Mass spectrometry of inorganic, coordination and organometallic compounds: tools, techniques, tips
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Chichester
Wiley
2005
|
| Schriftenreihe: | Inorganic chemistry
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Beschreibung: | XX, 271 S. Ill., graph. Darst. |
| ISBN: | 0470850159 0470850167 |
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| 245 | 1 | 0 | |a Mass spectrometry of inorganic, coordination and organometallic compounds |b tools, techniques, tips |c William Henderson amd J. Scott McIndoe |
| 264 | 1 | |a Chichester |b Wiley |c 2005 | |
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| 650 | 7 | |a Espectrometria |2 larpcal | |
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Datensatz im Suchindex
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| adam_text | Contents
Preface............................................................... XV
List of commonly-used abbreviations........................................ XIX
1 Fundamentals........................................................ 1
1.1 Introduction...................................................... 1
1.2 Inlets.......................................................... 1
1.3 Collision-Induced Dissociation........................................ 2
1.3.1 Bond dissociation energies from CID studies......................... 4
1.3.2 Presentation of CID data....................................... 4
1.4 Detectors....................................................... 6
1.5 Mass Resolution.................................................. 7
1.5.1 Mass accuracy............................................. 10
1.6 Data Processing................................................... 12
1.7 Isotopes........................................................ 14
1.7.1 Isotopic abundances of the elements.............................. 17
1.7.2 Isotope pattern matching...................................... 19
References.......................................................... 21
2 Mass analysers...................................................... 23
2.1 Introduction...................................................... 23
2.2 Sectors......................................................... 23
2.2.1 MS/MS.................................................. 26
2.2.2 Summary................................................. 26
2.3 Quadrupoles..................................................... 27
2.3.1 MS/MS.................................................. 29
2.3.2 Summary................................................. 30
2.4 Quadrupole Ion Trap............................................... 30
2.4.1 MS/MS and MS ............................................ 33
2.4.2 Summary................................................. 34
2.5 Time-of-Flight.................................................... 35
2.5.1 Reflectron instruments........................................ 37
2.5.2 Orthogonal TOF (oa-TOF)..................................... 38
2.5.3 MS/MS.................................................. 38
2.5.4 Summary................................................. 40
2.6 Fourier Transform Ion Cyclotron Resonance............................... 40
2.6.1 MS/MS.................................................. 43
2.6.2 Summary................................................. 44
References.......................................................... 45
Contents
Ionisation techniques................................................. 47
3.1 Introduction...................................................... 47
3.2 Electron Ionisation................................................. 47
3.2.1 Fragmentation of metal-containing compounds....................... 50
3.2.2 Applications............................................... 51
3.2.3 Summary................................................. 53
3.3 Chemical Ionisation................................................ 54
3.3.1 Applications............................................... 56
3.3.2 Summary................................................. 57
3.4 Field Ionisation/Field Desorption....................................... 58
3.4.1 Summary................................................. 59
3.5 Plasma Desorption................................................. 60
3.5.1 Applications............................................... 60
3.5.2 Summary................................................. 62
3.6 Fast Atom Bombardment / Liquid Secondary Ion Mass Spectrometry............. 62
3.6.1 Matrices.................................................. 63
3.6.2 Ions observed in FAB/LSIMS................................... 65
3.6.3 Applications............................................... 66
