Impedance spectroscopy: theory, experiment, and applications
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Hoboken, NJ
Wiley-Interscience
2005
|
| Ausgabe: | 2. ed. |
| Schlagworte: | |
| Online-Zugang: | Table of contents Contributor biographical information Publisher description Inhaltsverzeichnis |
| Beschreibung: | Includes bibliographical references and index |
| Beschreibung: | XVII, 595 S. Ill., graph. Darst. |
| ISBN: | 9780471647492 0471647497 |
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| 245 | 1 | 0 | |a Impedance spectroscopy |b theory, experiment, and applications |c ed. by Evgenij Barsoukov ... |
| 250 | |a 2. ed. | ||
| 264 | 1 | |a Hoboken, NJ |b Wiley-Interscience |c 2005 | |
| 300 | |a XVII, 595 S. |b Ill., graph. Darst. | ||
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| 650 | 7 | |a Eletroquímica (análise) |2 larpcal | |
| 650 | 4 | |a Spectroscopie d'impédance - Expériences | |
| 650 | 4 | |a Spectroscopie d'impédance - Manuels d'enseignement supérieur | |
| 650 | 4 | |a Electrochemical analysis |x Experiments | |
| 650 | 4 | |a Impedance spectroscopy |v Textbooks | |
| 650 | 4 | |a Impedance spectroscopy |x Experiments | |
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Datensatz im Suchindex
| _version_ | 1804133199896379392 |
|---|---|
| adam_text | Titel: Impedance spectroscopy
Autor: Barsoukov, Evgenij
Jahr: 2005
Contents
Preface xi
Preface to the First Edition xiii
Contributors xv
Contributors to the First Edition xvii
1. Fundamentals of Impedance Spectroscopy 1
J. Ross Macdonald and William B. Johnson
1.1 Background, Basic Definitions, and History I
1.1.1 The Importance of Interfaces i
1.1.2 The Basic Impedance Spectroscopy Experiment 2
1.1.3 Response to a Small-Signal Stimulus in the
Frequency Domain 4
1.1.4 Impedance-Related Functions 7
1.1.5 Early History 8
1.2 Advantages and Limitations 9
1.2.1 Differences Between Solid State and Aqueous
Electrochemistry 12
1.3 Elementary Analysis of Impedance Spectra 13
1.3.1 Physical Models for Equivalent Circuit Elements 13
1.3.2 Simple RC Circuits 14
1.3.3 Analysis of Single Impedance Arcs 16
1.4 Selected Applications of IS 20
2. Theory 27
Ian D. Raistrick, Donald R. Franeeschetti, and J. Ross Macdonald
2.1 The Electrical Analogs of Physical and Chemical Processes 27
2.1.1 Introduction 27
2.1.2 The Electrical Properties of Bulk Homogeneous Phases 29
2.1.2.1 Introduction 29
2.1.2.2 Dielectric Relaxation in Materials with a Single
Time Constant 30
2.1.2.3 Distributions of Relaxation Times 34
2.1.2.4 Conductivity and Diffusion in Electrolytes 42
2.1.2.5 Conductivity and Diffusion—a Statistical
Description 44
2.1.2.6 Migration in the Absence of Concentration Gradients 46
2.1.2.7 Transport in Disordered Media 49
v
Contents
2.1.3 Mass and Charge Transport in the Presence of Concentration
Gradients 34
2.1.3.1 Diffusion 34
2.1.3.2 Mixed Electronic-Ionic Conductors 38
2.1.3.3 Concentration Polarization 60
2.1.4 Interfaces and Boundary Conditions 62
2.1.4.1 Reversible and Irreversible Interlaces 62
2.1.4.2 Polarizable Electrodes 63
2.1.4.3 Adsorption atthe Electrode-Electrolyte Interface 66
2.1.4.4 Charge Transfer at the Electrode-Electrolyte Interface
2.1.3 Grain Boundary Effects 72
2.1.6 Current Distribution, Porous and Rough Electrodes—
the Effect of Geometry 74
2.1.6.1 Current Distribution Problems 74
2.1.6.2 Rough and Porous Electrodes 73
2.2 Physical and Electrochemical Models 80
Donald R. Franceschetti and J. Ross Macdonald
2.2.1 The Modeling of Electrochemical Systems 80
2.2.2 Equivalent Circuits 81
2.2.2.1 Unification of Immitance Responses 81
2.2.2.2 Distributed Circuit Elements 83
2.2.2.3 Ambiguous Circuits 91
2.2.3 Modeling Results 93
2.2.3.1 Introduction 93
2.2.3.2 Supported Situations 97
2.2.3.3 Unsupported Situations: Theoretical Models 102
2.2.3.4 Unsupported Situations: Equivalent Network Models
2.2.3.5 Unsupported Situations: Empirical and Semiempirical
