Comprehensive handbook of calorimetry and thermal analysis:
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| Format: | Book |
|---|---|
| Language: | English Japanese |
| Published: |
Chichester
Wiley
2004
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XXI, 534 S. Ill., graph. Darst |
| ISBN: | 047085152x |
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| adam_text | IMAGE 1
PREFACE XI
ACKNOWLEDGEMENTS XIII
LIST OF CONTRIBUTORS XV
PART I PRINCIPLES OF CALORIMETRY AND THERMAL ANALYSIS 1
1.1 CALORIMETRY 3 1.1.1 OVERVIEW 3 1.1.2 THERINODYNAMIC QUANTITIES
CHARACTERISTIC OF MULTI-COMPONENT SYSTEM 8 1.1.3 THERMODYNAMIC
QUANTITIES CHARACTERISTIC OF SURFACE AND
INTERFACE 13 1.1.4 THERMODYNAMIC QUANTITIES IN CHERNICAL REACTIONS 18
1.1.5 THERMODYNAMICS OF NON-EQUILIBRIUM STATES 2 1 1.1.6
BIOTHERMODYNAINICS 25
1.2 THERMAL ANALYSIS 29 1.2.1 OVERVIEW 29 1.2.2 THERMAL ANALYSIS FOR
CHEMICAL REACTIONS 33 1.2.3 THERMAL ANALYSIS FOR MECHANICAL PROPERTIES
37 1.2.4 DYNARNIC VISCOELASTIC PHENOMENA AND THERMAL ANALYSIS 43
1.2.5 REACTION KINETICS IN THE SOLID STATE 50 1.2.6 PERIODIC HEATING
METHOD 54
PART I1 EXPERINIENTAL METBODS 57
2.1 TEMPERATURE MEASUREMENT IN THERMAL STUDY 59
2.2 PRINCIPLES AND METHODS OF CALORIMETRY 63 2.2.1 CLASSIFICATION AND
BASIC PRINCIPLES OF CALORIMETERS 63 2.2.2 ADIABATIC HEAT CAPACITY
CALORIMETRY 68 2.2.3 HEAT CAPACITY CALORIMETRY BY RELAXATION METHOD 72
2.2.4 AC CALORIMETRY 75 2.2.5 LASER-FLASH CALORIMETRY 77 2.2.6
HIGH-TEMPERATURE CALORIMETRY 80
IMAGE 2
CONTENTS
2.2.7 LOW-TEMPERATURE CALORIMETRY 83 2.2.8 CALORIMETRY UNDER PRESSURE 86
2.2.9 CALORIMETRY UNDER MAGNETIC FIELD 89 2.2.10 TEMPERATURE JUMP
CALORIMETRY 92 2.2.1 1 CALVET CALORIMETER 95 2.2.12 HEAT OF VAPORIZATION
AND SUBLIMATION 99 2.2.13 REACTION CALORIMETRY 101 2.2.14 HEAT OF
SOLUTION AND MIXING 1.03 2.2.15 HEAT OF IRNRNERSION AND ADSORPTION 106
2.2.16 TITRATION CALORIMETRY 109 2.2.17 FLOW CALORIMETRY 11 1 2.2.18
HEAT CAPACITY SPECTROSCOPY 1 15 2.2.19 CALORIMETRY AT EXTREMELY HIGH
TEMPERATURES 1 17 2.2.20 ADIABATIC DIFFERENTIAL SCANNING CALORIMETRY FOR
BIOTHERMODYNARNICS 120
2.3 PRINCIPLES AND METHODS OF THERMAL ANALYSIS 123 2.3.1
THERMOGRAVIMETRY (TG) AND CONTROLLED-RATE TG 123 2.3.2 DIFFERENTIAL
THERMAL ANALYSIS (DTA) AND D.IFFERENTIA1 SCANNING CALORIMETRY (DSC) 128
2.3.3 THERMOMEC HANICAL ANAL Y SIS (TMA) AND DYNARNIC MECHANICAL
ANALYSIS (DMA) 135 2.3.4 TEMPERATURE-MODULATED DS C 140 2.3.5
TEMPERATURE WAVE CUIALYSIS 145 2.3.6 TRIPLE-CELL DSC 148 2.3.7
SIMULTANEOUS THERMAL ANALYSIS 15 1 2.3.8 MICRO THERMAL ANALYSIS BY
SCANNING PROBE MICROSCOPES 157 2.3.9 MICROMECHANICAL CALORIMETRY 160
2.4 OTHER EXPERIMENTS 162 2.4.1 DETERMINATION OF THERMAL EXPANSIVITY 162
2.4.2 STEADY STATE METHOD OF DETERMINATION OF THERMAL
CONDUCTIVITY/DIFFUSIVITY 167 2.4.3 TRANSIENT METHOD FOR DETERMINATION OF
THERMAL
CONDUCTIVITY/DIFFUSIVITY 17 1 2.4.4 MASS SPECTROMETRY 175 2.4.5