3.6.4 Summary................................................. 71
3.7 Matrix Assisted Laser Desorption Ionisation............................... 72
3.7.1 Matrices.................................................. 75
3.7.2 MALDI of air-sensitive samples................................. 76
3.7.3 Applications............................................... 77
3.7.4 Summary................................................. 87
3.8 Inductively Coupled Plasma Mass Spectrometry............................ 88
3.8.1 Applications............................................... 89
3.8.2 Summary................................................. 90
3.9 Electrospray Ionisation.............................................. 90
3.9.1 Electrochemistry in the ESI process.............................. 92
3.9.2 Multiply-charged species ...................................... 94
3.9.3 Nanospray................................................ 95
3.9.4 ESI MS: Practical considerations................................ 96
3.9.5 Applications............................................... 99
3.9.6 Summary................................................. 99
References......................................................... 100
The ESI MS behaviour of simple inorganic compounds....................... 107
4.1 Introduction..................................................... 107
4.2 Simple Metal Salts................................................ 107
4.2.1 Salts of singly-charged ions, M+X~.............................. 107
4.2.2 Salts of multiply-charged ions, e.g. M2+(X )2, M3+(X~)3 etc............. 112
4.2.3 Negative-ion ESI mass spectra of metal salts........................ 116
4.2.4 ESI MS behaviour of easily-reduced metal ions: copper(II), iron(III) and
mercury(II)................................................ 117
4.3 Polyanions Formed by Main Group Elements............................. 119
4.4 Oxoanions Formed by Main Group Elements............................. 119
4.5 Borane Anions................................................... 122
4.6 Fullerenes..................................................... 122
Contents xi
4.7 Inorganic Phosphorus Compounds: Phosphoranes and Cyclophosphazenes......... 123
4.8 Summary...................................................... 123
References......................................................... 123
5 The ESI MS behaviour of coordination complexes........................... 127
5.1 Introduction..................................................... 127
5.2 Charged, Simple Coordination Complexes.............................. 128
5.2.1 Cationic coordination complexes................................. 128
5.2.2 Anionic metal halide complexes................................. 132
5.2.3 Highly-charged, anionic transition metal complexes - cyanometallate anions. . 134
5.3 (Neutral) Metal Halide Coordination Complexes........................... 136
5.4 Metal Complexes of Polydentate Oxygen Donor Ligands: Polyethers, Crown Ethers,
Cryptands and Calixarenes.......................................... 139
5.5 Porphyrins and Metalloporphyrins..................................... 141
5.6 Metal Alkoxides - Highly Moisture-Sensitive Coordination Compounds.......... 144
5.7 /3-Diketonate Complexes............................................ 145
5.8 Metal Complexes of Carbohydrates.................................... 148
5.9 Metal Complexes of Amino Acids, Peptides and Proteins..................... 149
5.9.1 Amino acids............................................... 149
5.9.2 Proteins and peptides......................................... 150
5.10 Oxoanions, Polyoxoanions and Related Species............................ 151
5.10.1 Simple transition metal oxoanions................................ 151
5.10.2 Reactivity studies involving molybdate and tungstate ions............... 154
5.10.3 Polyoxoanions............................................. 155
5.10.4 Miscellaneous oxo complexes................................... 157
5.11 Metal Clusters................................................... 157
5.12 Compounds with Anionic Sulfur and Selenium Donor Ligands................. 158
5.12.1 Metal sulfide, selenide and related complexes........................ 158
5.12.2 Metal dithiocarbamate and dithiophosphate complexes................. 159
5.12.3 Metal thiolate complexes...................................... 160
5.13 Characterisation of Metal-Based Anticancer Drugs, their Reaction Products
and Metabolites.................................................. 163
5.13.1 Characterisation of anticancer-active platinum complexes............... 163
5.13.2 Reactions of platinum anticancer drugs with biomolecules and detection
