 513 9.1. FIXED WINDOW SCANS 513 9.2.
SPECTROSCOPY 516 REFERENCES 525 16 - NEUTRON INELASTIC SCATTERING AND
MOLECULAR MODELLING M.R. JOHNSON - G.J. KEARLEY-H.P. TROMMSDORFF. 529 1.
INTRODUCTION 529 2. THEORY FRAMEWORK FOR TUNNELLING, VIBRATIONS AND
TOTAL ENERGY CALCULATIONS 532 2.1. HAMILTONIANS FOR QUANTUM TUNNELLING
532 2.2. THE DYNAMICAL MATRIX FOR MOLECULAR VIBRATIONS 536 2.3. TOTAL
ENERGY CALCULATIONS FOR DETERMINING PES AND FORCE CONSTANTS 538 3.
EXPERIMENTAL TECHNIQUES FOR MEASURING ROTATIONAL TUNNELLING AND
MOLECULAR VIBRATIONS 540 TABLE OF CONTENTS XIII 4. NUMERICAL SIMULATIONS
FOR UNDERSTANDING INS SPECTRA 544 4.1. SPM METHYL GROUP TUNNELLING 544
4.2. MULTI-DIMENSIONAL TUNNELLING DYNAMICS OF METHYL GROUPS 546 4.3.
VIBRATIONAL SPECTROSCOPY OF MOLECULAR CRYSTALS 547 5. DISCUSSION 551
REFERENCES 553 INDEX 557 |
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| id | DE-604.BV021298444 |
| illustrated | Illustrated |
| index_date | 2024-07-02T13:51:56Z |
| indexdate | 2024-07-09T20:35:03Z |
| institution | BVB |
| isbn | 1402033370 9781402033377 9781402033360 1402033362 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-014619182 |
| oclc_num | 173302625 |
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| owner_facet | DE-91G DE-BY-TUM DE-703 DE-29T |
| physical | XXIV, 566 S. Ill., graph. Darst. |
| publishDate | 2006 |
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| publisher | Springer |
| record_format | marc |
| series2 | Grenoble sciences |
| spelling | Neutron and x-ray spectroscopy ed. by Françoise Hippert ... Dordrecht Springer 2006 XXIV, 566 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Grenoble sciences Neutrons - Diffusion Neutrons - Spectre Spectroscopie des rayons X Neutrons Scattering Neutrons Spectra X-ray spectroscopy Neutronenspektroskopie (DE-588)4328602-1 gnd rswk-swf Röntgenspektroskopie (DE-588)4050331-8 gnd rswk-swf Neutronenspektroskopie (DE-588)4328602-1 s DE-604 Röntgenspektroskopie (DE-588)4050331-8 s Hippert, Françoise Sonstige oth HEBIS Datenaustausch Darmstadt application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=014619182&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Neutron and x-ray spectroscopy Neutrons - Diffusion Neutrons - Spectre Spectroscopie des rayons X Neutrons Scattering Neutrons Spectra X-ray spectroscopy Neutronenspektroskopie (DE-588)4328602-1 gnd Röntgenspektroskopie (DE-588)4050331-8 gnd |
| subject_GND | (DE-588)4328602-1 (DE-588)4050331-8 |
| title | Neutron and x-ray spectroscopy |
| title_auth | Neutron and x-ray spectroscopy |
| title_exact_search | Neutron and x-ray spectroscopy |
| title_exact_search_txtP | Neutron and x-ray spectroscopy |
| title_full | Neutron and x-ray spectroscopy ed. by Françoise Hippert ... |
| title_fullStr | Neutron and x-ray spectroscopy ed. by Françoise Hippert ... |
| title_full_unstemmed | Neutron and x-ray spectroscopy ed. by Françoise Hippert ... |
| title_short | Neutron and x-ray spectroscopy |
| title_sort | neutron and x ray spectroscopy |
| topic | Neutrons - Diffusion Neutrons - Spectre Spectroscopie des rayons X Neutrons Scattering Neutrons Spectra X-ray spectroscopy Neutronenspektroskopie (DE-588)4328602-1 gnd Röntgenspektroskopie (DE-588)4050331-8 gnd |
| topic_facet | Neutrons - Diffusion Neutrons - Spectre Spectroscopie des rayons X Neutrons Scattering Neutrons Spectra X-ray spectroscopy Neutronenspektroskopie Röntgenspektroskopie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=014619182&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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