Models 117
Measuring Techniques and Data Analysis
3.1 Impedance Measurement Techniques 129
Michael C. H. McKuhre and Dighy D. Macdonald
3.1.1 Introduction 129
3.1.2 Frequency Domain Methods 130
3.1.2.1 Audio Frequency Bridges 130
3.1.2.2 Transformer Ratio Arm Bridges 133
3.1.2.3 Bcrberian-Colc Bridge 136
3.1.2.4 Considerations of Potentiostatic Control 139
3.1.2.5 Oscilloscopic Methods for Direct Measurement
3.1.2.6 Phase-Sensitive Detection for Direct Measurement
3.1.2.7 Automated Frequency Response Analysis 144
3.1.2.8 Automated Impedance Analyzers 147
3.1.2.9 The Use of Kramcrs-Kronig Transforms 149
3.1.2.10 Spectrum Analyzers 152
3.1.3 Time Domain Methods 154
31.3.1 Introduction 154
Contents vii
3.1.3.2 Analog-to-Digital (A/D) Conversion 155
3.1.3.3 Computer Interfacing 160
3.1.3.4 Digital Signal Processing 163
3.1.4 Conclusions 167
3.2 Commercially Available Impedance Measurement Systems 168
Brian Sayers
3.2.1 Electrochemical Impedance Measurement Systems 168
3.2.1.1 System Configuration 168
3.2.1.2 Why Use a Potentiostat? 169
3.2.1.3 Measurements Using 2, 3 or 4-Terminal Techniques 170
3.2.1.4 Measurement Resolution and Accuracy 171
3.2.1.5 Single Sine and FFT Measurement Techniques 172
3.2.1.6 Multielectrodc Techniques 177
3.2.1.7 Effects of Connections and Input Impedance 178
3.2.1.8 Verification of Measurement Performance 180
3.2.1.9 Floating Measurement Techniques 180
3.2.1.10 Multichannel Techniques 181
3.2.2 Materials Impedance Measurement Systems 182
3.2.2.1 System Configuration 182
3.2.2.2 Measurement of Low Impedance Materials 183
3.2.2.3 Measurement of High Impedance Materials 183
3.2.2.4 Reference Techniques 184
3.2.2.5 Normalization Techniques 185
3.2.2.6 High Voltage Measurement Techniques 185
3.2.2.7 Temperature Control 186
3.2.2.8 Sample Holder Considerations 187
3.3 Data Analysis 188
J. Ross Macdonaid
3.3.1 Data Presentation and Adjustment 188
3.3.1.1 Previous Approaches 188
3.3.1.2 Three-Dimensional Perspective Plotting 189
3.3.1.3 Treatment of Anomalies 192
3.3.2 Data Analysis Methods 194
3.3.2.1 Simple Methods 194
3.3.2.2 Complex Nonlinear Least Squares 195
3.3.2.3 Weighting 197
3.3.2.4 Which Impedance-Related Function to Fit? 197
3.3.2.5 The Question of What to Fit Revisited 198
3.3.2.6 Deconvolution Approaches 198
3.3.2.7 Examples of CNLS Fitting 199
3.3.2.8 Summary and Simple Characterization Example 202
4. Applications of Impedance Spectroscopy 205
4.1 Characterization of Materials 205
N. Bonanos, B. C. H. Steele, and E. P. Butler
4.1.1 Microstructural Models for Impedance Spectra of Materials 205
viii Contents
4.1.1.1 Introduction 205
4.1.1.2 Layer Models 207
4.1.1.3 Effective Medium Models 215
4.1.1.4 Modeling of Composite Electrodes 223
4.1.2 Experimental Techniques 227
4.1.2.1 Introduction 227
4.1.2.2 Measurement Systems 228
4.1.2.3 Sample Preparation—Electrodes 234
4.1.2.4 Problems Associated With the Measurement of Electrode
Properties 234
4.1.3 Interpretation of the Impedance Spectra of Ionic Conductors
and Interfaces 238
4.1.3.1 Introduction 238
4.1.3.2 Characterization of Grain Boundaries by IS 241
4.1.3.3 Characterization of Two-Phase Dispersions by IS 252
4.1.3.4 Impedance Spectra of Unusual Two-phase Systems 256
4.1.3.5 Impedance Spectra of Composite Electrodes 258
4.1.3.6 Closing Remarks 263
4.2 Characterization of the Electrical Response of High Resistivity Ionic
and Dielectric Solid Materials by Immittance Spectroscopy 264
J. Ross Macdonald
4.2.1 Introduction 264
4.2.2 Types of Dispersive Response Models: Strengths and Weaknesses 265
4.2.2.1 Overview 265
4.2.2.2 Variable-slope Models 266
4.2.2.3 Composite Models 267
4.2.3 Illustration of Typical Data Fitting Results for an Ionic Conductor 275
4.3 Solid State Devices 282
William B. Johnson and Wayne L. Worrell
4.3.1 Electrolyte-Insulator-Semiconductor (EIS) Sensors 284
4.3.2 Solid Electrolyte Chemical Sensors 292
