Catalytic distillation: dynamic modelling, simulation, and experimental validation
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Düsseldorf
VDI-Verl.
2003
|
| Edition: | Als Ms. gedr. |
| Series: | Fortschritt-Berichte VDI
Reihe 3, Verfahrenstechnik ; 784 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XII, 133 S. graph. Darst. |
| ISBN: | 3183784033 |
Staff View
MARC
| LEADER | 00000nam a2200000 cb4500 | ||
|---|---|---|---|
| 001 | BV017401371 | ||
| 003 | DE-604 | ||
| 005 | 20121004 | ||
| 007 | t | ||
| 008 | 030811s2003 d||| m||| 00||| eng d | ||
| 016 | 7 | |a 968410065 |2 DE-101 | |
| 020 | |a 3183784033 |9 3-18-378403-3 | ||
| 035 | |a (OCoLC)249430773 | ||
| 035 | |a (DE-599)BVBBV017401371 | ||
| 040 | |a DE-604 |b ger |e rakwb | ||
| 041 | 0 | |a eng | |
| 049 | |a DE-91G |a DE-210 |a DE-634 |a DE-83 | ||
| 084 | |a VN 7227 |0 (DE-625)147611:260 |2 rvk | ||
| 100 | 1 | |a Noeres, Christoph |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Catalytic distillation |b dynamic modelling, simulation, and experimental validation |c Christoph Noeres |
| 250 | |a Als Ms. gedr. | ||
| 264 | 1 | |a Düsseldorf |b VDI-Verl. |c 2003 | |
| 300 | |a XII, 133 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Fortschritt-Berichte VDI : Reihe 3, Verfahrenstechnik |v 784 | |
| 502 | |a Zugl.: Dortmund, Univ., Diss., 2002 | ||
| 650 | 4 | |a Reaktivdestillation - Katalyse | |
| 650 | 0 | 7 | |a Katalyse |0 (DE-588)4029921-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Reaktivdestillation |0 (DE-588)4491776-4 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Reaktivdestillation |0 (DE-588)4491776-4 |D s |
| 689 | 0 | 1 | |a Katalyse |0 (DE-588)4029921-1 |D s |
| 689 | 0 | |5 DE-604 | |
| 830 | 0 | |a Fortschritt-Berichte VDI |v Reihe 3, Verfahrenstechnik ; 784 |w (DE-604)BV001897067 |9 784 | |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010485640&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-010485640 | |
Record in the Search Index
| _version_ | 1808135277418381312 |
|---|---|
| adam_text |
CONTENTS
V
CONTENTS
CONTENTS
V
NOTATION
VII
1
INTRODUCTION
AND
OBJECTIVES
1
2
STATE
OF
THE
ART
4
2.1
REACTIVE
SEPARATION
PROCESSES
4
2.2
INTERNALS
FOR
CATALYTIC
DISTILLATION
10
2.3
MODELLING
OF
REACTIVE
DISTILLATION
14
2.3.1
EQUILIBRIUM
STAGE
MODEL
15
2.3.2
RATE-BASED
MODELS
15
2.3.3
CHEMICAL
REACTION
18
2.3.4
FLOW
MODELS
20
2.3.5
FLOW
REGIMES
IN
PACKED
COLUMNS
29
2.3.6
DYNAMIC
MODELLING
31
3
DYNAMIC
MODELLING
OF
CATALYTIC
DISTILLATION
PROCESSES
32
3.1
DYNAMIC
RATE-BASED
MODEL
32
3.1.1
DYNAMIC
BALANCES
33
3.1.2
RATE
EQUATIONS
35
3.1.3
CHEMICAL
REACTION
36
3.2
PERIPHERAL
COLUMN
ELEMENTS
37
3.3
NUMERICAL
SOLUTION
38
3.4
CONCLUDING
REMARKS
40
4
CHARACTERISTICS
OF
THE
CATALYTIC
PACKING
MULTIPAK
41
4.1
EXPERIMENTAL
EQUIPMENT
AND
PROCEDURE
41
4.1.1
CATALYTIC
PACKING
MULTIPAK
41
4.1.2
EXPERIMENTAL
SET-UP
&
METHODOLOGY
42
4.2
EXPERIMENTAL
RESULTS
46
4.2.1
NON-IDEAL
FLOW
BEHAVIOUR
46
VI
CONTENTS
4.2.2
LIQUID
HOLD-UP,
PRESSURE
DROP
&
MASS
TRANSFER
51
4.3
CONCLUDING
REMARKS
52
5
CHEMICAL
REACTION
SYSTEMS
55
5.1
REACTIVE
TEST
SYSTEM
SELECTION
55
5.2
METHYL
ACETATE
SYNTHESIS
56
5.2.1
REACTION
SYSTEM
56
5.2.2
EXPERIMENTAL
SET-UP
57
5.2.3
ADSORPTION
EQUILIBRIA
57
5.2.4
REACTION
KINETICS
61
5.3
DIETHYL
CARBONATE
SYNTHESIS
66
5.3.1
REACTION
SYSTEM
66
5.3.2
REACTION
KINETICS
66
5.4
CONCLUDING
REMARKS
69
6
EXPERIMENTAL
CD
MODEL
VALIDATION
-
METHYL
ACETATE
SYNTHESIS
70
6.1
EXPERIMENTAL
SET-UP
70
6.2
RESULTS
71
6.3
CONCLUDING
REMARKS
81
7
THEORETICAL
ANALYSIS
82
7.1
METHYL
ACETATE
SYNTHESIS
82
7.1.1
STEADY-STATE
AND
DYNAMIC
PROCESS
BEHAVIOUR
83
7.1.2
SENSITIVITY
ANALYSIS
84
7.2
DIETHYL
CARBONATE
SYNTHESIS
91
7.2.1
STEADY-STATE
AND
