Development of a reactor system for the gas phase reduction of prochiral ketones catalysed by alcohol dehydrogenases:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Aachen
Shaker
2005
|
| Schriftenreihe: | Berichte aus der Verfahrenstechnik
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIV, 127 S. Ill., graph. Darst. 21 cm, 215 gr. |
| ISBN: | 3832239286 |
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Datensatz im Suchindex
| _version_ | 1804134595816325120 |
|---|---|
| adam_text | BERICHTE AUS DER VERFAHRENSTECHNIK CLARA FERLONI DEVELOPMENT OF A
REACTOR SYSTEM FOR THE GAS-PHASE REDUCTION OF PROCHIRAL KETONES
CATALYSED BY ALCOHOL DEHYDROGENASES D 82 (DISS.RWTH AACHEN) SHAKER
VERLAG AACHEN 2005 CONTENTS NOMENCLATURE VIII KURZFASSUNG XII 1
INTRODUCTION 1 2 STATE OF THE ART 3 2.1 CHARACTERISTICS 3 2.2 ENZYMES
AND REACTIONS 4 2.3 APPLICATIONS 5 2.4 THE PRESENT PROJECT 7 3
THEORETICAL BACKGROUND 9 3.1 ENZYME IMMOBILISATION 10 3.2 VAPOUR-LIQUID
EQUILIBRIA 11 3.3 WATER ADSORPTION AND ENZYME ACTIVITY 13 3.4 REACTION
EQUILIBRIA 17 3.5 THEORETICAL METHODS FOR THE CALCULATION OF
THERMODYNAMIC PROPERTIES 18 3.5.1 BENSON S METHOD 19 3.5.2 GAUSSIAN-3 20
4 MATERIALS AND METHODS 21 4.1 ENZYMES 21 4.1.1 YADH (EC 1.1.1.1) 21
4.1.2 LBADH (EC 1.1.1.2) 21 4.2 REACTION SYSTEM 22 4.3 ENZYME
IMMOBILISATION 23 4.3.1 LYOPHILISATION 24 4.3.2 PHYSICAL ADSORPTION 24
4.4 ENZYME ANALYSIS 25 4.4.1 ENZYME ACTIVITY MEASUREMENT 25 4.4.2
BRADFORD TEST 27 4.4.3 KARL-FISCHER TITRATION 27 VI 4.4.4 SCANNING LASER
MICROSCOPE IMAGING 29 4.5 STABILITY TESTS OF IMMOBILISED PREPARATIONS 29
4.6 BATCH REACTOR PROTOTYPE I 30 4.7 BATCH REACTIONS 31 4.8 CONTINUOUS
REACTIONS 31 4.8.1 WATER ADSORPTION ANALYSIS 32 4.8.2 CONTINUOUS
REACTIONS: METHOD DEVELOPMENT 33 4.9 CHROMATOGRAPHIC SAMPLE ANALYSIS 34
4.9.1 LIQUID SAMPLES 34 4.9.2 GASEOUS SAMPLES 34 4.9.3 DETECTION LIMIT
37 5 RESULTS AND DISCUSSION 39 5.1 ENZYME IMMOBILISATION 39 5.1.1
LYOPHILISATION 39 5.1.2 IMMOBILISATION 42 5.1.3 ENZYME AND COFACTOR
STABILITY 44 5.2 BATCH REACTOR DEVELOPMENT 52 5.2.1 THE CONSTRUCTIVE
CONCEPT OF PROTOTYPE II 52 5.2.2 EXAMPLES OF CONSTRUCTION 53 5.3
DETERMINATION OF SUBSTRATE CONCENTRATION IN BATCH REACTORS . . . . 58
5.3.1 AQUEOUS PHASE 59 5.3.2 GAS PHASE 61 5.4 SUBSTRATE SCREENING 64 5.5
CONTINUOUS PACKED-BED REACTOR DEVELOPMENT 67 5.5.1 CONTINUOUS PACKED-BED
REACTOR PROTOTYPE I 67 5.5.2 FLOW CALCULATION 71 5.5.3 REACTOR
CHARACTERISATION 74 5.5.4 CONTINUOUS PACKED BED REACTOR PROTOTYPE II 77
5.5.5 CONTINUOUS PACKED BED REACTOR PROTOTYPE III 77 5.6 OPTIMISATION OF
THE REACTION CONDITIONS 79 5.6.1 WATER ADSORPTION STUDIES 79 5.6.2
REACTION THERMODYNAMICS 88 5.6.3 EFFECT OF TEMPERATURE ON REACTION
KINETICS 92 5.6.4 EFFECT OF SUBSTRATE ACTIVITY ON REACTION KINETICS 95
5.6.5 SCALE-UP 97 5.7 CONVERSION OF INTERESTING SUBSTRATES 100 5.7.1
2-OCTANONE 101 5.7.2 3-OCTANONE 103 5.8 ECONOMICAL EVALUATION 105 6
CONCLUSIONS 111 VII A BENSON S GROUP CONTRIBUTIONS 115 B ANTOINE