4.3.3 Photoelectrochemical Solar Cells 296
4.3.4 Impedance Response of Electrochromic Materials and Devices 302
Gunnar A. Niklasson. Anna Karin Johsson, and Maria Str0mme
4.3.4.1 Introduction 302
4.3.4.2 Materials 305
4.3.4.3 Experimental Techniques 306
4.3.4.4 Experimental Results on Single Materials 310
4.3.4.5 Experimental Results on Electrochromic Devices 320
4.3.4.6 Conclusions and Outlook 323
4.3.5 Time-Resolved Photocurrent Generation 325
Albert Goassens
4.3.5.1 Introduction—Semiconductors 325
4.3.5.2 Steady-State Photocurrents 329
4.3.5.3 Time-of-FIight 330
4.3.5.4 Intensity-Modulated Photocurrent Spectroscopy 334
4.3.5.5 Final Remarks 341
Contents ix
4.4 Corrosion of Materials 343
Digby D. Macdonald and Michael C. H. McKubre
4.4.1 Introduction 343
4.4.2 Fundamentals 343
4.4.3 Measurement of Corrosion Rate 344
4.4.4 Harmonic Analysis 350
4.4.5 Kramer-Kronig Transforms 356
4.4.6 Corrosion Mechanisms 359
4.4.6.1 Active Dissolution 359
4.4.6.2 Active-Passive Transition 363
4.4.6.3 The Passive State 365
4.4.7 Point Defect Model of the Passive State 382
Digby D. Macdonald
4.4.7.1 Introduction 382
4.4.7.2 Point Defect Model 386
4.4.7.3 Electrochemical Impedance Spectroscopy 389
4.4.7.4 Bilayer Passive Films 408
4.4.8 Equivalent Circuit Analysis 414
Digby D. Macdonald and Michael C. H. McKubre
4.4.8.1 Coatings 419
4.4.9 Other Impedance Techniques 421
4.4.9.1 Electrochemical Hydrodynamic Impedance (EHI) 422
4.4.9.2 Fracture Transfer Function (FTF) 424
4.4.9.3 Electrochemical Mechanical Impedance 424
4.5 Electrochemical Power Sources 430
4.5.1 Special Aspects of Impedance Modeling of Power Sources 430
Evgenij Barsoukov
4.5.1.1 Intrinsic Relation Between Impedance Properties and Power
Sources Performance 430
4.5.1.2 Linear Time-Domain Modeling Based on Impedance Models,
Laplace Transform 431
4.5.1.3 Expressing Model Parameters in Electrical Terms, Limiting
Resistances and Capacitances of Distributed Elements 433
4.5.1.4 Discretization of Distributed Elements, Augmenting
Equivalent Circuits 436
4.5.1.5 Nonlinear Time-Domain Modeling of Power Sources
Based on Impedance Models 439
4.5.1.6 Special Kinds of Impedance Measurement Possible with
Power Sources—Passive Load Excitation and Load
Interrupt 441
4.5.2 Batteries 444
Evgenij Barsoukov
4.5.2.1 Generic Approach to Battery Impedance Modeling 444
4.5.2.2 Lead Acid Batteries 457
4.5.2.3 Nickel Cadmium Batteries 459
4.5.2.4 Nickel Metal-hydride Batteries 461
4.5.2.5 Li-ion Batteries 462
x Contents
4.5.3 Impedance Behavior of Electrochemical Supercapacitors and
Porous Electrodes 469
Brian E. Conway
4.5.3.1 Introduction 469
4.5.3.2 The Time Factor in Capacitance Charge or Discharge 472
4.5.3.3 Nyquist (or Argand) Complex-Plane Plots for
Representation of Impedance Behavior 475
4.5.3.4 Bode Plots of Impedance Parameters for Capacitors 478
4.5.3.5 Hierarchy of Equivalent Circuits and Representation of
Electrochemical Capacitor Behavior 479
4.5.3.6 Impedance and Voltammetry Behavior of Brush
Electrode Models of Porous Electrodes 485
4.5.3.7 Impedance Behavior of Supercapacitors Based on
Pseudocapacitance 489
4.5.3.8 Deviations of Double-layer Capacitance from Ideal Behavior:
Representation by a Constant-phase Element (CPE) 494
4.5.4 Fuel Cells 497
Norbert Wagner (
4.5.4.1 Introduction 497
4.5.4.2 Alkaline Fuel Cells (AFC) 509
4.5.4.3 Polymer Electrolyte Fuel Cells (PEFC) 517
4.5.4.4 Solid Oxide Fuel Cells (SOFC) 530
Appendix 539
Abbreviations and Definitions of Models 539
References 541
Index 583
|
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| discipline | Chemie / Pharmazie Maschinenbau / Maschinenwesen Physik Chemie Mess-/Steuerungs-/Regelungs-/Automatisierungstechnik |
| edition | 2. ed. |
| format | Book |
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| id | DE-604.BV019735834 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T20:04:56Z |
| institution | BVB |
| isbn | 9780471647492 0471647497 |