DYNAMIC
PROCESS
BEHAVIOUR
92
7.2.2
SENSITIVITY
ANALYSIS
98
7.3
CONCLUDING
REMARKS
104
8
CONCLUSIONS
AND
OUTLOOK
106
A
EXPERIMENTAL
DATA
110
A.L
CATALYST
SPECIFICATION
OF
LEWATIT
K2621
110
A.2
CATALYST
PREPARATION
111
A.3
REACTION
KINETICS
OF
METHYL
ACETATE
SYNTHESIS
113
A.4
COMPOSITION
ANALYSIS
113
A.4.1
GAS-CHROMATOGRAPH
(GC)
113
A.4.2
NEAR
INFRARED
SPECTROMETER
(NIR)
116
A.5
HEAT
LOSSES
117
A.6
PHOTOS
OF
EXPERIMENTAL
SET-UPS
118
REFERENCES
121 |
| any_adam_object | 1 |
| author | Noeres, Christoph |
| author_facet | Noeres, Christoph |
| author_role | aut |
| author_sort | Noeres, Christoph |
| author_variant | c n cn |
| building | Verbundindex |
| bvnumber | BV017401371 |
| classification_rvk | VN 7227 |
| ctrlnum | (OCoLC)249430773 (DE-599)BVBBV017401371 |
| discipline | Chemie / Pharmazie |
| edition | Als Ms. gedr. |
| format | Thesis Book |
| fullrecord | <?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>00000nam a2200000 cb4500</leader><controlfield tag="001">BV017401371</controlfield><controlfield tag="003">DE-604</controlfield><controlfield tag="005">20121004</controlfield><controlfield tag="007">t</controlfield><controlfield tag="008">030811s2003 d||| m||| 00||| eng d</controlfield><datafield tag="016" ind1="7" ind2=" "><subfield code="a">968410065</subfield><subfield code="2">DE-101</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">3183784033</subfield><subfield code="9">3-18-378403-3</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)249430773</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)BVBBV017401371</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-604</subfield><subfield code="b">ger</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1="0" ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-91G</subfield><subfield code="a">DE-210</subfield><subfield code="a">DE-634</subfield><subfield code="a">DE-83</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">VN 7227</subfield><subfield code="0">(DE-625)147611:260</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Noeres, Christoph</subfield><subfield code="e">Verfasser</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Catalytic distillation</subfield><subfield code="b">dynamic modelling, simulation, and experimental validation</subfield><subfield code="c">Christoph Noeres</subfield></datafield><datafield tag="250" ind1=" " ind2=" "><subfield code="a">Als Ms. gedr.</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">Düsseldorf</subfield><subfield code="b">VDI-Verl.</subfield><subfield code="c">2003</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">XII, 133 S.</subfield><subfield code="b">graph. Darst.</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="490" ind1="1" ind2=" "><subfield code="a">Fortschritt-Berichte VDI : Reihe 3, Verfahrenstechnik</subfield><subfield code="v">784</subfield></datafield><datafield tag="502" ind1=" " ind2=" "><subfield code="a">Zugl.: Dortmund, Univ., Diss., 2002</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Reaktivdestillation - Katalyse</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Katalyse</subfield><subfield code="0">(DE-588)4029921-1</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Reaktivdestillation</subfield><subfield code="0">(DE-588)4491776-4</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="655" ind1=" " ind2="7"><subfield code="0">(DE-588)4113937-9</subfield><subfield code="a">Hochschulschrift</subfield><subfield code="2">gnd-content</subfield></datafield><datafield tag="689" ind1="0" ind2="0"><subfield code="a">Reaktivdestillation</subfield><subfield code="0">(DE-588)4491776-4</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="1"><subfield