PARAMETERS 116 C THERMODYNAMIC DATA 117 C.I STANDARD ENTHALPY OF
FORMATION 117 C.2 STANDARD ENTROPY OF FORMATION 117 C.3 STANDARD GIBBS
ENERGY OF FORMATION 118 BIBLIOGRAPHY 119
|
| adam_txt |
BERICHTE AUS DER VERFAHRENSTECHNIK CLARA FERLONI DEVELOPMENT OF A
REACTOR SYSTEM FOR THE GAS-PHASE REDUCTION OF PROCHIRAL KETONES
CATALYSED BY ALCOHOL DEHYDROGENASES D 82 (DISS.RWTH AACHEN) SHAKER
VERLAG AACHEN 2005 CONTENTS NOMENCLATURE VIII KURZFASSUNG XII 1
INTRODUCTION 1 2 STATE OF THE ART 3 2.1 CHARACTERISTICS 3 2.2 ENZYMES
AND REACTIONS 4 2.3 APPLICATIONS 5 2.4 THE PRESENT PROJECT 7 3
THEORETICAL BACKGROUND 9 3.1 ENZYME IMMOBILISATION 10 3.2 VAPOUR-LIQUID
EQUILIBRIA 11 3.3 WATER ADSORPTION AND ENZYME ACTIVITY 13 3.4 REACTION
EQUILIBRIA 17 3.5 THEORETICAL METHODS FOR THE CALCULATION OF
THERMODYNAMIC PROPERTIES 18 3.5.1 BENSON'S METHOD 19 3.5.2 GAUSSIAN-3 20
4 MATERIALS AND METHODS 21 4.1 ENZYMES 21 4.1.1 YADH (EC 1.1.1.1) 21
4.1.2 LBADH (EC 1.1.1.2) 21 4.2 REACTION SYSTEM 22 4.3 ENZYME
IMMOBILISATION 23 4.3.1 LYOPHILISATION 24 4.3.2 PHYSICAL ADSORPTION 24
4.4 ENZYME ANALYSIS 25 4.4.1 ENZYME ACTIVITY MEASUREMENT 25 4.4.2
BRADFORD TEST 27 4.4.3 KARL-FISCHER TITRATION 27 VI 4.4.4 SCANNING LASER
MICROSCOPE IMAGING 29 4.5 STABILITY TESTS OF IMMOBILISED PREPARATIONS 29
4.6 BATCH REACTOR PROTOTYPE I 30 4.7 BATCH REACTIONS 31 4.8 CONTINUOUS
REACTIONS 31 4.8.1 WATER ADSORPTION ANALYSIS 32 4.8.2 CONTINUOUS
REACTIONS: METHOD DEVELOPMENT 33 4.9 CHROMATOGRAPHIC SAMPLE ANALYSIS 34
4.9.1 LIQUID SAMPLES 34 4.9.2 GASEOUS SAMPLES 34 4.9.3 DETECTION LIMIT
37 5 RESULTS AND DISCUSSION 39 5.1 ENZYME IMMOBILISATION 39 5.1.1
LYOPHILISATION 39 5.1.2 IMMOBILISATION 42 5.1.3 ENZYME AND COFACTOR
STABILITY 44 5.2 BATCH REACTOR DEVELOPMENT 52 5.2.1 THE CONSTRUCTIVE
CONCEPT OF PROTOTYPE II 52 5.2.2 EXAMPLES OF CONSTRUCTION 53 5.3
DETERMINATION OF SUBSTRATE CONCENTRATION IN BATCH REACTORS . . . . 58
5.3.1 AQUEOUS PHASE 59 5.3.2 GAS PHASE 61 5.4 SUBSTRATE SCREENING 64 5.5
CONTINUOUS PACKED-BED REACTOR DEVELOPMENT 67 5.5.1 CONTINUOUS PACKED-BED
REACTOR PROTOTYPE I 67 5.5.2 FLOW CALCULATION 71 5.5.3 REACTOR
CHARACTERISATION 74 5.5.4 CONTINUOUS PACKED BED REACTOR PROTOTYPE II 77
5.5.5 CONTINUOUS PACKED BED REACTOR PROTOTYPE III 77 5.6 OPTIMISATION OF
THE REACTION CONDITIONS 79 5.6.1 WATER ADSORPTION STUDIES 79 5.6.2
REACTION THERMODYNAMICS 88 5.6.3 EFFECT OF TEMPERATURE ON REACTION
KINETICS 92 5.6.4 EFFECT OF SUBSTRATE ACTIVITY ON REACTION KINETICS 95
5.6.5 SCALE-UP 97 5.7 CONVERSION OF INTERESTING SUBSTRATES 100 5.7.1
2-OCTANONE 101 5.7.2 3-OCTANONE 103 5.8 ECONOMICAL EVALUATION 105 6
CONCLUSIONS 111 VII A BENSON'S GROUP CONTRIBUTIONS 115 B ANTOINE
PARAMETERS 116 C THERMODYNAMIC DATA 117 C.I STANDARD ENTHALPY OF
FORMATION 117 C.2 STANDARD ENTROPY OF FORMATION 117 C.3 STANDARD GIBBS
ENERGY OF FORMATION 118 BIBLIOGRAPHY 119 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Ferloni, Clara 1975- |
| author_GND | (DE-588)130012408 |