| language | English |
| lccn | 2004019536 |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-013062656 |
| oclc_num | 56347932 |
| open_access_boolean | |
| owner | DE-91G DE-BY-TUM DE-384 DE-703 DE-1102 DE-20 DE-29T DE-1046 DE-91 DE-BY-TUM DE-634 DE-83 DE-706 DE-860 |
| owner_facet | DE-91G DE-BY-TUM DE-384 DE-703 DE-1102 DE-20 DE-29T DE-1046 DE-91 DE-BY-TUM DE-634 DE-83 DE-706 DE-860 |
| physical | XVII, 595 S. Ill., graph. Darst. |
| publishDate | 2005 |
| publishDateSearch | 2005 |
| publishDateSort | 2005 |
| publisher | Wiley-Interscience |
| record_format | marc |
| spelling | Impedance spectroscopy theory, experiment, and applications ed. by Evgenij Barsoukov ... 2. ed. Hoboken, NJ Wiley-Interscience 2005 XVII, 595 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Includes bibliographical references and index Analyse électrochimique - Expériences Eletroquímica (análise) larpcal Spectroscopie d'impédance - Expériences Spectroscopie d'impédance - Manuels d'enseignement supérieur Electrochemical analysis Experiments Impedance spectroscopy Textbooks Impedance spectroscopy Experiments Impedanzspektroskopie (DE-588)4161400-8 gnd rswk-swf Impedanzspektroskopie (DE-588)4161400-8 s DE-604 Barsoukov, Evgenij Sonstige oth text/html http://www.loc.gov/catdir/toc/ecip0421/2004019536.html Table of contents Inhaltsverzeichnis text/html http://www.loc.gov/catdir/enhancements/fy0616/2004019536-b.html Contributor biographical information Autorenbiografie text/html http://www.loc.gov/catdir/enhancements/fy0616/2004019536-d.html Publisher description Beschreibung für Leser HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=013062656&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Impedance spectroscopy theory, experiment, and applications Analyse électrochimique - Expériences Eletroquímica (análise) larpcal Spectroscopie d'impédance - Expériences Spectroscopie d'impédance - Manuels d'enseignement supérieur Electrochemical analysis Experiments Impedance spectroscopy Textbooks Impedance spectroscopy Experiments Impedanzspektroskopie (DE-588)4161400-8 gnd |
| subject_GND | (DE-588)4161400-8 |
| title | Impedance spectroscopy theory, experiment, and applications |
| title_auth | Impedance spectroscopy theory, experiment, and applications |
| title_exact_search | Impedance spectroscopy theory, experiment, and applications |
| title_full | Impedance spectroscopy theory, experiment, and applications ed. by Evgenij Barsoukov ... |
| title_fullStr | Impedance spectroscopy theory, experiment, and applications ed. by Evgenij Barsoukov ... |
| title_full_unstemmed | Impedance spectroscopy theory, experiment, and applications ed. by Evgenij Barsoukov ... |
| title_short | Impedance spectroscopy |
| title_sort | impedance spectroscopy theory experiment and applications |
| title_sub | theory, experiment, and applications |
| topic | Analyse électrochimique - Expériences Eletroquímica (análise) larpcal Spectroscopie d'impédance - Expériences Spectroscopie d'impédance - Manuels d'enseignement supérieur Electrochemical analysis Experiments Impedance spectroscopy Textbooks Impedance spectroscopy Experiments Impedanzspektroskopie (DE-588)4161400-8 gnd |
| topic_facet | Analyse électrochimique - Expériences Eletroquímica (análise) Spectroscopie d'impédance - Expériences Spectroscopie d'impédance - Manuels d'enseignement supérieur Electrochemical analysis Experiments Impedance spectroscopy Textbooks Impedance spectroscopy Experiments Impedanzspektroskopie |
| url | http://www.loc.gov/catdir/toc/ecip0421/2004019536.html http://www.loc.gov/catdir/enhancements/fy0616/2004019536-b.html http://www.loc.gov/catdir/enhancements/fy0616/2004019536-d.html http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=013062656&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT barsoukovevgenij impedancespectroscopytheoryexperimentandapplications |