DETERMINATION OF ELECTROMOTIVE FORCE 179 2.4.6 SURFACE TENSION 183
PART I11 DATA ANALYSIS 187
3.1 DATA ANALYSIS OF CALORIMETRY 189 3.1.1 PURITY DETERMINATION 189
3.1.2 PHASE TRANSITION AND NORMAL HEAT CAPACITY 191
IMAGE 3
VII
3.1.3 DETERMINATION OF PARTIAL MOLAR QUANTITIES 195 3.1.4 STATISTICAL
THERMODYNAMIC ANALYSIS IN BIOCALORIMETRY 200 3.1.5 DATA ANALYSIS IN
TITRATION CALORIMETRY 208
3.2 TECHNIQUES OF THERMAL ANALYSIS AND THE DATA ANALYSIS 213 3.2.1
SOLID-STATE REACTION KINETICS BY TG 213 3.2.2 BASELINE AND THERMAL
ANOMALY IN DTA AND DSC 219 3.2.3 HEAT CAPACITY MEASUREMENT BY DSC AND
TM-DSC 224
3.2.4 ANALYSIS OF ISOTHERMAL CRYSTALLIZATION BY DSC 228 3.2.5 GLASS
TRANSITION AND RELAXATION PHENOMENA 233 3.2.6 DETERMINATION OF PHASE
DIAGRAMS BY DTADSC 237 3.2.7 PURITY DETERRNINATION BY DSC 241
PART IV HOW T 0 LTTILIZE THE THERMODUNAMIC DATABASE 247
4.1 THERMODYNAMIC AND RELATED DATABASE 249 4.1.1 RECENT DEVELOPMENT OF
THERMODYNAMIC DATABASE SYSTEMS 249 4.1.2 PHASE DIAGRAM CALCULATIONS 253
4.1.3 THERMOPHYSICAL PROPERTY DATABASE 257
4.2 UTILIZATION OF THERMODYNAMIC DATABASE 262 4.2.1 CALCULATED PHASE
DIAGRARN VS OBSERVED PHASE DIAGRAM 262 4.2.2 APPLICATION OF CHEINICAL
EQUILIBRIUM CALCULATIONS 268 4.2.3 APPLICATION OF CHEMICAL POTENTIAL
DIAGRAM 272
4.3 THERMODYNAMIC DATABASE FOR BIOMOLECULES 276 4.3.1 PROTEINS AND
MUTANTS 276 4.3.2 PROTEIN-NUCLEIC ACID INTERACTIONS 280
PART V ACTUAL APPLICATIONS 285
5.1 METALS AND ALLOYS 287 5.1.1 THERMAL ANALYSIS OF ARNORPHOUS ALLOYS
287 5.1.2 THERMAL ANALYSIS OF HYDROGEN-ABSORBING ALLOY 29 1 5.1.3
THERMAL ANALYSES OF HEAT-RESISTANT TYPE STEELS AND ALLOYS 294 5.1..4
THERMODYNARNIC ANALYSIS OF LIQUID ALLOYS BY TEMPERATURE-JUINP
CALORIMETRY 297 5.1.5 EMF METHOD WITH SOLID ELECTROLYTE FOR LIQUID
ALLOYS 300 5.1.6 CONSTRUCTION OF ALLOY PHASE DIAGRAMS 303 5.1.7
ELECTRONIC DENSITY OF STATES OF QUASICRYSTALS 307 5.1.8 KINETICS OF
OXIDATION IN THIN META1 FILMS 309 5.1.9 LATTICE-DEFECT CONCENTRATION IN
SOLIDS FROM THERMAL EXPANSION 3 12
IMAGE 4
. . . V L L L CONTEN TS
5.2 INORGANIC MATERIALS AND CERAMICS 315 5.2.1 HEAT CAPACITY OF U 0 2 UP
TO 8000 K 3 15 5 -2.2 BATTERY MATERIALS : S PINELS CONTAINING MN FOR
LITHIUM SECONDARY BATTERY 3 18 5.2.3 THERMAL CONDUCTIVITY OF DIARNOND
FILM 321 5.2.4 KINETIC FEATURES OF TL-IE THERMAL DEHYDRATION OF
INORGANIC
HYDRATES 324 5.2.5 DEHYDRATION OF INORGANIC SALTS UNDER REDUCED PRESSURE
327 5.2.6 THERMAL ANALYSIS OF WATER-COILTAIILING SILICATE ININERALS 329
5.2.7 HEAT OF ADSORPTION AND EVALUATION OF ACTIVE SITES OLL THE
SURFACE 332 5.2.8 NONSTOICHIOMETRY OF OXIDES BY CONSTANT TEMPERATURE TG
335 5.2.9 HEAT OF L-IYDRATION OF ZEOLITE 338 5.2.10 HEAT CAPACITY OF
YTTRIA-STABILIZED ZIRCONIA 342 5.2.1 1 ACOUSTIC EMISSION AND THERMAL
ANALYSIS OF PHASE TRANSITIONS 345 5.2.12 PORE-SIZE DISTRIBUTIONS IN
SILICA GELS 348 5.2.13 CALORIINETRY FOR FAST ION CONDUCTING GLASSES 352
5.2.14 NEGATIVE THERMAL EXPANSION OF ZRW208 355