code="a">Katalyse</subfield><subfield code="0">(DE-588)4029921-1</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="830" ind1=" " ind2="0"><subfield code="a">Fortschritt-Berichte VDI</subfield><subfield code="v">Reihe 3, Verfahrenstechnik ; 784</subfield><subfield code="w">(DE-604)BV001897067</subfield><subfield code="9">784</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">DNB Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010485640&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="943" ind1="1" ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-010485640</subfield></datafield></record></collection> |
| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV017401371 |
| illustrated | Illustrated |
| indexdate | 2024-08-23T00:16:13Z |
| institution | BVB |
| isbn | 3183784033 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-010485640 |
| oclc_num | 249430773 |
| open_access_boolean | |
| owner | DE-91G DE-BY-TUM DE-210 DE-634 DE-83 |
| owner_facet | DE-91G DE-BY-TUM DE-210 DE-634 DE-83 |
| physical | XII, 133 S. graph. Darst. |
| publishDate | 2003 |
| publishDateSearch | 2003 |
| publishDateSort | 2003 |
| publisher | VDI-Verl. |
| record_format | marc |
| series | Fortschritt-Berichte VDI |
| series2 | Fortschritt-Berichte VDI : Reihe 3, Verfahrenstechnik |
| spelling | Noeres, Christoph Verfasser aut Catalytic distillation dynamic modelling, simulation, and experimental validation Christoph Noeres Als Ms. gedr. Düsseldorf VDI-Verl. 2003 XII, 133 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Fortschritt-Berichte VDI : Reihe 3, Verfahrenstechnik 784 Zugl.: Dortmund, Univ., Diss., 2002 Reaktivdestillation - Katalyse Katalyse (DE-588)4029921-1 gnd rswk-swf Reaktivdestillation (DE-588)4491776-4 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Reaktivdestillation (DE-588)4491776-4 s Katalyse (DE-588)4029921-1 s DE-604 Fortschritt-Berichte VDI Reihe 3, Verfahrenstechnik ; 784 (DE-604)BV001897067 784 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010485640&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Noeres, Christoph Catalytic distillation dynamic modelling, simulation, and experimental validation Fortschritt-Berichte VDI Reaktivdestillation - Katalyse Katalyse (DE-588)4029921-1 gnd Reaktivdestillation (DE-588)4491776-4 gnd |
| subject_GND | (DE-588)4029921-1 (DE-588)4491776-4 (DE-588)4113937-9 |
| title | Catalytic distillation dynamic modelling, simulation, and experimental validation |
| title_auth | Catalytic distillation dynamic modelling, simulation, and experimental validation |
| title_exact_search | Catalytic distillation dynamic modelling, simulation, and experimental validation |
| title_full | Catalytic distillation dynamic modelling, simulation, and experimental validation Christoph Noeres |
| title_fullStr | Catalytic distillation dynamic modelling, simulation, and experimental validation Christoph Noeres |
| title_full_unstemmed | Catalytic distillation dynamic modelling, simulation, and experimental validation Christoph Noeres |
| title_short | Catalytic distillation |
| title_sort | catalytic distillation dynamic modelling simulation and experimental validation |
| title_sub | dynamic modelling, simulation, and experimental validation |
| topic | Reaktivdestillation - Katalyse Katalyse (DE-588)4029921-1 gnd Reaktivdestillation (DE-588)4491776-4 gnd |
| topic_facet | Reaktivdestillation - Katalyse Katalyse Reaktivdestillation Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010485640&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV001897067 |
| work_keys_str_mv | AT noereschristoph catalyticdistillationdynamicmodellingsimulationandexperimentalvalidation |