of metabolites................................................... 165
5.13.3 Other non-platinum anticancer agents............................. 166
5.14 In situ Formation of Coordination Complexes as an Ionisation Technique......... 166
5.15 Summary...................................................... 167
References......................................................... 168
6 The ESI MS behaviour of main group organometallic compounds............... 175
6.1 Introduction..................................................... 175
6.2 Organometallic Derivatives of Group 14 Elements.......................... 175
6.2.1 Organosilicon compounds..................................... 175
6.2.2 Organogermanium compounds.................................. 176
6.2.3 Organotin compounds........................................ 176
6.2.4 Organolead compounds....................................... 178
6.3 Organometallic Derivatives of Group 15 Elements.......................... 180
xii Contents
6.3.1 Organophosphorus compounds.................................. 180
6.3.2 Organoarsenic compounds..................................... 185
6.3.3 Organoantimony and -bismuth compounds.......................... 187
6.4 Organometallic Derivatives of Group 16 Elements; Organosulfur, -Selenium and -Tellurium
Compounds..................................................... 188
6.5 Organomercury Compounds......................................... 188
6.6 Other Organometallic Derivatives..................................... 190
6.7 Summary...................................................... 190
References......................................................... 190
7 The ESI MS behaviour of transition metal and lanthanide organometallic compounds 195
7.1 Introduction..................................................... 195
7.2 Metal Carbonyl Complexes.......................................... 195
7.2.1 Ionic mononuclear metal carbonyl compounds....................... 196
7.2.2 Ionic metal carbonyl clusters................................... 196
7.2.3 Neutral metal carbonyl compounds............................... 198
7.2.4 Oxidation and reduction processes involving metal carbonyls............. 201
7.2.5 Characterisation of reaction mixtures involving metal carbonyl clusters...... 201
7.2.6 Fragmentation of transition metal carbonyl clusters; electrospray as a source
of bare metal clusters........................................ 203
7.2.7 The use of Electrospray-friendly ligands in organometallic chemistry...... 204
7.3 Metal Isocyanide Complexes......................................... 204
7.4 Metal Cyclopentadienyl and Related Complexes........................... 205
7.4.1 Ferrocene-based compounds.................................... 205
7.4.2 Use of ferrocene derivatives as electroactive derivatisation agents for
electrospray ionisation........................................ 209
7.4.3 Other metallocene systems..................................... 210
7.4.4 Monocyclopentadienyl complexes................................ 210
7.5 Metal 773-allyl Complexes........................................... 211
7.6 Metal Arene Complexes............................................ 212
7.7 Formation of 7r-Hydrocarbon Complexes and their Use as an Ionisation Aid....... 212
7.8 Metal-Acetylene/acetylide Complexes and Complexes of Metal-Acetylides........ 213
7.9 Transition Metal a-Alkyl and Aryl Complexes............................ 214
7.10 Mass Spectrometry of Lanthanide Organometallic Complexes.................. 215
7.11 Summary...................................................... 215
References......................................................... 215
8 A selection of special topics............................................ 221
8.1 Introduction..................................................... 221
8.2 Characterisation of Dendrimers Using ESI and MALDI-TOF MS Techniques....... 221
8.3 Investigating the Formation of Supramolecular Coordination Assemblies Using ESI MS 222
8.4 Using ESI MS as a Tool for Directing Chemical Synthesis: A Case Study Involving the
Platinum Metalloligands [Pt2(/i-E)2(PPh3)4].............................. 224
8.4.1 Background............................................... 224
8.4.2 Analysis of the metalloligands; formation of protonated species........... 225
8.4.3 Reactivity of [Pt2(/i-E)2(PPh3)4] towards metal-halide complexes.......... 226
8.5 Applications of ESI MS in the Detection of Reactive Intermediates and
Catalyst Screening................................................ 228
Contents xiii
8.5.1 Detection of intermediates in reactions of organic compounds............ 228
8.5.2 Detection and chemistry of reaction intermediates in the gas phase........ 230