| author_facet | Ferloni, Clara 1975- |
| author_role | aut |
| author_sort | Ferloni, Clara 1975- |
| author_variant | c f cf |
| building | Verbundindex |
| bvnumber | BV020870175 |
| ctrlnum | (OCoLC)76754595 (DE-599)BVBBV020870175 |
| dewey-full | 660 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering |
| dewey-raw | 660 |
| dewey-search | 660 |
| dewey-sort | 3660 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie |
| discipline_str_mv | Chemie / Pharmazie |
| format | Thesis Book |
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| genre_facet | Hochschulschrift |
| id | DE-604.BV020870175 |
| illustrated | Illustrated |
| index_date | 2024-07-02T13:25:49Z |
| indexdate | 2024-07-09T20:27:07Z |
| institution | BVB |
| isbn | 3832239286 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-014191930 |
| oclc_num | 76754595 |
| open_access_boolean | |
| owner | DE-91 DE-BY-TUM DE-634 |
| owner_facet | DE-91 DE-BY-TUM DE-634 |
| physical | XIV, 127 S. Ill., graph. Darst. 21 cm, 215 gr. |
| publishDate | 2005 |
| publishDateSearch | 2005 |
| publishDateSort | 2005 |
| publisher | Shaker |
| record_format | marc |
| series2 | Berichte aus der Verfahrenstechnik |
| spelling | Ferloni, Clara 1975- Verfasser (DE-588)130012408 aut Development of a reactor system for the gas phase reduction of prochiral ketones catalysed by alcohol dehydrogenases Clara Ferloni Development of a reactor system for the gas-phase reduction of prochiral ketones catalysed by alcohol dehydrogenases Aachen Shaker 2005 XIV, 127 S. Ill., graph. Darst. 21 cm, 215 gr. txt rdacontent n rdamedia nc rdacarrier Berichte aus der Verfahrenstechnik Zugl.: Aachen, Techn. Hochsch., Diss., 2004 Ketone (DE-588)4129416-6 gnd rswk-swf Enzymreaktor (DE-588)4740797-9 gnd rswk-swf Alkoholdehydrogenasen (DE-588)4285029-0 gnd rswk-swf Produktentwicklung (DE-588)4139402-1 gnd rswk-swf Katalytische Reduktion (DE-588)4275223-1 gnd rswk-swf Immobilisiertes Enzym (DE-588)4161361-2 gnd rswk-swf Festbettreaktor (DE-588)4113549-0 gnd rswk-swf Enzymkatalyse (DE-588)4152480-9 gnd rswk-swf Gasphasenreaktor (DE-588)4156044-9 gnd rswk-swf Alkohole sekundär- (DE-588)4343428-9 gnd rswk-swf Konstruktion (DE-588)4032231-2 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Ketone (DE-588)4129416-6 s Katalytische Reduktion (DE-588)4275223-1 s Alkohole sekundär- (DE-588)4343428-9 s Enzymkatalyse (DE-588)4152480-9 s Alkoholdehydrogenasen (DE-588)4285029-0 s Immobilisiertes Enzym (DE-588)4161361-2 s DE-604 Festbettreaktor (DE-588)4113549-0 s Gasphasenreaktor (DE-588)4156044-9 s Enzymreaktor (DE-588)4740797-9 s Konstruktion (DE-588)4032231-2 s Produktentwicklung (DE-588)4139402-1 s HEBIS Datenaustausch Darmstadt application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=014191930&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Ferloni, Clara 1975- Development of a reactor system for the gas phase reduction of prochiral ketones catalysed by alcohol dehydrogenases Ketone (DE-588)4129416-6 gnd Enzymreaktor (DE-588)4740797-9 gnd Alkoholdehydrogenasen (DE-588)4285029-0 gnd Produktentwicklung (DE-588)4139402-1 gnd Katalytische Reduktion (DE-588)4275223-1 gnd Immobilisiertes Enzym (DE-588)4161361-2 gnd Festbettreaktor (DE-588)4113549-0 gnd Enzymkatalyse (DE-588)4152480-9 gnd Gasphasenreaktor (DE-588)4156044-9 gnd Alkohole sekundär- (DE-588)4343428-9 gnd Konstruktion (DE-588)4032231-2 gnd |
