The science and engineering of granulation processes:
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Dordrecht [u.a.]
Kluwer Academic Publishers
2004
|
| Schriftenreihe: | Particle technology series
15 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Includes index. |
| Beschreibung: | XII, 250 S. Ill., graph. Darst. |
| ISBN: | 1402018770 |
Internformat
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| 264 | 1 | |a Dordrecht [u.a.] |b Kluwer Academic Publishers |c 2004 | |
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Datensatz im Suchindex
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| adam_text | THE SCIENCE AND ENGINEERING OF GRANULATION PROCESSES JIM LITSTER THE
UNIVERSITY OF QUEENSLAND, BRISBANE, AUSTRALIA BRYAN ENNIS E&G
ASSOCIATES, NASHVILLE, TENNESSEE, U.S.A. AND LIAN LIU (ASSOCIATE EDITOR)
THE UNIVERSITY OF QUEENSLAND, BRISBANE, AUSTRALIA KLUWER ACADEMIC
PUBLISHERS DORDRECHT / BOSTON / LONDON CONTENTS PREFACE VII 1
INTRODUCTION 1 1.1 GRANULATION RATE PROCESSES 4 1.2 CONSIDERING A
GRANULATOR AS A REACTOR 6 1.3 GRANULATION AS PARTICLE DESIGN 8 1.4 HOW
TO USE THIS BOOK 9 2 PARTICLE AND GRANULE MORPHOLOGY 2.1 PARTICLE SIZE,
SHAPE AND SIZE DISTRIBUTION 12 2.1.1 PARTICLE SIZE DEFINITIONS 12 2.1.2
PARTICLE SHAPE 13 2.1.3 BASIC PARTICLE SIZE DISTRIBUTION DEFINITIONS 17
2.1.4 DIFFERENT WAYS TO REPRESENT PARTICLE SIZE DISTRIBUTIONS 20 2.1.5
MEASURES OF MEAN SIZE AND SPREAD OF THE SIZE DISTRIBUTION 22 2.1.6
PARTICLE SIZE MEASUREMENT 23 2.1.7 PARTICLE SIZE SUMMARY 24 2.2 DENSITY,
POROSITY AND PORE SIZE DISTRIBUTION 25 2.2.1 DENSITY AND POROSITY
DEFINITIONS 25 2.2.2 DENSITY MEASUREMENT 27 2.2.3 POROSITY AND PORE SIZE
DISTRIBUTION MEASUREMENT 28 2.3 GRANULE PROPERTIES 2.3.1 GRANULE SIZE
DISTRIBUTION 30 2.3.2 POROSITY AND GRANULE DENSITY 31 2.3.3 WET GRANULE
MORPHOLOGY 32 2.3.4 GRANULE PERFORMANCE PROPERTIES 32 2.4 SUMMARY 2.5
BIBLIOGRAPHY 34 2.6 NOMENCLATURE 3 WETTING, NUCLEATION AND BINDER
DISTRIBUTION 3.1 POWDER SURFACE PROPERTIES 40 3.1.1 SOME DEFINITIONS 40
3.1.2 METHODS OF MEASUREMENT 43 3.2 WETTING AND NUCLEATION REGIMES FOR
GRANULATION 52 3.2.1 DROP PENETRATION INTO POWDER BEDS 53 3.2.2 ANALYSIS
OF THE SPRAY ZONE IN GRANULATORS- THE DIMENSIONLESS 59 SPRAY FLUX 3.2.3
A NUCLEATION REGIME MAP 63 3.2.4 RELATED STUDIES ON WETTING AND
NUCLEATION 65 3.3 CONTROL OF WETTING AND NUCLEATION FOR PARTICLE DESIGN
68 IX 3.3.1 ADHESION TENSION CONTROL 69 3.3.2 OTHER POWDER AND LIQUID
PROPERTIES 69 3.3.3 SPRAY DISTRIBUTION 70 3.3.4 AGITATION INTENSITY 70
3.3.5 SIMULTANEOUS DRYING 70 3.3.6 CONCLUDING COMMENTS 71 3.4
BIBLIOGRAPHY 72 4 CONSOLIDATION, COALESCENCE AND GROWTH 4. 1 GRANULE
MECHANICS 75 4.1.1 MEASURING THE DYNAMIC YIELD STRESS OF A PARTICLE
ASSEMBLY 78 4.2 GRANULE CONSOLIDATION 82 4.2.1 A MECHANISTIC
UNDERSTANDING OF GRANULATION 84 4.2.2 EFFECT OF FORMULATION PROPERTIES
AND PROCESS CONDITIONS 86 ON CONSOLIDATION 4.2.3 GRANULE CONSOLIDATION
WITH SIMULTANEOUS DRYING 88 4.2.4 THEORETICAL MODELS FOR CONSOLIDATION
89 4.3 GRANULE COALESCENCE CRITERIA FOR NEAR ELASTIC PARTICLES 91 4.3.1
GROWTH REGIMES FOR NEAR ELASTIC GRANULES 92 4.3.2 ESTIMATING THE