8.5.3 Screening of new catalysts using mass spectrometry................... 231
References......................................................... 232
Appendix 1 Naturally occurring isotopes.................................... 235
Appendix 2 Periodic table of the elements................................... 247
Appendix 3 Alphabetical list of elements.................................... 249
Appendix 4 Glossary of terms............................................ 251
Appendix 5 Useful sources of information................................... 265
Index............................................................... 267
|
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| indexdate | 2024-07-09T20:04:35Z |
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| isbn | 0470850159 0470850167 |
| language | English |
| lccn | 2004023728 |
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| record_format | marc |
| series2 | Inorganic chemistry |
| spelling | Henderson, William Verfasser aut Mass spectrometry of inorganic, coordination and organometallic compounds tools, techniques, tips William Henderson amd J. Scott McIndoe Chichester Wiley 2005 XX, 271 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Inorganic chemistry Compostos organometálicos (química inorgânica) larpcal Espectrometria de massas larpcal Espectrometria larpcal Mass spectrometry Chemistry, Inorganic Organometallic compounds Metallorganische Verbindungen (DE-588)4038906-6 gnd rswk-swf Massenspektrometrie (DE-588)4037882-2 gnd rswk-swf Komplexe (DE-588)4133953-8 gnd rswk-swf Anorganische Verbindungen (DE-588)4002147-6 gnd rswk-swf Metallorganische Verbindungen (DE-588)4038906-6 s Massenspektrometrie (DE-588)4037882-2 s DE-604 Anorganische Verbindungen (DE-588)4002147-6 s Komplexe (DE-588)4133953-8 s b DE-604 McIndoe, J. Scott Sonstige oth http://www.loc.gov/catdir/toc/ecip052/2004023728.html Inhaltsverzeichnis HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=013047469&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Henderson, William Mass spectrometry of inorganic, coordination and organometallic compounds tools, techniques, tips Compostos organometálicos (química inorgânica) larpcal Espectrometria de massas larpcal Espectrometria larpcal Mass spectrometry Chemistry, Inorganic Organometallic compounds Metallorganische Verbindungen (DE-588)4038906-6 gnd Massenspektrometrie (DE-588)4037882-2 gnd Komplexe (DE-588)4133953-8 gnd Anorganische Verbindungen (DE-588)4002147-6 gnd |
| subject_GND | (DE-588)4038906-6 (DE-588)4037882-2 (DE-588)4133953-8 (DE-588)4002147-6 |
| title | Mass spectrometry of inorganic, coordination and organometallic compounds tools, techniques, tips |
| title_auth | Mass spectrometry of inorganic, coordination and organometallic compounds tools, techniques, tips |
| title_exact_search | Mass spectrometry of inorganic, coordination and organometallic compounds tools, techniques, tips |
| title_full | Mass spectrometry of inorganic, coordination and organometallic compounds tools, techniques, tips William Henderson amd J. Scott McIndoe |
| title_fullStr | Mass spectrometry of inorganic, coordination and organometallic compounds tools, techniques, tips William Henderson amd J. Scott McIndoe |
| title_full_unstemmed | Mass spectrometry of inorganic, coordination and organometallic compounds tools, techniques, tips William Henderson amd J. Scott McIndoe |
| title_short | Mass spectrometry of inorganic, coordination and organometallic compounds |
| title_sort | mass spectrometry of inorganic coordination and organometallic compounds tools techniques tips |
| title_sub | tools, techniques, tips |
| topic | Compostos organometálicos (química inorgânica) larpcal Espectrometria de massas larpcal Espectrometria larpcal Mass spectrometry Chemistry, Inorganic Organometallic compounds Metallorganische Verbindungen (DE-588)4038906-6 gnd Massenspektrometrie (DE-588)4037882-2 gnd Komplexe (DE-588)4133953-8 gnd Anorganische Verbindungen (DE-588)4002147-6 gnd |
| topic_facet | Compostos organometálicos (química inorgânica) Espectrometria de massas Espectrometria Mass spectrometry Chemistry, Inorganic Organometallic compounds Metallorganische Verbindungen Massenspektrometrie Komplexe Anorganische Verbindungen |
| url | http://www.loc.gov/catdir/toc/ecip052/2004023728.html http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=013047469&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT hendersonwilliam massspectrometryofinorganiccoordinationandorganometalliccompoundstoolstechniquestips AT mcindoejscott massspectrometryofinorganiccoordinationandorganometalliccompoundstoolstechniquestips |
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