5.2.15 CALORIMETRY OF HIGH-PRESSURE MINERALS 357 5.2.16 HEAT CAPACITY OF
DIAMOND AND GRAPHITE 360 5.2.17 HEAT CAPACITY ANOMALY IN LEAD-BASED
COMPLEX PEROVSKITE RELAXOI-S 362
5.3 ORGANIC MATERIALS AND POLYMERS 365 5.3.1 STRAIN AND RESONANCE
ENERGIES OF FULLERENES 365 5.3.2 HEAT CAPACITY OF MOLECULAR MONOLAYERS
367 5.3.3 ENTROPY OF TRANSITION OF RNIXED CRYSTALS 370 5.3.4 GLASS
TRANSITION AND RESIDUAL ENTROPY 372 5.3.5 HEAT CAPACITY OF EXOTIC
SUPERCONDUCTORS 375 5.3.6 MAGNETIC DIMENSIONALITY AND SPIN-WAVE
EXCITATION OF
INOLECULE-BASED MAGNET 379 5.3.7 CALORIINETRY OF LIQUID CRYSTALS 382
5.3.8 ALKYL-CHAIN-LENGTH DEPENDENCE OF ENTROPY OF TRANSITION 384 5.3.9
HIGH-PRESSURE DTA OF LIQUID CRYSTALS 386 5.3.10 CRYSTALLIZATIOI~ OF
POLYMERS 389
5.3.1 1 MELTING OF POLYINER CRYSTALS STUDIED BY TEMPERATURE-INODULATED
DSC 392 5.3.12 ORIGIN OF DOUBLE MELTING PEAKS OF DRAWN NYLON 6 395
5.3.13 GLASS TRANSITION AND RELAXATION IN POLYMERS 398 5.3.14 THERMAL
DECOMPOSITION OF POLYURETHANES CONTAINING NATURAL
CORNPOUNDS 400 5.3.15 CURING OF EPOXY RESINS CONTAINING PLANT
COMPOIIENTS 403 5.3.16 PHASE TRANSITION IN SPIN-CROSSOVER COMPLEX 406
5.3.17 FREQUENCY-DEPENDENT HEAT CAPACITY NEAR A GLASS TRANSITION 409
IMAGE 5
CONTENTS IX
5.3.18 HEAT CAPACITY OF MOLECULAR MAGNETS UNDER MAGNETIC FIELD 412
5.3.19 MICRO THERMAL ANALYSIS OF POLYRNERS BY SCANNING PROBE RNICROSCOPY
4 15
5.4 BIOMOLECULES 419 5.4.1 PHASE TRANSITION OF LIPID 41 9 5.4.2 THERMAL
STABILITY AND FUNCTION OF MYB PROTEIN 422 5.4.3 THERMAL STABILITY OF
MUTANT LYSOZYRNES 425 5.4.4 STEPWISE MELTING OF PLASMID DNA IN THE
PRESENCE OF
ION 428
5.4.5 VOLUME AND COMPRESSIBILITY OF PROTEINS 43 1 5.4.6 ENZYME ACTIVITY
433 5.4.7 PROTEIN-DNA INTERACTION 436 5.4.8 MOLECULAR RECOGNITION OF
ANTIBODY 438 5.4.9 GLASS TRANSITION OF PROTEIN 442
5.5 MEDICINES 445 5.5.1 PURITY DETERMINATION OF MEDICINES BY DSC 445
5.5.2 EVALUATION OF POLYMORPHIC TRANSFORRNATION OF DRUGS 448 5.5.3
DETERMINATION OF HEAT OF HYDRATION AND HYDRATION KINETICS OF
THEOPHYLLINE HYDRATES 452 5.5.4 INCLUSION COMPOUND FORMATION BETWEEN
HOST MATERIAL AND RNEDICINAL RNOLECULES 454 5.5.5 ESTIRNATION OF INITIAL
DISSOLUTION RATE OF DRUG SUBSTAIICES BY THERMAL
ANALYSIS 457 5.5.6 LONG-TERIN STABILITY 460 5.5.7 EFFECT OF DRUGS ON
RNICROBIAL GROWTH ACTIVITIES 463 5.5.8 DRUG INTERACTIOII IN HUMAN BLOOD
466
5.6 FOODS AND BIOMATERIALS 469 5.6.1 PHASE TRANSITION OF GLYCOLIPIDS 469
5.6.2 SOL-GEL TRANSITION IN POLYSACCHARIDES 472 5.6.3 PHASE TRANSITION
OF POLY SACCHARIDE HELIX 475
5.6.4 INTERACTION BETWEEN STACH AND WATER 478 5.6.5 NOVEL
BIOMATERIAL-WATER INTERACTION PRODUCED BY HEAT TREATRNENT 48 1 5.6.6
NONFREEZING WATER IN FOOD 484 5.6.7 QUANTITATIVE EVALUATION OF FOOD
PUTREFACTION 487 5.6.8 THERMAL ANALYSIS OF VARIOUS PLANT RNATERIALS 490
5.6.9 DYNARNIC VISCOELASTICITY OF HAIR 494
APPENDIX 497
A.1 THE INTERNATIONAL TEMPERATURE SCALE OF 1990 (ITS-90) 499 A. 2