CHARACTERISTIC COLLISION VELOCITY 93 4.3.3 EXAMPLES OF APPLICATION OF
THE STOKES REGIME ANALYSIS 94 4.3.4 LIMITATIONS OF THE STOKES REGIME
ANALYSIS AND FINAL REMARKS 97 4.4 GRANULE COALESCENCE CRITERIA FOR
DEFORMABLE, POROUS GRANULES 98 4.4.1 DEVELOPMENT OF COALESCENCE CRITERIA
98 4.4.2 IMPLICATIONS OF THE COALESCENCE CRITERIA 102 4.4.3 EXTENSION TO
SURFACE DRY GRANULES 103 4.4.4 COMPARISON WITH LABORATORY GRANULATION
DATA 105 4.4.5 SUMMARY 107 4.5 GRANULATION BEHAVIOUR FOR DEFORMABLE
GRANULES: A GROWTH REGIME 107 MAP 4.6 CONTROL OF GROWTH AND
CONSOLIDATION FOR PARTICLE DESIGN 112 4.6.1 ELASTIC GRANULE SYSTEMS 112
4.6.2 DEFORMABLE GRANULE SYSTEMS 113 4.7 BIBLIOGRAPHY 118 4.8
NOMENCLATURE 119 5 BREAKAGE AND ATTRITION 5.1 BREAKAGE OF WET GRANULES
121 5.1.1 EXPERIMENTAL OBSERVATIONS 121 5.1.2 PREDICTING CONDITIONS FOR
BREAKAGE 124 5.1.3 CONTROLLING GRANULE ATTRIBUTES THROUGH BREAKAGE 125
5.2 ATTRITION AND FRACTURE OF DRY GRANULES 126 5.2.1 FRACTURE PROPERTIES
OF DRY GRANULES 126 5.2.2 MEASUREMENTS OF FRACTURE PROPERTIES 128 5.2.3
EMPIRICAL CRUSH STRENGTH AND ATTRITION TESTS 131 5.2.4 BREAKAGE
MECHANISMS FOR DRY GRANULES 132 5.2.5 CASE STUDY - FLUID BED ATTRITION
OF AGGLOMERATES 134 XI 5.3 PARTICLE DESIGN FOR CONTROLLING ATTRITION AND
BREAKAGE 135 5.3.1 EFFECT OF PROCESS VARIABLES 135 5.3.2 EFFECT OF
FORMULATION PROPERTIES 137 5.3.3 CONTROLLING GRANULE DISPERSIBILITY 139
5.4 CONCLUDING COMMENTS 140 5.5 BIBLIOGRAPHY 140 5.6 NOMENCLATURE 141 6
MATHEMATICAL MODELLING OF AGGLOMERATION PROCESSES 6.1 DERIVATION OF THE
MACROSCOPIC POPULATION BALANCE 144 6.1.1 MOMENTS OF THE PB 148 6.2
KINETIC EXPRESSIONS FOR GRANULATION RATE PROCESSES 149 6.2.1 NUCLEATION
150 6.2.2 LAYERING 151 6.2.3 COALESCENCE 152 6.2.4 CONSOLIDATION 155
6.2.5 ATTRITION AND BREAKAGE 155 6.2.6 THE COMPLETE POPULATION BALANCE
FOR GRANULATION 156 6.3 SOLUTION OF THE POPULATION BALANCE EQUATION 157
6.3.1 ANALYTICAL SOLUTIONS 157 6.3.2 NUMERICAL SOLUTIONS 159 6.4 EXAMPLE
APPLICATIONS OF THE POPULATION BALANCE 162 6.4.1 GROWTH BY LAYERING 62
6.4.2 GROWTH BY COALESCENCE 164 6.4.3 EFFECT OF MIXING IN THE GRANULATOR
167 6.5 SUMMARY 69 6.6 REFERENCES 69 6.7 NOMENCLATURE ^0 7
CLASSIFICATION AND CHOICE OF SIZE ENLARGEMENT EQUIPMENT 7.1
CLASSIFICATION OF SIZE ENLARGEMENT EQUIPMENT 76 7.2 FUTURE DIRECTIONS
IN GRANULATION PROCESS EQUIPMENT 177 7.3 BIBLIOGRAPHY 178 8 TUMBLING
GRANULATION 8.1 INTRODUCTION 179 8.2 DISC GRANULATORS 179 8.2.1 GRANULE
HOLD UP, MIXING AND SEGREGATION ON THE DISC 180 8.3 DRUM GRANULATORS L84
8.3.1 GRANULE HOLD UP, MIXING AND SEGREGATION 185 8.3.2 GRANULATION DRUM
CIRCUITS 85 8.4 GRANULATION RATE PROCESSES 86 8.4.1 NUCLEATION 186
8.4.2 CONSOLIDATION L87 8.4.3 GRANULE GROWTH BY COALESCENCE 188 8.4.4
LAYERING 191 XLL 8.5 SCALE UP AND OPERATION OF TUMBLING GRANULATORS 192
8.6 VARIATIONS ON A THEME 194 8.7 BIBLIOGRAPHY 194 8.8 NOMENCLATURE 194
9 FLUIDISED GRANULATORS 9.1 HYDRODYNAMICS OF FLUIDISED BEDS 198 9.1.1
MINIMUM FLUIDISATION VELOCITY AND PRESSURE DROP 200 9.1.2 TYPES OF
FLUIDISATION BEHAVIOUR 201 9.1.3 THE ROLE OF BUBBLES IN FLUIDISED BEDS
202 9.2 MASS AND ENERGY BALANCES 204 9.3 GRANULATION MECHANISMS AND RATE
PROCESSES 205 9.3.1 NUCLEATION 206 9.3.2 COALESCENCE 208 9.3.3 LAYERING