| subject_GND | (DE-588)4129416-6 (DE-588)4740797-9 (DE-588)4285029-0 (DE-588)4139402-1 (DE-588)4275223-1 (DE-588)4161361-2 (DE-588)4113549-0 (DE-588)4152480-9 (DE-588)4156044-9 (DE-588)4343428-9 (DE-588)4032231-2 (DE-588)4113937-9 |
| title | Development of a reactor system for the gas phase reduction of prochiral ketones catalysed by alcohol dehydrogenases |
| title_alt | Development of a reactor system for the gas-phase reduction of prochiral ketones catalysed by alcohol dehydrogenases |
| title_auth | Development of a reactor system for the gas phase reduction of prochiral ketones catalysed by alcohol dehydrogenases |
| title_exact_search | Development of a reactor system for the gas phase reduction of prochiral ketones catalysed by alcohol dehydrogenases |
| title_exact_search_txtP | Development of a reactor system for the gas phase reduction of prochiral ketones catalysed by alcohol dehydrogenases |
| title_full | Development of a reactor system for the gas phase reduction of prochiral ketones catalysed by alcohol dehydrogenases Clara Ferloni |
| title_fullStr | Development of a reactor system for the gas phase reduction of prochiral ketones catalysed by alcohol dehydrogenases Clara Ferloni |
| title_full_unstemmed | Development of a reactor system for the gas phase reduction of prochiral ketones catalysed by alcohol dehydrogenases Clara Ferloni |
| title_short | Development of a reactor system for the gas phase reduction of prochiral ketones catalysed by alcohol dehydrogenases |
| title_sort | development of a reactor system for the gas phase reduction of prochiral ketones catalysed by alcohol dehydrogenases |
| topic | Ketone (DE-588)4129416-6 gnd Enzymreaktor (DE-588)4740797-9 gnd Alkoholdehydrogenasen (DE-588)4285029-0 gnd Produktentwicklung (DE-588)4139402-1 gnd Katalytische Reduktion (DE-588)4275223-1 gnd Immobilisiertes Enzym (DE-588)4161361-2 gnd Festbettreaktor (DE-588)4113549-0 gnd Enzymkatalyse (DE-588)4152480-9 gnd Gasphasenreaktor (DE-588)4156044-9 gnd Alkohole sekundär- (DE-588)4343428-9 gnd Konstruktion (DE-588)4032231-2 gnd |
| topic_facet | Ketone Enzymreaktor Alkoholdehydrogenasen Produktentwicklung Katalytische Reduktion Immobilisiertes Enzym Festbettreaktor Enzymkatalyse Gasphasenreaktor Alkohole sekundär- Konstruktion Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=014191930&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT ferloniclara developmentofareactorsystemforthegasphasereductionofprochiralketonescatalysedbyalcoholdehydrogenases |