ELECTROMOTIVE FORCE OF THERMOCOUPLES 506
IMAGE 6
CONTENTS
A.3 STANDARD REFERENCE MATERIALS FOR THERMAL ANALYSIS 5 12 A.4 SYMBOLS
AND NOTATIONS FOR THERMODYNARNIC AND RELATED QUANTITIES AND THEIR
PRINTING 5 15 A.5 GUIDELINES FOR PRESENTATION OF EXPERIMENTAL RESULTS 5
18
INDEX 523
|
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| id | DE-604.BV019386589 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T19:59:06Z |
| institution | BVB |
| isbn | 047085152x |
| language | English Japanese |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-012849474 |
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| owner_facet | DE-91G DE-BY-TUM DE-19 DE-BY-UBM |
| physical | XXI, 534 S. Ill., graph. Darst |
| publishDate | 2004 |
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| publishDateSort | 2004 |
| publisher | Wiley |
| record_format | marc |
| spelling | Netsuryo sokutei netsu bunseki handobukku Comprehensive handbook of calorimetry and thermal analysis Michio Sorai (ed.-in-chief) Chichester Wiley 2004 XXI, 534 S. Ill., graph. Darst txt rdacontent n rdamedia nc rdacarrier Análisis térmico diferencial - Manuales Calorimetría - Manuales Kalorimetrie (DE-588)4029367-1 gnd rswk-swf Thermoanalyse (DE-588)4135675-5 gnd rswk-swf Thermoanalyse (DE-588)4135675-5 s DE-604 Kalorimetrie (DE-588)4029367-1 s Sorai, Michio Sonstige oth OEBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=012849474&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Comprehensive handbook of calorimetry and thermal analysis Análisis térmico diferencial - Manuales Calorimetría - Manuales Kalorimetrie (DE-588)4029367-1 gnd Thermoanalyse (DE-588)4135675-5 gnd |
| subject_GND | (DE-588)4029367-1 (DE-588)4135675-5 |
| title | Comprehensive handbook of calorimetry and thermal analysis |
| title_alt | Netsuryo sokutei netsu bunseki handobukku |
| title_auth | Comprehensive handbook of calorimetry and thermal analysis |
| title_exact_search | Comprehensive handbook of calorimetry and thermal analysis |
| title_full | Comprehensive handbook of calorimetry and thermal analysis Michio Sorai (ed.-in-chief) |
| title_fullStr | Comprehensive handbook of calorimetry and thermal analysis Michio Sorai (ed.-in-chief) |
| title_full_unstemmed | Comprehensive handbook of calorimetry and thermal analysis Michio Sorai (ed.-in-chief) |
| title_short | Comprehensive handbook of calorimetry and thermal analysis |
| title_sort | comprehensive handbook of calorimetry and thermal analysis |
| topic | Análisis térmico diferencial - Manuales Calorimetría - Manuales Kalorimetrie (DE-588)4029367-1 gnd Thermoanalyse (DE-588)4135675-5 gnd |
| topic_facet | Análisis térmico diferencial - Manuales Calorimetría - Manuales Kalorimetrie Thermoanalyse |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=012849474&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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