211 9.3.4 CONSOLIDATION 211 9.3.5 ATTRITION 212 9.3.6 SUMMARY 212 9.4
SCALE UP OF FLUIDISED BED GRANULATORS 213 9.5 OPERATION OF FLUIDISED BED
GRANULATORS 214 9.6 DRAFT TUBE AND SPOUTED BED COATERS 215 9.7
CONCLUDING COMMENTS 218 9.8 BIBLIOGRAPHY 219 9.9 NOMENCLATURE 219 10
MIXER GRANULATORS 10.1 INTRODUCTION 221 10.2 DESCRIPTION OF MIXER
GRANULATION EQUIPMENT 222 10.2.1 HIGH SHEAR MIXER GRANULATORS 222 10.2.2
LOW SHEAR MIXER GRANULATORS 226 10.3 POWDER FLOW IN MIXER GRANULATORS
226 10.3.1 POWDER FLOW IN A VERTICAL SHAFT MIXER 227 10.3.2 POWDER FLOW
IN HORIZONTAL AXIS LODIGE GRANULATOR 228 10.4 GRANULATION RATE PROCESSES
IN MIXER GRANULATORS 230 10.4.1 WETTING AND NUCLEATION 230 CASE STUDY 1
232 10.4.2 CONSOLIDATION AND GROWTH 234 10.4.3 GRANULE BREAKAGE 235 10.5
SCALE UP OF MIXER GRANULATORS 237 10.5.1 SCALE UP OF A VERTICAL SHAFT
MIXER 238 CASE STUDY 2 240 10.6 INSTRUMENTATION AND CONTROL IN MIXERS
242 10.7 SUMMARY 246 10.8 BIBLIOGRAPHY 246 10.9 NOMENCLATURE 247 INDEX
249
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| indexdate | 2024-07-09T19:57:52Z |
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| isbn | 1402018770 |
| language | English |
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| spelling | Litster, Jim Verfasser aut The science and engineering of granulation processes Jim Litster ; Bryan Ennis and Lian Liu (associate ed.) Dordrecht [u.a.] Kluwer Academic Publishers 2004 XII, 250 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Particle technology series 15 Includes index. Korrelvorming gtt Poeder (procestechnologie) gtt Granulation Particles Granulieren (DE-588)4158043-6 gnd rswk-swf Granulieren (DE-588)4158043-6 s DE-604 Ennis, Bryan Verfasser aut Particle technology series 15 (DE-604)BV013647981 15 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=012799171&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Litster, Jim Ennis, Bryan The science and engineering of granulation processes Particle technology series Korrelvorming gtt Poeder (procestechnologie) gtt Granulation Particles Granulieren (DE-588)4158043-6 gnd |
| subject_GND | (DE-588)4158043-6 |
| title | The science and engineering of granulation processes |
| title_auth | The science and engineering of granulation processes |
| title_exact_search | The science and engineering of granulation processes |
| title_full | The science and engineering of granulation processes Jim Litster ; Bryan Ennis and Lian Liu (associate ed.) |
| title_fullStr | The science and engineering of granulation processes Jim Litster ; Bryan Ennis and Lian Liu (associate ed.) |
| title_full_unstemmed | The science and engineering of granulation processes Jim Litster ; Bryan Ennis and Lian Liu (associate ed.) |
| title_short | The science and engineering of granulation processes |
| title_sort | the science and engineering of granulation processes |
| topic | Korrelvorming gtt Poeder (procestechnologie) gtt Granulation Particles Granulieren (DE-588)4158043-6 gnd |
| topic_facet | Korrelvorming Poeder (procestechnologie) Granulation Particles Granulieren |
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